Science & Technology Review
|
2015, 33(9): 35-39
• Articles •
Preparation and characterization of activated carbon based on external wall insulation board residual material by alkali activation method
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GAO Lijuan1, WU Hongyun1, WU Hongxia2, XU Yan1, ZHAO Xuefei1
Affiliations
1. School of Chemical Engineering, University of Science and Technology of Liaoning, Anshan 114051, China;
2. Natural Gas Development Company of Qinghai Oilfield, Geermu 816000, China
Published: 2015-05-13
doi: 10.3981/j.issn.1000-7857.2015.09.005
Outline
Activated carbons are prepared from the external wall insulation board residual material by the alkali activation method. The performance of the activated carbon is characterized by the FT-IR spectroscopy, the X-ray diffraction, the BET specific surface area, the pore size distribution and the iodine adsorption value. The external wall insulation board is heated from the room temperature to 800℃ at the rate of 10℃/min under the atmosphere of nitrogen and maintains for 30 min. Then it cools to the ambient temperature to obtain charcoal powder. At the ratio of 4∶1(alkali/carbon), the charcoal powder is impregnated for 8 h with 0.1 g/mL KOH solution and is transferred to the activation furnace after being heated to remove water. The charcoal powder is heated from the room temperature to 800℃ at the rate of 10℃/min under the atmosphere of nitrogen, is activated for 60 min, naturally cools down to the room temperature, is washed with 5% hydrochloric acid and water to neutralize, and then is dried to a state of constant weight at 120℃. In the process, the index parameters of the activated carbon are found to be as follows: The iodine value is 2300.27 mg/g, the specific surface area is 1293.45 m2g, the average pore size is 2.4 nm, which is mainly composed of micro pores and small middle pores.
external wall insulation board residual material
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alkali activation method
/
iodine value
/
specific surface area
/
pore size distribution
高丽娟, 吴红运, 吴红霞, 徐妍, 赵雪飞.
碱活化法制备外墙保温板残料活性炭及表征.
科技导报,
2015
, 33
(9)
: 35
-39
.
DOI: 10.3981/j.issn.1000-7857.2015.09.005
GAO Lijuan, WU Hongyun, WU Hongxia, XU Yan, ZHAO Xuefei.
Preparation and characterization of activated carbon based on external wall insulation board residual material by alkali activation method[J].
Science & Technology Review,
2015
, 33
(9)
: 35
-39
.
DOI: 10.3981/j.issn.1000-7857.2015.09.005
Year 2015 volume 33 Issue 9
PDF
570
212
Cite this Article
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Article Info
doi: 10.3981/j.issn.1000-7857.2015.09.005
- Receive Date:2014-11-28
- Online Date:2015-05-15
- Published:2015-05-13