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Identification of Testudinis Carapax et Plastrum and Trionycis Carapax Form Ge jie Ding chuan Pill base on UPLC-MS/MS
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Hong-jun YIN, Yue WU, Xiao-Yi HUA, Qing DING, Jin ZHANG*
Laboratory Testing | 2024, 2(2) : 10 - 13
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Laboratory Testing | 2024, 2(2): 10-13
• Innovative Applications •
Identification of Testudinis Carapax et Plastrum and Trionycis Carapax Form Ge jie Ding chuan Pill base on UPLC-MS/MS
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Hong-jun YIN, Yue WU, Xiao-Yi HUA, Qing DING, Jin ZHANG*
Affiliations
  • Wuxi Instituteof Drug Safety Control Wuxi 21400 China
Published: 2024-02-08
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Objective To develop an ultra high performance liquid chromatography tandem mass spectrometry (UPLC-MS/MS) to identification of the feeding status of turtle and turtle shell components in different batches of Gejie Dingchuan Pills. Methods This study used the identification method of characteristic peptides of Animal medicine for reference, Enzymatic hydrolysis of different batches of Ge jie Ding chuan Pill samples using trypsin, and Identification by using the ultra high performance liquid chromatography tandem mass spectrometry (UPLC-MS/MS). The characteristic ion pairs of Testudinis Carapax et Plastrum and Trionycis Carapax were as detection ion pairs. The positive electrospray ionization and multiple reaction monitoring were adopted. Result: 51 batches of Gejie Ding chuan Pills form 8 companies have all detected turtle shell components, but no other turtle source components have been detected. Conclusion This method is raliable for identification of Testudinis Carapax et Plastrum and Trionycis Carapax form Ge jie Ding chuan Pill.

Gejie Ding chuan Pill  /  Testudinis Carapax et Plastrum  /  Trionycis Carapax  /  characteristic ion  /  UPLC-MS/MS
Hong-jun YIN, Yue WU, Xiao-Yi HUA, Qing DING, Jin ZHANG. Identification of Testudinis Carapax et Plastrum and Trionycis Carapax Form Ge jie Ding chuan Pill base on UPLC-MS/MS[J]. Laboratory Testing, 2024 , 2 (2) : 10 -13 .
Funding
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  • Science and Technology Plan Project of Jiangsu Provincial Administration for Market Regulation "Research on the Quality Control of Animal Drugs and Mineral Drugs"(KJ2023044项目)
  • the second batch of key projects of the China Drug Supervision Scientific Action Plan "Effectiveness and Safety Evaluation of Traditional Chinese Medicine and the Whole Process "Quality Control Research", Project Name: Research on Quality Control and Evaluation of Turtle Medicinal Materials and Decoction Pieces(NMPAJGKX-2023-045)
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Article Info
  • Online Date：2025-07-29
  • Published：2024-02-08
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Funding
Science and Technology Plan Project of Jiangsu Provincial Administration for Market Regulation "Research on the Quality Control of Animal Drugs and Mineral Drugs"(KJ2023044项目)
the second batch of key projects of the China Drug Supervision Scientific Action Plan "Effectiveness and Safety Evaluation of Traditional Chinese Medicine and the Whole Process "Quality Control Research", Project Name: Research on Quality Control and Evaluation of Turtle Medicinal Materials and Decoction Pieces(NMPAJGKX-2023-045)
Affiliations
    Wuxi Instituteof Drug Safety Control Wuxi 21400 China

Corresponding:

*ZHANG Jin, Master, Deputy Chief Chinese Pharmacist, Wuxi Instituteof Drug Safety Control, Wuxi 21400, China. E-mail:
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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