Article(id=1317125576062775549, tenantId=1146029695717560320, journalId=1255847919539208197, issueId=1317125500041015883, articleNumber=null, orderNo=null, doi=10.13193/j.issn.1673-7717.2026.02.040, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1791956808342, onlineDateStr=2026-10-14, pubDate=1770652800000, pubDateStr=2026-02-10, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1791956808342, onlineIssueDateStr=2026-10-14, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1791956808342, creator=13701087609, updateTime=1791956808342, updator=13701087609, issue=Issue{id=1317125500041015883, tenantId=1146029695717560320, journalId=1255847919539208197, year='2026', volume='44', issue='2', pageStart='1', pageEnd='258', issueExtLink='null', onlineDate='null', pubDate='1770652800000', pubDateStr='2026-02-10', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1791956790217, creator='13701087609', updateTime=1791958795145, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1317133909368877755, tenantId=1146029695717560320, journalId=1255847919539208197, issueId=1317125500041015883, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1317133909373072060, tenantId=1146029695717560320, journalId=1255847919539208197, issueId=1317125500041015883, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=230, endPage=233, ext={EN=ArticleExt(id=1317125576264102142, articleId=1317125576062775549, tenantId=1146029695717560320, journalId=1255847919539208197, language=EN, title=Uncertainty Evaluation of Determination of Benzene Dichloro-Diphenyl-Trichloroethane（DDT）in Baishao（Paeoniae Radix Alba）by Gas Chromatography-Tandem Mass Spectrometry, columnId=1256183365644968140, journalTitle=Chinese Archives of Traditional Chinese Medicine, columnName=Platform of Provincial Project, runingTitle=null, highlight=null, articleAbstract=

Based on“method for the determination of multiple residues of prohibited pesticides in medicinal materials and herbal slices（Plants）” in Chinese Pharmacopoeia（2020 edition），the uncertainty in determination of benzene dichloro-diphenyl-trichloroethane（DDT）residues in Baishao（Paeoniae Radix Alba）was evaluated by gas chromatography-tandem mass spectrometry（GC-MS/MS）was carried out. The measurement mathematical model was established. Source analysis including preparation of standard solution，sample preparation，measurement repeatability，standard curve，recovery and GC-MS/MS. By calculating and synthesizing each uncertainty component，the measured result of 4，4’-DDE，2，4’-DDT，4，4’-DDD and 4，4’-DDT can be respectively reported as（0.14±0.01），（0.13±0.01），（0.14±0.01），（0.13±0.03）mg·kg^-1（k=2）. The uncertainty of the determination result was mainly affected by the uncertainty of standard curve，standard solution preparation.

, authors=Mei YAN, Qin HE, authorsList=Mei YAN, Qin HE, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1317125576582869248, articleId=1317125576062775549, tenantId=1146029695717560320, journalId=1255847919539208197, language=CN, title=气相色谱-串联质谱法测定白芍中滴滴涕的不确定度评定, columnId=1256183369033965799, journalTitle=中华中医药学刊, columnName=省级项目平台, runingTitle=null, highlight=null, articleAbstract=

对气相色谱-串联质谱法（GC-MS/MS）测定白芍中禁用的滴滴涕（DDT）残留量的不确定度进行评定，参考《中华人民共和国药典》（2020版）“药材及饮片（植物类）中禁用农药多残留测定方法”，建立测量数学模型，对不确定度来源进行分析，包括标准溶液配制、样品制备、测量重复性、标准曲线、气相色谱-串联质谱仪、回收率。通过计算各个不确定度分量并合成，得到4，4’-滴滴伊（4，4’-DDE）、2，4’-滴滴涕（2，4’-DDT）、4，4’-滴滴滴（4，4’-DDD）、4，4’-滴滴涕（4，4’-DDT）的结果可分别报告为（0.14±0.01）、（0.13±0.01）、（0.14±0.01）、（0.13±0.03）mg·kg^-1，（k=2）。测定结果的不确定度主要受标准曲线拟合、标准溶液配制的因素影响。

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