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Simultaneous determination of four kinds of haloacetic acids and chlorite in drinking water by ion chromatography with large volume injection
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Yan YOU*, Xian-Lin DING, Wei-Xin LI
Laboratory Testing | 2024, 2(2) : 18 - 22
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Laboratory Testing | 2024, 2(2): 18-22
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Simultaneous determination of four kinds of haloacetic acids and chlorite in drinking water by ion chromatography with large volume injection
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Yan YOU*, Xian-Lin DING, Wei-Xin LI
Affiliations
  • Luqiao District Center for Disease Control and Prevention Taizhou 318050 China
Published: 2024-02-08
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Objective A method for simultaneous determination of MBAA, DBAA, DCAA, TCAA and ${\mathrm{{ClO}}}_{2}{}^{- }$ in drinking water was established by ion chromatography. Methods The water samples were determined by ${0.22\mu}\mathrm{m}$ qeuosystem filter membrane with a volume of ${500\mu }\mathrm{L}$ . The samples were rinsed with $\mathrm{{KOH}}$ solution gradient and separated by IonPac AS19 anion column. The column temperature was set at ${30}^{\circ }\mathrm{C}$ , and the current of the inhibitor was ${75}\mathrm{\;{mA}}$ . Results The results showed that the linearity ranges of ${\mathrm{{ClO}}}_{2}{}^{- }$ , MBAA, DBAA, DCAA and TCAA were found in the range of ${10}\sim {1000\mu}\mathrm{g}/\mathrm{L},\mathrm{r}> {0.9990}$ , with detection limits $\left({3\mathrm{\;S}/\mathrm{N}}\right)$ of ${0.32},{0.76},{1.30},{0.69},{1.58\mu}\mathrm{g}/\mathrm{L}$ . The standard recoveries were ${80}\%\sim {110}\%$ and RSD (n=6) of the determined values were all less than 5.0%. Conclusion The method was simple, sensitive, can meet the detection requirements of four kinds of Haloaeetic Acids and Chlorite in drinking water. The method can be used for the determination of kour kinds of haloaeetic acids and chlorite in drinking water.

ion chromatography  /  four kinds of haloaeetic acids  /  chlorite  /  drinking water
Yan YOU, Xian-Lin DING, Wei-Xin LI. Simultaneous determination of four kinds of haloacetic acids and chlorite in drinking water by ion chromatography with large volume injection[J]. Laboratory Testing, 2024 , 2 (2) : 18 -22 .
Year 2024 volume 2 Issue 2
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  • Online Date:2025-07-29
  • Published:2024-02-08
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Affiliations
    Luqiao District Center for Disease Control and Prevention Taizhou 318050 China

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*YOU Yan, Master, Chief Technician, Luqiao District Center for Disease Control and Prevention, Taizhou, 318050, China. E-mail:
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表12种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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