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Research on Pesticide Residue Detection Methods and Limit Standards in Lycium barbarum L.
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Ying WANG1, Yuanxi LIU1, Mingrui SHEN2, Tingting ZHOU1, Xianrui ZHANG1, Yi HE2, Hongyu JIN1, *, Feng WEI1, Shuangcheng MA2, *
Chinese Pharmaceutical Journal | 2024, 59(16) : 1453 - 1459
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Chinese Pharmaceutical Journal | 2024, 59(16): 1453-1459
Research on Pesticide Residue Detection Methods and Limit Standards in Lycium barbarum L.
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Ying WANG1, Yuanxi LIU1, Mingrui SHEN2, Tingting ZHOU1, Xianrui ZHANG1, Yi HE2, Hongyu JIN1, *, Feng WEI1, Shuangcheng MA2, *
Affiliations
  • 1 National Institutes for Food and Drug Control, Beijing 102629, China
  • 2 Chinese Pharmacopoeia Commission, Beijing 100061, China
Published: 2024-08-22 doi: 10.11669/cpj.2024.16.001
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OBJECTIVE To develop the limited standard and supporting detection methods of commonly used pesticides in Lycium barbarum L. (L. barbarum). METHODS In previous research, the “the Principle of Conversion of Limit Standards of Traditional Chinese Medicine in <GB 2763 national food safety standard-maximum residue limits for pesticides in food>” have been drafted. In this research, the L. barbarum was used as the research object to study the conversion scope, risk assessment, detection methods and conversion judgment principle. RESULTS A method for the determination of 13 pesticide residues in the L. barbarum was established by using acetonitrile extraction and HLB column purification. And the GC-MS/MS and LC-MS/MS technology were used to detect the pesticide residues. In addition, the maximum residue limit of 13 pesticides in L. barbarum was finally formulated by sample determination. CONCLUSION The specific implementation steps are provided for the conversion of GB 2763 standard to traditional Chinese medicine standard in this study, and it is of great significance for promoting the connection between planting and circulation supervision of L. barbarum.

Lycium barbarum L.  /  GB 2763  /  limited standard  /  conversion principle  /  pesticide residue
Ying WANG, Yuanxi LIU, Mingrui SHEN, Tingting ZHOU, Xianrui ZHANG, Yi HE, Hongyu JIN, Feng WEI, Shuangcheng MA. Research on Pesticide Residue Detection Methods and Limit Standards in Lycium barbarum L.[J]. Chinese Pharmaceutical Journal, 2024 , 59 (16) : 1453 -1459 . DOI: 10.11669/cpj.2024.16.001
Year 2024 volume 59 Issue 16
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doi: 10.11669/cpj.2024.16.001
  • Receive Date:2024-02-25
  • Online Date:2025-10-29
  • Published:2024-08-22
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  • Received:2024-02-25
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    1 National Institutes for Food and Drug Control, Beijing 102629, China
    2 Chinese Pharmacopoeia Commission, Beijing 100061, China
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表12种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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