Article(id=1319291167720723368, tenantId=1146029695717560320, journalId=1255847919539208197, issueId=1319291166823142311, articleNumber=null, orderNo=null, doi=10.13193/j.issn.1673-7717.2026.09.002, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1792473125628, onlineDateStr=2026-10-20, pubDate=1788969600000, pubDateStr=2026-09-10, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792473125628, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792473125628, creator=13701087609, updateTime=1792473125628, updator=13701087609, issue=Issue{id=1319291166823142311, tenantId=1146029695717560320, journalId=1255847919539208197, year='2026', volume='44', issue='9', pageStart='1', pageEnd='258', issueExtLink='null', onlineDate='null', pubDate='1788969600000', pubDateStr='2026-09-10', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1792473125414, creator='13701087609', updateTime=1792473357559, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1319292140618896016, tenantId=1146029695717560320, journalId=1255847919539208197, issueId=1319291166823142311, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1319292140618896017, tenantId=1146029695717560320, journalId=1255847919539208197, issueId=1319291166823142311, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=8, endPage=13, ext={EN=ArticleExt(id=1319291167972381609, articleId=1319291167720723368, tenantId=1146029695717560320, journalId=1255847919539208197, language=EN, title=Preparation and Evaluation of Moisture-resistant Intermediates of Yuzhu (
Polygonatum odoratum) Polysaccharide Based on Ca
2+ Crosslinking Under Guidance of Condensed Matter Theory, columnId=1256183423710970242, journalTitle=Chinese Archives of Traditional Chinese Medicine, columnName=New Opinion of Ph.D. Supervisor, runingTitle=null, highlight=null, articleAbstract=
Objective Under the guidance of condensed matter theory, calcium salt cross-linking is used to prepare moisture-resistant intermediates of Yuzhu (Polygonatum odoratum) polysaccharide, reduce its hygroscopicity, improve moisture resistance and provide new methods for moisture-proofing of traditional Chinese medicine extracts.
Methods Single-factor experiment investigated the effects of cross-linking agent type and dosage, polysaccharide concentration, stirring time, stirring speed and stirring temperature on moisture absorption rate of moisture-resistant intermediates, and used the response surface method to optimize the prescription and process. The equilibrium moisture absorption rate and critical relative humidity of moisture-proof intermediates were measured, and the glass transition temperature Tg was measured by differential scanning calorimeter (DSC), the microscopic morphology was observed by scanning electron microscope (SEM), and the rheometer was used to measure the apparent viscosity and viscoelasticity.
Results The type and dosage of cross-linking agent, polysaccharide concentration and stirring temperature all had significant effects on the moisture absorption rate of the intermediate. The optimal prescription and process were 5.0% calcium hydrogen phosphate, polysaccharide concentration 0.6 g/mL and stirring temperature 50 ℃. The evaluation results of moisture-resistant intermediates showed that the equilibrium moisture absorption rates of polysaccharides, polysaccharides+CaHPO4 and moisture-resistant intermediates were 22.87%, 18.44% and 15.04%, respectively, with critical relative humidity of 51.97%, 56.53% and 66.32%, respectively, and the values of Tg were 63.5 ℃, 68.5 ℃ and 80.0 ℃, respectively. SEM showed that moisture-resistant intermediates of Polygonatum odoratum polysaccharide had a large particle size and adhesions between the particles. The rheological analysis has found that the apparent viscosity of moisture-resistant intermediates of Yuzhu (Polygonatum odoratum) polysaccharide and the elasticity increased.
Conclusion Traditional Chinese medicine extracts with polymers as the active ingredient can change their condensed state structure through cross-linking, thereby reducing hygroscopicity and improving moisture resistance.
, authors=Huasheng YANG, Yawen DUAN, Bilian DENG, Yin XIAO, Ruige CHU, Lu WU, authorsList=Huasheng YANG, Yawen DUAN, Bilian DENG, Yin XIAO, Ruige CHU, Lu WU, authorCompany=null, correspAuthors=Ruige CHU, Lu WU, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319291168278565802, articleId=1319291167720723368, tenantId=1146029695717560320, journalId=1255847919539208197, language=CN, title=凝聚态理论指导下基于Ca
2+交联的玉竹多糖防潮中间体的制备及评价, columnId=1256183426563096985, journalTitle=中华中医药学刊, columnName=博士导师新论, runingTitle=null, highlight=null, articleAbstract=
目的 在凝聚态理论指导下采用钙盐交联制备玉竹多糖中间体，降低其吸湿性，提高防潮性能，为中药浸膏的防潮提供新方法。
方法 单因素实验考察交联剂种类及用量、多糖浓度及搅拌时间、速度、温度对防潮中间体吸湿率的影响，采用响应面法优化处方及工艺。测定防潮中间体的平衡吸湿率及临界相对湿度，采用差示扫描量热法（differential scanning calorimetry，DSC）测定玻璃化转变温度（Tg），扫描电镜（Scanning Electron Microscope，SEM）观察微观形态，流变仪测定表观黏度和黏弹性。
结果 交联剂种类及用量、多糖浓度、搅拌温度对中间体吸湿率均有显著影响，其最优处方及工艺：磷酸氢钙5.0%，多糖浓度0.6 g/mL、搅拌温度50 ℃；防潮中间体评价结果显示，多糖、多糖+磷酸氢钙、防潮中间体的平衡吸湿率分别为22.87%、18.44%、15.04%，临界相对湿度分别为51.97%、56.53%、66.32%，Tg分别为63.5 ℃、68.5 ℃、80.0 ℃；SEM显示玉竹多糖防潮中间体粒径较大，且颗粒之间有粘连；流变学分析发现，玉竹多糖防潮中间体表观黏度增加，弹性增加。
结论 以高分子为有效成分的中药浸膏，可通过交联改变其凝聚态结构，进而降低吸湿性，提高防潮性能。
, authors=杨华生, 段亚文, 邓碧莲, 肖音, 楚瑞阁, 吴璐, authorsList=杨华生, 段亚文, 邓碧莲, 肖音, 楚瑞阁, 吴璐, authorCompany=null, correspAuthors=楚瑞阁, 吴璐, authorNote=
杨华生（1974-），男，湖南衡阳人，教授，博士研究生导师，博士，研究方向：传统中医药理论及中药制剂。
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杨华生（1974-），男，湖南衡阳人，教授，博士研究生导师，博士，研究方向：传统中医药理论及中药制剂。
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杨华生（1974-），男，湖南衡阳人，教授，博士研究生导师，博士，研究方向：传统中医药理论及中药制剂。
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