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Comparative analysis of aconitine alkaloids in aconite tube using direct ionization and wooden tip spray mass spectrometry
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Jia-jie LU1, Jing YAN1, *, Qing-xuan XU2, *
Acta Pharmaceutica Sinica | 2019, 54(7) : 1271 - 1276
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Acta Pharmaceutica Sinica | 2019, 54(7): 1271-1276
• Original Articles •
Comparative analysis of aconitine alkaloids in aconite tube using direct ionization and wooden tip spray mass spectrometry
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Jia-jie LU1, Jing YAN1, *, Qing-xuan XU2, *
Affiliations
  • 1. Heilongjiang University of Traditional Chinese Medicine, Harbin 150040, China
  • 2. Heilongjiang University, Harbin 150081, China
Published: 2019-07-12 doi: 10.16438/j.0513-4870.2019-0131
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In this manuscript, a rapid and simple analysis method for aconitine alkaloids was established. The method was based on the use of direct ionization and wooden tip spray ionization technology to detect the aconite. The aconite tuber slices were wrapped with wet filter paper overnight, cut into triangles, and extracted with a few solvents for direct ionization and wooden tip spray mass spectrometry. The results showed that alkaloids in aconite tuber can be rapid detected by two mass spectrometric methods without tedious sample pretreatment. Both methods are superior to that of traditional capillary electrospray ionization mass spectrometry (ESI-MS). The direct ionization MS is better than the wooden tip spray MS for analysis of aconite except under the condition of methylene chloride as extract or spray solvent. Different types of alkaloids in aconite tuber can be selectively detected when different solvents are used. The experiments provide a rapid and no pretreatment MS spectrometric method for analysis of alkaloids in aconite. These sample methods are important for research on aspects of plant varieties, storage, prescription compatibility, and quality control of aconite.

ESI-MS  /  wooden tip spray  /  direct ionization  /  aconite tube  /  aconitine alkaloids
Jia-jie LU, Jing YAN, Qing-xuan XU. Comparative analysis of aconitine alkaloids in aconite tube using direct ionization and wooden tip spray mass spectrometry[J]. Acta Pharmaceutica Sinica, 2019 , 54 (7) : 1271 -1276 . DOI: 10.16438/j.0513-4870.2019-0131
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Article Info
doi: 10.16438/j.0513-4870.2019-0131
  • Receive Date：2019-02-24
  • Online Date：2026-01-26
  • Published：2019-07-12
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  • Received：2019-02-24
  • Revised：2019-04-23
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Affiliations
    1. Heilongjiang University of Traditional Chinese Medicine, Harbin 150040, China
    2. Heilongjiang University, Harbin 150081, China
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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