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Antioxidant properties and fatty acid content of walnut oil from different matrices based on gas chromatography-mass spectrometry analysis
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Wen-Fang YAN1, Kong YANG1, *, Yu-Xin ZHANG1, Hai-Ying YANG2, Ze-Qian SONG3, Yu-Fen PAN3, Yong WU3, Ting LI3, Heng LIU4
Journal of Food Safety & Quality | 2025, 16(10) : 19 - 27
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Journal of Food Safety & Quality | 2025, 16(10): 19-27
Highlight: The 9th Academic Conference Papers on Food Quality, Safety and Intelligent Testing
Antioxidant properties and fatty acid content of walnut oil from different matrices based on gas chromatography-mass spectrometry analysis
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Wen-Fang YAN1, Kong YANG1, *, Yu-Xin ZHANG1, Hai-Ying YANG2, Ze-Qian SONG3, Yu-Fen PAN3, Yong WU3, Ting LI3, Heng LIU4
Affiliations
  • 1. School of Engineering, Dali Agricultural and Forestry Vocational and Technical College, Dali 671003, China
  • 2. College of Chemistry and Environment, Yunnan Minzu University, Kunming 650500, China
  • 3. Institute of Health Science and Technology, Dianxi University of Applied Sciences, Dali 671006, China
  • 4. College of Pharmacy, Dali University, Dali 671000, China
Published: 2025-05-25 doi: 10.19812/j.cnki.jfsq11-5956/ts.20250319002
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Objective To explore the antioxidant effects and fatty acid content of walnut oil derived from different substrates. Methods Gas chromatography-mass spectrometry (GC-MS) was used to analyze the fatty acid content in walnut oil and unqualified walnut oil at different pressing temperatures. Single variable control method was used to study the antioxidant effects of walnut oil with different air content. After adding a complex of natural antioxidants, fat soluble rosemary at 0.04 g/100 g and vitamin E at 0.1 g/100 g, 2 sets of experiments were conducted. The first set contained 100, 200, 300, 400 and 500 mL oil samples in 500 mL glass bottles, while the second set contained 100 mL oil samples in 100, 250 and 500 mL glass bottles. The samples were rapidly oxidized in a constant temperature drying oven at 63 ℃±1 ℃ and kept at that temperature for 70 days. The aroma, taste, peroxide value and acid value of the oil samples were measured every 10 days. Results The fatty acids in walnut oil were palmitic acid, linoleic acid, stearic acid and oleic acid. The content of fatty acids varies with storage time and pressing temperature, and the unqualified oil sample didn’t contain oleic acid. The walnut oil pressure pressing temperature of 130-140 ℃ had the best quality. The 2 sets of experiments had confirmed that walnut oil with lower air content could be stored for a longer period of time, up to a maximum of 100 days. Conclusion The less contact with air during storage or the decrease in the ratio of initial air volume to initial oil sample volume, the longer the shelf life. The conduct of this study provides a reference for the storage conditions of walnut oil.

walnut oil  /  gas chromatography-mass spectrometry  /  air content  /  antioxidant
Wen-Fang YAN, Kong YANG, Yu-Xin ZHANG, Hai-Ying YANG, Ze-Qian SONG, Yu-Fen PAN, Yong WU, Ting LI, Heng LIU. Antioxidant properties and fatty acid content of walnut oil from different matrices based on gas chromatography-mass spectrometry analysis[J]. Journal of Food Safety & Quality, 2025 , 16 (10) : 19 -27 . DOI: 10.19812/j.cnki.jfsq11-5956/ts.20250319002
Year 2025 volume 16 Issue 10
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doi: 10.19812/j.cnki.jfsq11-5956/ts.20250319002
  • Receive Date:2025-03-19
  • Online Date:2025-07-15
  • Published:2025-05-25
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  • Received:2025-03-19
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Affiliations
    1. School of Engineering, Dali Agricultural and Forestry Vocational and Technical College, Dali 671003, China
    2. College of Chemistry and Environment, Yunnan Minzu University, Kunming 650500, China
    3. Institute of Health Science and Technology, Dianxi University of Applied Sciences, Dali 671006, China
    4. College of Pharmacy, Dali University, Dali 671000, China
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表12种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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