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Three butylphthalide derivatives from the Rhizome of Ligusticum chuanxiong
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Xiang YUAN, Bing HAN, Zi-ming FENG, Jian-shuang JIANG, Ya-nan YANG, Pei-cheng ZHANG*
Acta Pharmaceutica Sinica | 2020, 55(11) : 2674 - 2678
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Acta Pharmaceutica Sinica | 2020, 55(11): 2674-2678
• Original Articles •
Three butylphthalide derivatives from the Rhizome of Ligusticum chuanxiong
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Xiang YUAN, Bing HAN, Zi-ming FENG, Jian-shuang JIANG, Ya-nan YANG, Pei-cheng ZHANG*
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  • State Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China
Published: 2020-11-12 doi: 10.16438/j.0513-4870.2020-0887
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Three butylphthalide derivatives were isolated from the Rhizome of Ligusticum chuanxiong using a series of isolation and purification approaches including macroporous resin, ODS-A column, Sephadex LH-20 and preparative HPLC. These structures were elucidated based on extensive spectroscopic data (UV, IR, HR-ESI-MS and NMR) and identified as (3Z, 3aE)-(6R, 7R, 2'S)-6-hydroxy-7-(2-carboxyl-2-hydroxyethylthio)-3-(2-hydroxybutylidene)-4, 5, 6, 7-tetrahydro-phthalide (1), (3Z, 3aZ)-3-butylidene-6, 7-dihydroxy-4, 5, 6, 7-tetrahydro-phthalide 7-O-α-D-glucopyranosyl-(1→2)-β-D-fructo-furanoside (2) and 3-(3-β-D-glucopyranosyloxy-butylidene)-7-hydroxy-phthalide (3).

Ligusticum chuanxiong  /  NMR  /  butylphthalides
Xiang YUAN, Bing HAN, Zi-ming FENG, Jian-shuang JIANG, Ya-nan YANG, Pei-cheng ZHANG. Three butylphthalide derivatives from the Rhizome of Ligusticum chuanxiong[J]. Acta Pharmaceutica Sinica, 2020 , 55 (11) : 2674 -2678 . DOI: 10.16438/j.0513-4870.2020-0887
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Article Info
doi: 10.16438/j.0513-4870.2020-0887
  • Receive Date：2020-06-03
  • Online Date：2026-01-23
  • Published：2020-11-12
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  • Received：2020-06-03
  • Revised：2020-07-03
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    State Key Laboratory of Bioactive Substance and Function of Natural Medicines, Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, China
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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