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Optimization of the Preparation Process of Sea Buckthorn Seed Oil Microcapsules by Spray Drying and Its Physicochemical Properties and Structural Characterization
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Libin ZHU1, 2, Xin LIU1, 3, Guangcai NIU1, 2, *, Dan ZHU4, *, Wenyi WEI1, 2, Jian JIA1, 2, Sensen WANG1, 2
Science and Technology of Food Industry | 2026, 47(18) : 192 - 201
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Science and Technology of Food Industry | 2026, 47(18): 192-201
• Process Innovation and Intelligent Manufacturing •
Optimization of the Preparation Process of Sea Buckthorn Seed Oil Microcapsules by Spray Drying and Its Physicochemical Properties and Structural Characterization
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Libin ZHU1, 2, Xin LIU1, 3, Guangcai NIU1, 2, *, Dan ZHU4, *, Wenyi WEI1, 2, Jian JIA1, 2, Sensen WANG1, 2
Affiliations
  • 1College of Food Science and Engineering, Heilongjiang Bayi Agricultural University, Daqing 163319, China
  • 2Agri-food Processing and Engineering Technology Research Center of Heilongjiang Province, Daqing 163319, China
  • 3Shenyang Food and Drug Inspection Institute, Shenyang 110124, China
  • 4College of Life Science and Biotechnology, Heilongjiang Bayi Agricultural University, Daqing 163319, China
Published: 2026-09-15 doi: 10.13386/j.issn1002-0306.2025070378
Outline
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To develop new products of sea buckthorn seed oil, the microencapsulated products were prepared by spray drying, and their physicochemical properties and structural characteristics were analyzed. The preparation process was optimized by single factor experiment and response surface experiment. The results showed that the optimal preparation parameters were as follows: inlet air temperature was 158 ℃, inlet air volume was 0.63 m3/min, feed temperature was 70 ℃ and feed rate was 4.80 mL/min. Under these conditions, the embedding rate of microcapsules was 91.31%. The physicochemical properties showed that the moisture content of the microcapsule product was 3.47%, the angle of repose was 37.2°, and the solubility was 96.52%. The results of thermal analysis showed that its glass transition temperature was 68.3 ℃, which indicated that it had good thermal stability. The results of microstructure determination showed that the microcapsules were spherical or ellipsoidal, with uniform particle size distribution (1~10 μm), smooth and dense surface and intact structure. The successful embedding of microcapsules was further confirmed by infrared spectroscopy. The results of storage stability showed that microencapsulation improved the storage stability of sea buckthorn seed oil and prolonged its storage time. This research provides an effective technological solution for the development of functional foods with sea buckthorn seed oil.

sea buckthorn seed oil  /  microcapsules  /  spray drying  /  physicochemical properties  /  structural characterization
朱立斌, 刘鑫, 牛广财, 朱丹, 魏文毅, 贾建, 王森森. 沙棘籽油微胶囊喷雾干燥法制备工艺优化及其理化性质与结构表征. 食品工业科技, 2026 , 47 (18) : 192 -201 . DOI: 10.13386/j.issn1002-0306.2025070378
Libin ZHU, Xin LIU, Guangcai NIU, Dan ZHU, Wenyi WEI, Jian JIA, Sensen WANG. Optimization of the Preparation Process of Sea Buckthorn Seed Oil Microcapsules by Spray Drying and Its Physicochemical Properties and Structural Characterization[J]. Science and Technology of Food Industry, 2026 , 47 (18) : 192 -201 . DOI: 10.13386/j.issn1002-0306.2025070378
Year 2026 volume 47 Issue 18
87
39
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doi: 10.13386/j.issn1002-0306.2025070378
  • Receive Date:2025-08-01
  • Online Date:2026-10-24
  • Published:2026-09-15
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  • Received:2025-08-01
Affiliations
    1College of Food Science and Engineering, Heilongjiang Bayi Agricultural University, Daqing 163319, China
    2Agri-food Processing and Engineering Technology Research Center of Heilongjiang Province, Daqing 163319, China
    3Shenyang Food and Drug Inspection Institute, Shenyang 110124, China
    4College of Life Science and Biotechnology, Heilongjiang Bayi Agricultural University, Daqing 163319, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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