Article(id=1320880633191191201, tenantId=1146029695717560320, journalId=1260987677001138203, issueId=1320880262012056083, articleNumber=null, orderNo=null, doi=10.13386/j.issn1002-0306.2025040353, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1745942400000, receivedDateStr=2025-04-30, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1792852083728, onlineDateStr=2026-10-24, pubDate=1789401600000, pubDateStr=2026-09-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792852083728, onlineIssueDateStr=2026-10-24, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792852083728, creator=13701087609, updateTime=1792852083728, updator=13701087609, issue=Issue{id=1320880262012056083, tenantId=1146029695717560320, journalId=1260987677001138203, year='2026', volume='47', issue='18', pageStart='1', pageEnd='613', issueExtLink='null', onlineDate='null', pubDate='1789401600000', pubDateStr='2026-09-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1792851995232, creator='13701087609', updateTime=1792921655980, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1321172440479290195, tenantId=1146029695717560320, journalId=1260987677001138203, issueId=1320880262012056083, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1321172440479290196, tenantId=1146029695717560320, journalId=1260987677001138203, issueId=1320880262012056083, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=263, endPage=273, ext={EN=ArticleExt(id=1320880633811948194, articleId=1320880633191191201, tenantId=1146029695717560320, journalId=1260987677001138203, language=EN, title=Determination of 30 Pesticide Residues in 5 Kinds of Ginseng Health Food Ingredients by Ultra-high Performance Liquid Chromatography-Tandem Mass Spectrometry (UPLC-MS/MS) Based on Modified QuEChERS-Novel Porous Organic Polymers, columnId=1320880262846722580, journalTitle=Science and Technology of Food Industry, columnName=Modern Analysis and Intelligent Detection, runingTitle=null, highlight=null, articleAbstract=
In order to study the pesticide residues in ginseng health food ingredients, an analysis method for determination of 30 pesticide residues in Korean Red Ginseng, Salvia miltiorrhiza Bge, Scrophularia radix, Radix Codonopsis, and Pseudostellaria radix was established by combining the modified QuEChERS-novel porous organic polymers (POPs) purification with ultra-high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). The samples were soaked in 1% ice acetic acid and extracted by acetonitrile, then purified by QuEChERS method without graphitized of carbon black. The purificated solutions were adsorbed and desorbed by novel porous organic polymers, concentrated by nitrogen stream and dissolved in 1 mL acetonitrile solution (volume ratio 6+4). The filtrates were separated by the Phenomenx Kinetex C18 (100 mm×2.1 mm) chromatography column, using gradient elution of 0.1% formic acid aqueous solution containing 5 mmol/L ammonium formate-acetonitrile, determined by electrospray ionization, in positive ion switching dynamic multiple reaction monitoring mode, and quantified by the internal standard method. The results showed that the adsorption rate of 10 mg POPs materials self-made by the chemical method for 30 kinds of pesticides could reach more than 95%, and the desorption capacity reached 99% when eluted with acetonitrile-toluene (volume ratio 3+1) solution. The recoveries of 30 kinds of pesticides were increased to 5%~40% by modified QuEChERS-novel porous organic polymers purification. Method validation revealed that all 30 pesticides had good linearities in the range of 0.05~100 µg/kg, with correlation coefficients (r) higher than 0.990, and limits of detection (LOD, S/N=3) were 0.05~5.0 µg/kg. The average recoveries of 5 kinds of ginseng health food ingredients were ranged from 86.4% to 113.1%, with relative standard deviations (RSD, n=6) of 0.36%~8.74% at low, medium and high addition levels. While the limits of quantification (LOQ, S/N=10) were 0.10~15.0 µg/kg. This method has high recovery and high sensitivity, also can solve the issues of low pesticide recovery and strong matrix interference in ginseng health food ingredients by conventional QuEChERS pretreatment.
, authors=Suoyin YU
1, *, Jia LIANG
2, *, Yueyang YU
3, authorsList=Suoyin YU, Jia LIANG, Yueyang YU, authorCompany=null, correspAuthors=Suoyin YU, Jia LIANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=Copyright © 2026 Science and Technology of Food Industry. All rights reserved., copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1320880635959431845, articleId=1320880633191191201, tenantId=1146029695717560320, journalId=1260987677001138203, language=CN, title=基于改良QuEChERS-新型超交联聚合物净化的超高效液相-串联四级杆质谱联用法测定5种参类保健食品原料中30种农药残留, columnId=1320880262997717526, journalTitle=食品工业科技, columnName=现代分析与智能检测, runingTitle=null, highlight=null, articleAbstract=
为研究参类保健食品原料中农药残留污染现状，建立了改良QuEChERS-新型超交联聚合物（porous organic polymers，POPs）联用净化，超高效液相-串联四级杆质谱测定高丽红参、丹参、玄参、党参和太子参中30种农药残留量分析方法。样品经1%冰乙酸浸润、乙腈提取，QuEChERS（不含石墨化碳黑）净化液经新型超交联聚合物吸附、解吸处理、解吸液浓缩后用1 mL乙腈+水（体积比6+4）定容。滤液经Phenomenx Kinetex C18色谱柱（100 mm×2.1 mm）分离，0.1%甲酸（含5 mmol/L甲酸铵）-乙腈梯度洗脱，电喷雾离子化、正离子扫描和动态多反应监测模式测定，内标法定量。结果表明：化学法自制的10 mg POPs材料对30种农药吸附率可达95%以上，用乙腈+甲苯（体积比3+1）洗脱解吸率达99%、改良QuEChERS-新型超交联聚合物联用净化法使30种农药回收率均提升了5%~40%。30种农药在0.05~100 µg/kg范围内均有较好的线性关系（r>0.990），检出限（limits of detection，LOD，S/N=3）为0.05~5.0 µg/kg。5种参类保健食品原料在低、中、高三水平下的平均回收率为86.4%~113.1%，相对标准偏差（relative standard deviations，RSD，n=6）为0.36%~8.74%，方法定量限（limits of quantification detection，LOQ，S/N=10）为0.10~15.0 µg/kg。本方法回收率高、灵敏度高，能够解决传统QuEChERS前处理对参类保健食品原料中农药回收率低、基质干扰强的问题。
, authors=俞所银
1, *, 梁佳
2, *, 俞跃洋
3, authorsList=俞所银, 梁佳, 俞跃洋, authorCompany=null, correspAuthors=俞所银, 梁佳, authorNote=
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1, *, address=
1Shanghai Institute of Quality Inspection and Technical Research Co., Ltd., Shanghai 200233, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1320880636647297715, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, authorId=1320880636466942640, language=CN, stringName=俞所银, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
1, *, address=
1上海市质量监督检验技术研究院有限公司，上海 200233, bio={"content":"
俞所银（1986−），男，硕士，工程师，研究方向：食品药品化妆品质量检测与分析，E-mail：yusuoyin@163.com
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俞所银（1986−），男，硕士，工程师，研究方向：食品药品化妆品质量检测与分析，E-mail：yusuoyin@163.com
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2College of Food Sciences and Pharmaceutics, Zhejiang Ocean University, Zhoushan 316022, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1320880636890567352, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, authorId=1320880636722795189, language=CN, stringName=梁佳, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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2浙江海洋大学食品与药学学院，浙江舟山 316022, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1320880636290781865, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, xref=2, ext=[AuthorCompanyExt(id=1320880636299170474, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, companyId=1320880636290781865, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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3Jiangsu Vocational College of Agriculture and Forestry, Jurong 212400, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1320880637121254077, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, authorId=1320880636966064826, language=CN, stringName=俞跃洋, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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3江苏农林职业技术学院，江苏句容 212400, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1320880636374667948, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, xref=3, ext=[AuthorCompanyExt(id=1320880636383056557, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, companyId=1320880636374667948, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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3江苏农林职业技术学院，江苏句容 212400)])])], keywords=[Keyword(id=1320880637230305982, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, orderNo=1, keyword=modified QuEChERS-novel porous organic polymers purification), Keyword(id=1320880637314192063, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, orderNo=2, keyword=ginseng health food ingredients), Keyword(id=1320880637410661056, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, orderNo=3, keyword=ultra-high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS)), Keyword(id=1320880637477769921, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, orderNo=4, keyword=pesticide residues), Keyword(id=1320880637553267394, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, orderNo=1, keyword=改良QuEChERS-新型超交联聚合物), Keyword(id=1320880637624570563, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, orderNo=2, keyword=参类保健食品原料), Keyword(id=1320880637712650948, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, orderNo=3, keyword=超高效液相-串联四级杆质谱联（UPLC-MS/MS）), Keyword(id=1320880637788148421, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, orderNo=4, keyword=农药残留)], refs=[Reference(id=1320880640417977044, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, doi=null, pmid=null, pmcid=null, year=null, volume=null, issue=null, pageStart=null, pageEnd=null, url=null, language=null, rfNumber=1, rfOrder=0, authorNames=null, journalName=null, refType=null, unstructuredReference=李燕兰, 方泓, 成颜琦, 等. 高丽红参干预虚证疲劳双盲、随机、安慰剂对照的临床研究[J]. 现代医学与健康研究, 2022, 6(20): 31−37. [LI Y L, FANG H, CHENG Y Q, et al. Double-blind, randomized, placebo-controlled clinical study of Korean red ginseng intervention on fatiguewith deficiency syndrome[J]. Modern Medicine and Health Research, 2022, 6(20): 31−37.], articleTitle=null, refAbstract=null), Reference(id=1320880640527028949, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, doi=null, pmid=null, pmcid=null, year=null, volume=null, issue=null, pageStart=null, pageEnd=null, url=null, language=null, rfNumber=1, rfOrder=1, authorNames=null, journalName=null, refType=null, unstructuredReference=LI Y L, FANG H, CHENG Y Q, et al. Double-blind, randomized, placebo-controlled clinical study of Korean red ginseng intervention on fatiguewith deficiency syndrome[J]. Modern Medicine and Health Research, 2022, 6（20）: 31−37., articleTitle=null, refAbstract=null), Reference(id=1320880640598332118, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, doi=null, pmid=null, pmcid=null, year=null, volume=null, issue=null, pageStart=null, pageEnd=null, url=null, language=null, rfNumber=2, rfOrder=2, authorNames=null, journalName=null, refType=null, unstructuredReference=刘沁荣, 杜紫薇, 李佳珍, 等. 不同产地丹参及根际土壤无机元素分析与评价[J]. 光谱学与光谱分析, 2021, 41(11): 3618−3624. [LIU Q R, DU Z W, LI J Z, et al. Analysis and evaluation of inorganic elements in
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Effect of POPs material usage on the adsorption of 30 kinds of pesticide resticides in Korean Red Ginseng, figureFileSmall=RVMrXigRmY6e4VUbu+e43Q==, figureFileBig=dlc4KkkKhhgnsiVnWkgyNQ==, tableContent=null), ArticleFig(id=1320880638014640839, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, label=图1, caption=
POPs材料用量对高丽红参30种农药吸附量影响, figureFileSmall=RVMrXigRmY6e4VUbu+e43Q==, figureFileBig=dlc4KkkKhhgnsiVnWkgyNQ==, tableContent=null), ArticleFig(id=1320880638215967432, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, label=Table 1, caption=
ESI+-MS/MS conditions for mass spectrometry parameters of 30 pesticide residues
, figureFileSmall=null, figureFileBig=null, tableContent=
| 序号 | 农药 | 保留时间（min） | 母离子（m/z） | 子离子（m/z） | 去簇电压（V） | 碰撞能量（eV） |
|---|
| 1 | 甲基硫环磷 | 2.18 | 228.0 | 168.1*，108.9 | 100 | 19，35 |
| 2 | 内吸磷 | 4.95 | 259.1 | 89.0*，60.9 | 43 | 30，33 |
| 3 | 蝇毒磷 | 7.84 | 363.0 | 227.0*，307.0 | 100 | 36，25 |
| 4 | 灭线磷 | 6.24 | 243.0 | 131.0*，97.0 | 51 | 29，41 |
| 5 | 苯线磷 | 6.11 | 304.2 | 217.1*，202.0 | 77 | 31，45 |
| 6 | 苯线磷砜 | 3.67 | 336.0 | 266.1*，188.3 | 60,85 | 28，38 |
| 7 | 苯线磷亚砜 | 2.71 | 320.1 | 233.0*，292.1 | 60 | 34，21 |
| 8 | 水胺硫磷 | 5.41 | 312.0 | 270.2*，236.2 | 67 | 23，22 |
| 9 | 甲拌磷 | 7.98 | 261.1 | 75.0*，47.0 | 51，47 | 21，46 |
| 10 | 甲拌磷砜 | 5.36 | 293.0 | 247.1*，115.1 | 60 | 12，33 |
| 11 | 甲拌磷亚砜 | 4.24 | 277.0 | 97.1*，171.1 | 60 | 44，16 |
| 12 | 胺苯磺隆 | 4.21 | 411.1 | 196.1*，168.1 | 49 | 23，35 |
| 13 | 硫线磷 | 7.66 | 271.0 | 159.0*，97.0 | 65 | 19，51 |
| 14 | 克百威 | 3.78 | 222.1 | 165.0*，123.1 | 70 | 17，29 |
| 15 | 3-羟基克百威 | 1.61 | 238.0 | 181.0*，163.0 | 65 | 14，20 |
| 16 | 地虫硫磷 | 7.83 | 247.0 | 137.1*，109.1 | 60，50 | 15，25 |
| 17 | 氯唑磷 | 7.08 | 314.0 | 162.0*，120.0 | 70 | 22，40 |
| 18 | 氯磺隆 | 4.02 | 358.0 | 141.0*，167.0 | 51 | 23，25 |
| 19 | 硫环磷 | 2.19 | 256.2 | 140.0*，168.0 | 80，65 | 32，22 |
| 20 | 甲磺隆 | 3.64 | 382.0 | 167.0*，199.0 | 36 | 21，27 |
| 21 | 涕灭威 | 2.78 | 208.1 | 116.2*，89.2 | 22 | 12，25 |
| 22 | 涕灭威砜 | 1.21 | 223.0 | 148.0*，86.0 | 63 | 12，20 |
| 23 | 涕灭威亚砜 | 1.04 | 207.0 | 132.0*，89.0 | 51 | 10，20 |
| 24 | 磷胺 | 2.75 | 300.0 | 174.0*，126.9 | 70 | 20，28 |
| 25 | 甲基异柳磷 | 7.74 | 332.0 | 231.0*，273.0 | 40 | 20，9 |
| 26 | 甲胺磷 | 1.00 | 142.0 | 94.0*，79.0 | 46 | 19，28 |
| 27 | 特丁硫磷砜 | 6.28 | 321.0 | 171.0*，265.0 | 50，85 | 18，12 |
| 28 | 特丁硫磷亚砜 | 5.39 | 305.0，187.0 | 187.0*，159.0 | 52，75 | 17，13 |
| 29 | 久效磷 | 1.16 | 224.1 | 127.0*，98.0 | 71 | 21，17 |
| 30 | 杀虫脒 | 1.30 | 197.1 | 117.1*，89.0 | 75 | 39，61 |
| 31 | 氘代莠去津a | 4.25 | 221.0 | 178.8*，101.1 | 35 | 13 |
), ArticleFig(id=1320880638283076297, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, label=表1, caption=
30种农残测定的ESI+-MS/MS质谱参数表
, figureFileSmall=null, figureFileBig=null, tableContent=
| 序号 | 农药 | 保留时间（min） | 母离子（m/z） | 子离子（m/z） | 去簇电压（V） | 碰撞能量（eV） |
|---|
| 1 | 甲基硫环磷 | 2.18 | 228.0 | 168.1*，108.9 | 100 | 19，35 |
| 2 | 内吸磷 | 4.95 | 259.1 | 89.0*，60.9 | 43 | 30，33 |
| 3 | 蝇毒磷 | 7.84 | 363.0 | 227.0*，307.0 | 100 | 36，25 |
| 4 | 灭线磷 | 6.24 | 243.0 | 131.0*，97.0 | 51 | 29，41 |
| 5 | 苯线磷 | 6.11 | 304.2 | 217.1*，202.0 | 77 | 31，45 |
| 6 | 苯线磷砜 | 3.67 | 336.0 | 266.1*，188.3 | 60,85 | 28，38 |
| 7 | 苯线磷亚砜 | 2.71 | 320.1 | 233.0*，292.1 | 60 | 34，21 |
| 8 | 水胺硫磷 | 5.41 | 312.0 | 270.2*，236.2 | 67 | 23，22 |
| 9 | 甲拌磷 | 7.98 | 261.1 | 75.0*，47.0 | 51，47 | 21，46 |
| 10 | 甲拌磷砜 | 5.36 | 293.0 | 247.1*，115.1 | 60 | 12，33 |
| 11 | 甲拌磷亚砜 | 4.24 | 277.0 | 97.1*，171.1 | 60 | 44，16 |
| 12 | 胺苯磺隆 | 4.21 | 411.1 | 196.1*，168.1 | 49 | 23，35 |
| 13 | 硫线磷 | 7.66 | 271.0 | 159.0*，97.0 | 65 | 19，51 |
| 14 | 克百威 | 3.78 | 222.1 | 165.0*，123.1 | 70 | 17，29 |
| 15 | 3-羟基克百威 | 1.61 | 238.0 | 181.0*，163.0 | 65 | 14，20 |
| 16 | 地虫硫磷 | 7.83 | 247.0 | 137.1*，109.1 | 60，50 | 15，25 |
| 17 | 氯唑磷 | 7.08 | 314.0 | 162.0*，120.0 | 70 | 22，40 |
| 18 | 氯磺隆 | 4.02 | 358.0 | 141.0*，167.0 | 51 | 23，25 |
| 19 | 硫环磷 | 2.19 | 256.2 | 140.0*，168.0 | 80，65 | 32，22 |
| 20 | 甲磺隆 | 3.64 | 382.0 | 167.0*，199.0 | 36 | 21，27 |
| 21 | 涕灭威 | 2.78 | 208.1 | 116.2*，89.2 | 22 | 12，25 |
| 22 | 涕灭威砜 | 1.21 | 223.0 | 148.0*，86.0 | 63 | 12，20 |
| 23 | 涕灭威亚砜 | 1.04 | 207.0 | 132.0*，89.0 | 51 | 10，20 |
| 24 | 磷胺 | 2.75 | 300.0 | 174.0*，126.9 | 70 | 20，28 |
| 25 | 甲基异柳磷 | 7.74 | 332.0 | 231.0*，273.0 | 40 | 20，9 |
| 26 | 甲胺磷 | 1.00 | 142.0 | 94.0*，79.0 | 46 | 19，28 |
| 27 | 特丁硫磷砜 | 6.28 | 321.0 | 171.0*，265.0 | 50，85 | 18，12 |
| 28 | 特丁硫磷亚砜 | 5.39 | 305.0，187.0 | 187.0*，159.0 | 52，75 | 17，13 |
| 29 | 久效磷 | 1.16 | 224.1 | 127.0*，98.0 | 71 | 21，17 |
| 30 | 杀虫脒 | 1.30 | 197.1 | 117.1*，89.0 | 75 | 39，61 |
| 31 | 氘代莠去津a | 4.25 | 221.0 | 178.8*，101.1 | 35 | 13 |
), ArticleFig(id=1320880638379545290, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, label=Table 2, caption=
Desorption rates of 30 pesticide residues in Korean red ginseng using different types of desorption solvents (n=6)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 解吸溶剂 | 解吸率（%） |
|---|
| 均值 | 标准差 |
|---|
| 乙腈 | 85.12 | 6.31 |
| 含1%磷酸的乙腈 | 30.06 | 20.04 |
| 乙腈+甲苯（3+1） | 99.02 | 4.55 |
| 甲醇 | 79.25 | 9.20 |
| 含1%氨水的甲醇 | 23.10 | 19.27 |
), ArticleFig(id=1320880638442459851, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, label=表2, caption=
不同解吸溶剂对高丽红参中30种农药的解吸率（n=6）
, figureFileSmall=null, figureFileBig=null, tableContent=
| 解吸溶剂 | 解吸率（%） |
|---|
| 均值 | 标准差 |
|---|
| 乙腈 | 85.12 | 6.31 |
| 含1%磷酸的乙腈 | 30.06 | 20.04 |
| 乙腈+甲苯（3+1） | 99.02 | 4.55 |
| 甲醇 | 79.25 | 9.20 |
| 含1%氨水的甲醇 | 23.10 | 19.27 |
), ArticleFig(id=1320880638501180108, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, label=Table 3, caption=
Recoveries rate of 30 kinds of pesticide residues in Korean Red Ginseng with different sorbents
, figureFileSmall=null, figureFileBig=null, tableContent=
| 农药 | QuEChERS | | 改良QuEChERS（不含GCB） | | POPs材料 | | QuEChERS（不含GCB）+POPs |
|---|
| 平均回收率（%） | RSD（%） | | 平均回收率（%） | RSD（%） | | 平均回收率（%） | RSD（%） | | 平均回收率（%） | RSD（%） |
|---|
| 甲基硫环磷 | 81.7 | 2.36 | | 85.8 | 1.45 | | 67.2 | 1.66 | | 98.0 | 1.62 |
| 内吸磷 | 84.8 | 4.19 | | 92.6 | 2.88 | | 60.2 | 4.82 | | 94.1 | 4.56 |
| 蝇毒磷 | 88.6 | 1.76 | | 93.8 | 3.49 | | 67.6 | 1.89 | | 98.3 | 2.84 |
| 灭线磷 | 89.5 | 2.15 | | 93.8 | 5.08 | | 58.7 | 2.29 | | 97.3 | 2.78 |
| 苯线磷 | 91.5 | 0.744 | | 100.8 | 3.12 | | 72.6 | 2.66 | | 100.7 | 2.61 |
| 苯线磷砜 | 80.1 | 1.63 | | 84.1 | 4.10 | | 65.8 | 7.52 | | 96.9 | 1.48 |
| 苯线磷亚砜 | 87.9 | 3.10 | | 88.2 | 8.07 | | 58.2 | 4.67 | | 96.5 | 6.44 |
| 水胺硫磷 | 77.6 | 6.28 | | 78.6 | 3.64 | | 50.6 | 5.07 | | 92.2 | 3.06 |
| 甲拌磷 | 81.6 | 2.55 | | 86.9 | 3.57 | | 56.6 | 3.41 | | 98.5 | 1.56 |
| 甲拌磷砜 | 81.5 | 0.580 | | 81.8 | 2.94 | | 43.0 | 5.84 | | 96.5 | 2.51 |
| 甲拌磷亚砜 | 69.6 | 5.25 | | 74.2 | 5.72 | | 36.4 | 15.0 | | 92.1 | 1.45 |
| 胺苯磺隆 | 82.8 | 2.99 | | 85.3 | 1.90 | | 41.0 | 15.1 | | 93.1 | 4.24 |
| 硫线磷 | 75.4 | 2.81 | | 80.1 | 1.27 | | 65.8 | 7.91 | | 91.6 | 2.46 |
| 克百威 | 88.6 | 2.99 | | 92.1 | 3.26 | | 69.6 | 7.78 | | 96.1 | 3.25 |
| 3-羟基克百威 | 95.3 | 3.15 | | 100.7 | 5.64 | | 84.4 | 4.69 | | 107.5 | 5.22 |
| 地虫硫磷 | 90.6 | 3.09 | | 97.1 | 2.55 | | 74.8 | 5.05 | | 101.9 | 3.25 |
| 氯唑磷 | 93.2 | 2.54 | | 91.7 | 2.38 | | 64.6 | 9.21 | | 102.2 | 5.73 |
| 氯磺隆 | 64.5 | 7.16 | | 97.1 | 4.64 | | 59.5 | 6.10 | | 98.3 | 1.02 |
| 硫环磷 | 81.1 | 4.24 | | 85.0 | 4.59 | | 64.4 | 9.68 | | 105.3 | 9.60 |
| 甲磺隆 | 91.5 | 2.75 | | 90.2 | 1.71 | | 71.8 | 4.89 | | 94.5 | 4.68 |
| 涕灭威 | 92.3 | 2.36 | | 93.2 | 1.78 | | 82.2 | 3.57 | | 94.8 | 2.13 |
| 涕灭威砜 | 84.3 | 6.78 | | 99.6 | 5.72 | | 70.6 | 3.64 | | 91.7 | 1.36 |
| 涕灭威亚砜 | 91.3 | 1.49 | | 99.6 | 2.31 | | 80.0 | 1.39 | | 94.3 | 3.87 |
| 磷胺 | 85.3 | 3.58 | | 87.3 | 2.01 | | 75.3 | 5.52 | | 96.3 | 2.65 |
| 甲基异柳磷 | 86.4 | 4.43 | | 91.0 | 2.89 | | 66.7 | 6.77 | | 97.4 | 1.93 |
| 甲胺磷 | 74.7 | 4.90 | | 83.8 | 2.42 | | 45.3 | 7.97 | | 97.6 | 4.38 |
| 特丁硫磷砜 | 80.6 | 1.51 | | 84.4 | 3.48 | | 56.5 | 8.47 | | 93.8 | 2.23 |
| 特丁硫磷亚砜 | 80.1 | 1.19 | | 80.9 | 3.32 | | 62.5 | 9.70 | | 93.6 | 1.27 |
| 久效磷 | 81.0 | 1.64 | | 85.0 | 2.83 | | 72.8 | 4.21 | | 95.4 | 3.62 |
| 杀虫脒 | 84.3 | 2.47 | | 84.7 | 1.37 | | 55.6 | 4.67 | | 94.5 | 2.08 |
), ArticleFig(id=1320880638585066189, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, label=表3, caption=
不同净化材料对高丽红参净化后30种农药的回收率
, figureFileSmall=null, figureFileBig=null, tableContent=
| 农药 | QuEChERS | | 改良QuEChERS（不含GCB） | | POPs材料 | | QuEChERS（不含GCB）+POPs |
|---|
| 平均回收率（%） | RSD（%） | | 平均回收率（%） | RSD（%） | | 平均回收率（%） | RSD（%） | | 平均回收率（%） | RSD（%） |
|---|
| 甲基硫环磷 | 81.7 | 2.36 | | 85.8 | 1.45 | | 67.2 | 1.66 | | 98.0 | 1.62 |
| 内吸磷 | 84.8 | 4.19 | | 92.6 | 2.88 | | 60.2 | 4.82 | | 94.1 | 4.56 |
| 蝇毒磷 | 88.6 | 1.76 | | 93.8 | 3.49 | | 67.6 | 1.89 | | 98.3 | 2.84 |
| 灭线磷 | 89.5 | 2.15 | | 93.8 | 5.08 | | 58.7 | 2.29 | | 97.3 | 2.78 |
| 苯线磷 | 91.5 | 0.744 | | 100.8 | 3.12 | | 72.6 | 2.66 | | 100.7 | 2.61 |
| 苯线磷砜 | 80.1 | 1.63 | | 84.1 | 4.10 | | 65.8 | 7.52 | | 96.9 | 1.48 |
| 苯线磷亚砜 | 87.9 | 3.10 | | 88.2 | 8.07 | | 58.2 | 4.67 | | 96.5 | 6.44 |
| 水胺硫磷 | 77.6 | 6.28 | | 78.6 | 3.64 | | 50.6 | 5.07 | | 92.2 | 3.06 |
| 甲拌磷 | 81.6 | 2.55 | | 86.9 | 3.57 | | 56.6 | 3.41 | | 98.5 | 1.56 |
| 甲拌磷砜 | 81.5 | 0.580 | | 81.8 | 2.94 | | 43.0 | 5.84 | | 96.5 | 2.51 |
| 甲拌磷亚砜 | 69.6 | 5.25 | | 74.2 | 5.72 | | 36.4 | 15.0 | | 92.1 | 1.45 |
| 胺苯磺隆 | 82.8 | 2.99 | | 85.3 | 1.90 | | 41.0 | 15.1 | | 93.1 | 4.24 |
| 硫线磷 | 75.4 | 2.81 | | 80.1 | 1.27 | | 65.8 | 7.91 | | 91.6 | 2.46 |
| 克百威 | 88.6 | 2.99 | | 92.1 | 3.26 | | 69.6 | 7.78 | | 96.1 | 3.25 |
| 3-羟基克百威 | 95.3 | 3.15 | | 100.7 | 5.64 | | 84.4 | 4.69 | | 107.5 | 5.22 |
| 地虫硫磷 | 90.6 | 3.09 | | 97.1 | 2.55 | | 74.8 | 5.05 | | 101.9 | 3.25 |
| 氯唑磷 | 93.2 | 2.54 | | 91.7 | 2.38 | | 64.6 | 9.21 | | 102.2 | 5.73 |
| 氯磺隆 | 64.5 | 7.16 | | 97.1 | 4.64 | | 59.5 | 6.10 | | 98.3 | 1.02 |
| 硫环磷 | 81.1 | 4.24 | | 85.0 | 4.59 | | 64.4 | 9.68 | | 105.3 | 9.60 |
| 甲磺隆 | 91.5 | 2.75 | | 90.2 | 1.71 | | 71.8 | 4.89 | | 94.5 | 4.68 |
| 涕灭威 | 92.3 | 2.36 | | 93.2 | 1.78 | | 82.2 | 3.57 | | 94.8 | 2.13 |
| 涕灭威砜 | 84.3 | 6.78 | | 99.6 | 5.72 | | 70.6 | 3.64 | | 91.7 | 1.36 |
| 涕灭威亚砜 | 91.3 | 1.49 | | 99.6 | 2.31 | | 80.0 | 1.39 | | 94.3 | 3.87 |
| 磷胺 | 85.3 | 3.58 | | 87.3 | 2.01 | | 75.3 | 5.52 | | 96.3 | 2.65 |
| 甲基异柳磷 | 86.4 | 4.43 | | 91.0 | 2.89 | | 66.7 | 6.77 | | 97.4 | 1.93 |
| 甲胺磷 | 74.7 | 4.90 | | 83.8 | 2.42 | | 45.3 | 7.97 | | 97.6 | 4.38 |
| 特丁硫磷砜 | 80.6 | 1.51 | | 84.4 | 3.48 | | 56.5 | 8.47 | | 93.8 | 2.23 |
| 特丁硫磷亚砜 | 80.1 | 1.19 | | 80.9 | 3.32 | | 62.5 | 9.70 | | 93.6 | 1.27 |
| 久效磷 | 81.0 | 1.64 | | 85.0 | 2.83 | | 72.8 | 4.21 | | 95.4 | 3.62 |
| 杀虫脒 | 84.3 | 2.47 | | 84.7 | 1.37 | | 55.6 | 4.67 | | 94.5 | 2.08 |
), ArticleFig(id=1320880638677340878, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, label=Table 4, caption=
Linear ranges, regression equations, correlation coefficients, LOD, LOQ and residue limiys (MRL) of 30 pesticides
, figureFileSmall=null, figureFileBig=null, tableContent=
| 序号 | 农药 | 线性范围
（µg/L） | 回归方程 | 决定系数
（r2） | 检出限LOD
（µg/kg） | 定量限LOQ
（µg/kg） | 最大残留量MRL
（µg/kg） |
|---|
| 1 | 甲基硫环磷 | 0.05~100 | y=3.67E-01x+6.99E-03 | 0.9990 | 0.10 | 0.30 | 20 |
| 2 | 内吸磷 | 0.05~100 | y=4.80E-03x+2.02E-04 | 0.9988 | 5.0 | 15 | 20 |
| 3 | 蝇毒磷 | 0.05~100 | y=1.12E-01x+7.27E-04 | 0.9993 | 0. 50 | 1.5 | 50 |
| 4 | 灭线磷 | 0.05~100 | y=1.21E-01x+4.49E-03 | 0.9997 | 0.10 | 0.30 | 20 |
| 5 | 苯线磷 | 0.05~100 | y=3.45E-01x+4.22E-03 | 0.9992 | 0.025 | 0.10 | 苯线磷及其氧类似物（砜、亚砜）之和小于20 |
| 6 | 苯线磷砜 | 0.05~100 | y=1.10E-01x+9.92E-03 | 0.9995 | 0.20 | 1.0 |
| 7 | 苯线磷亚砜 | 0.05~100 | y=9.28E-02x+1.07E-03 | 0.9997 | 0.10 | 0.30 |
| 8 | 水胺硫磷 | 0.05~100 | y=4.72E-03x+3.46E-04 | 0.9981 | 4.0 | 15 | 50 |
| 9 | 甲拌磷 | 0.05~100 | y=5.02E-03x+4.78E-04 | 0.9983 | 0.25 | 1.0 | 甲拌磷及其氧类似物（砜、亚砜）之和小于20 |
| 10 | 甲拌磷砜 | 0.05~100 | y=1.25E-02x+2.28E-03 | 0.9990 | 0.50 | 1.5 |
| 11 | 甲拌磷亚砜 | 0.05~100 | y=8.12E-02x+5.20E-03 | 0.9992 | 0.20 | 1.0 |
| 12 | 胺苯磺隆 | 0.05~100 | y=2.45E-01x+5.06E-03 | 0.9982 | 0.015 | 0.10 | 50 |
| 13 | 硫线磷 | 0.05~100 | y=2.25E-01x+4.77E-03 | 0.9996 | 0.050 | 0.15 | 20 |
| 14 | 克百威 | 0.05~100 | y=6.11E-01x+7.05E-02 | 0.9995 | 0.020 | 0.10 | 克百威及3-羟基克百威之和小于50 |
| 15 | 3-羟基克百威 | 0.05~100 | y=8.24E-02x+5.14E-03 | 0.9993 | 0.20 | 1.0 |
| 16 | 地虫硫磷 | 0.05~100 | y=2.03E-02x+5.27E-04 | 0.9994 | 0.50 | 1.5 | 20 |
| 17 | 氯唑磷 | 0.05~100 | y=9.02E-02x+2.19E-03 | 0.9997 | 0.30 | 1.0 | 10 |
| 18 | 氯磺隆 | 0.05~100 | y=6.66E-02x+4.20E-04 | 0.9992 | 0.075 | 0.50 | 50 |
| 19 | 硫环磷 | 0.05~100 | y=3.02E-01x+1.21E-02 | 0.9998 | 0.050 | 0.15 | 30 |
| 20 | 甲磺隆 | 0.05~100 | y=1.56E-01x+1.77E-03 | 0.9999 | 0.030 | 0.10 | 50 |
| 21 | 涕灭威 | 0.05~100 | y=1.98E-02x+2.50E-04 | 0.9990 | 0.20 | 1.0 | 涕灭威及其氧类似物（砜、亚砜）之和小于10 |
| 22 | 涕灭威砜 | 0.05~100 | y=4.13E-02x+2.04E-03 | 0.9995 | 0.40 | 1.5 |
| 23 | 涕灭威亚砜 | 0.05~100 | y=7.09E-02x+3.02E-03 | 0.9992 | 0.50 | 1.5 |
| 24 | 磷胺 | 0.05~100 | y=4.82E-01x+8.08E-03 | 0.9995 | 0.040 | 0.15 | 50 |
| 25 | 甲基异柳磷 | 0.05~100 | y=8.51E-02x+2.17E-03 | 0.9996 | 0.25 | 1.0 | 20 |
| 26 | 甲胺磷 | 0.05~100 | y=1.32E-01x+8.52E-03 | 0.9996 | 0.50 | 1.5 | 50 |
| 27 | 特丁硫磷砜 | 0.05~100 | y=4.58E-02x+2.23E-03 | 0.9992 | 0.20 | 1.0 | 20 |
| 28 | 特丁硫磷亚砜 | 0.05~100 | y=1.85E-01x+1.24E-03 | 0.9998 | 0.08 | 0.30 | 20 |
| 29 | 久效磷 | 0.05~100 | y=1.37E-01x+4.83E-03 | 0.9997 | 0.10 | 0.30 | 30 |
| 30 | 杀虫脒 | 0.05~100 | y=5.75E-02x+9.12E-04 | 0.9985 | 0.50 | 1.5 | 20 |
), ArticleFig(id=1320880639860134607, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, label=表4, caption=
30种农药的线性范围、回归方程、相关系数、检出限、定量限和最大残留限量
, figureFileSmall=null, figureFileBig=null, tableContent=
| 序号 | 农药 | 线性范围
（µg/L） | 回归方程 | 决定系数
（r2） | 检出限LOD
（µg/kg） | 定量限LOQ
（µg/kg） | 最大残留量MRL
（µg/kg） |
|---|
| 1 | 甲基硫环磷 | 0.05~100 | y=3.67E-01x+6.99E-03 | 0.9990 | 0.10 | 0.30 | 20 |
| 2 | 内吸磷 | 0.05~100 | y=4.80E-03x+2.02E-04 | 0.9988 | 5.0 | 15 | 20 |
| 3 | 蝇毒磷 | 0.05~100 | y=1.12E-01x+7.27E-04 | 0.9993 | 0. 50 | 1.5 | 50 |
| 4 | 灭线磷 | 0.05~100 | y=1.21E-01x+4.49E-03 | 0.9997 | 0.10 | 0.30 | 20 |
| 5 | 苯线磷 | 0.05~100 | y=3.45E-01x+4.22E-03 | 0.9992 | 0.025 | 0.10 | 苯线磷及其氧类似物（砜、亚砜）之和小于20 |
| 6 | 苯线磷砜 | 0.05~100 | y=1.10E-01x+9.92E-03 | 0.9995 | 0.20 | 1.0 |
| 7 | 苯线磷亚砜 | 0.05~100 | y=9.28E-02x+1.07E-03 | 0.9997 | 0.10 | 0.30 |
| 8 | 水胺硫磷 | 0.05~100 | y=4.72E-03x+3.46E-04 | 0.9981 | 4.0 | 15 | 50 |
| 9 | 甲拌磷 | 0.05~100 | y=5.02E-03x+4.78E-04 | 0.9983 | 0.25 | 1.0 | 甲拌磷及其氧类似物（砜、亚砜）之和小于20 |
| 10 | 甲拌磷砜 | 0.05~100 | y=1.25E-02x+2.28E-03 | 0.9990 | 0.50 | 1.5 |
| 11 | 甲拌磷亚砜 | 0.05~100 | y=8.12E-02x+5.20E-03 | 0.9992 | 0.20 | 1.0 |
| 12 | 胺苯磺隆 | 0.05~100 | y=2.45E-01x+5.06E-03 | 0.9982 | 0.015 | 0.10 | 50 |
| 13 | 硫线磷 | 0.05~100 | y=2.25E-01x+4.77E-03 | 0.9996 | 0.050 | 0.15 | 20 |
| 14 | 克百威 | 0.05~100 | y=6.11E-01x+7.05E-02 | 0.9995 | 0.020 | 0.10 | 克百威及3-羟基克百威之和小于50 |
| 15 | 3-羟基克百威 | 0.05~100 | y=8.24E-02x+5.14E-03 | 0.9993 | 0.20 | 1.0 |
| 16 | 地虫硫磷 | 0.05~100 | y=2.03E-02x+5.27E-04 | 0.9994 | 0.50 | 1.5 | 20 |
| 17 | 氯唑磷 | 0.05~100 | y=9.02E-02x+2.19E-03 | 0.9997 | 0.30 | 1.0 | 10 |
| 18 | 氯磺隆 | 0.05~100 | y=6.66E-02x+4.20E-04 | 0.9992 | 0.075 | 0.50 | 50 |
| 19 | 硫环磷 | 0.05~100 | y=3.02E-01x+1.21E-02 | 0.9998 | 0.050 | 0.15 | 30 |
| 20 | 甲磺隆 | 0.05~100 | y=1.56E-01x+1.77E-03 | 0.9999 | 0.030 | 0.10 | 50 |
| 21 | 涕灭威 | 0.05~100 | y=1.98E-02x+2.50E-04 | 0.9990 | 0.20 | 1.0 | 涕灭威及其氧类似物（砜、亚砜）之和小于10 |
| 22 | 涕灭威砜 | 0.05~100 | y=4.13E-02x+2.04E-03 | 0.9995 | 0.40 | 1.5 |
| 23 | 涕灭威亚砜 | 0.05~100 | y=7.09E-02x+3.02E-03 | 0.9992 | 0.50 | 1.5 |
| 24 | 磷胺 | 0.05~100 | y=4.82E-01x+8.08E-03 | 0.9995 | 0.040 | 0.15 | 50 |
| 25 | 甲基异柳磷 | 0.05~100 | y=8.51E-02x+2.17E-03 | 0.9996 | 0.25 | 1.0 | 20 |
| 26 | 甲胺磷 | 0.05~100 | y=1.32E-01x+8.52E-03 | 0.9996 | 0.50 | 1.5 | 50 |
| 27 | 特丁硫磷砜 | 0.05~100 | y=4.58E-02x+2.23E-03 | 0.9992 | 0.20 | 1.0 | 20 |
| 28 | 特丁硫磷亚砜 | 0.05~100 | y=1.85E-01x+1.24E-03 | 0.9998 | 0.08 | 0.30 | 20 |
| 29 | 久效磷 | 0.05~100 | y=1.37E-01x+4.83E-03 | 0.9997 | 0.10 | 0.30 | 30 |
| 30 | 杀虫脒 | 0.05~100 | y=5.75E-02x+9.12E-04 | 0.9985 | 0.50 | 1.5 | 20 |
), ArticleFig(id=1320880640011129552, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=EN, label=Table 5, caption=
Recoveries rate and relative standard deviations (RSDs) of 30 pesticide residues in 5 kinds of ginseng health food ingredients (n=6)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 农药 | 添加水平
（µg/kg） | 高丽红参 | | 丹参 | | 玄参 | | 党参 | | 太子参 |
|---|
平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） |
|---|
| 甲基硫环磷 | 0.3 | 96.8 | 1.06 | | 99.6 | 2.23 | | 99.8 | 6.85 | | 97.7 | 6.10 | | 97.5 | 2.41 |
| 0.6 | 99.8 | 1.76 | | 99.1 | 3.47 | | 95.6 | 3.91 | | 96.8 | 2.39 | | 101.2 | 2.45 |
| 3.0 | 97.4 | 4.69 | | 93.9 | 2.74 | | 95.7 | 4.38 | | 97.7 | 2.65 | | 99.2 | 3.89 |
| 内吸磷 | 15.0 | 90.2 | 1.80 | | 94.9 | 5.19 | | 91.5 | 2.21 | | 97.6 | 2.61 | | 96.7 | 1.65 |
| 30.0 | 98.7 | 1.55 | | 95.5 | 2.17 | | 98.2 | 6.16 | | 100.9 | 1.39 | | 99.2 | 1.48 |
| 150.0 | 93.4 | 2.67 | | 105.0 | 4.33 | | 94.3 | 3.19 | | 97.4 | 5.12 | | 93.7 | 3.14 |
| 蝇毒磷 | 1.5 | 95.8 | 1.82 | | 93.5 | 1.45 | | 103.2 | 1.56 | | 99.6 | 2.00 | | 96.9 | 1.76 |
| 3.0 | 101.3 | 2.53 | | 103.4 | 3.94 | | 103.3 | 3.45 | | 101.5 | 2.18 | | 103.1 | 6.85 |
| 15.0 | 97.7 | 4.89 | | 98.3 | 4.09 | | 99.2 | 3.50 | | 98.4 | 4.32 | | 97.9 | 3.75 |
| 灭线磷 | 0.3 | 99.9 | 3.40 | | 95.8 | 3.28 | | 96.8 | 1.53 | | 102.8 | 3.68 | | 98.3 | 1.95 |
| 0.6 | 94.5 | 7.19 | | 98.0 | 4.09 | | 101.9 | 2.44 | | 101.5 | 2.52 | | 100.4 | 2.25 |
| 3.0 | 97.4 | 5.26 | | 95.5 | 6.64 | | 97.9 | 4.70 | | 98.2 | 4.76 | | 97.0 | 5.47 |
| 苯线磷 | 0.1 | 100.2 | 3.22 | | 90.6 | 2.15 | | 94.3 | 5.83 | | 90.5 | 5.74 | | 94.2 | 5.32 |
| 0.2 | 103.5 | 5.33 | | 96.2 | 2.11 | | 96.9 | 4.03 | | 98.2 | 2.41 | | 95.3 | 6.01 |
| 1.0 | 98.3 | 7.52 | | 90.4 | 5.41 | | 101.2 | 7.71 | | 100.8 | 2.66 | | 97.5 | 7.12 |
| 苯线磷砜 | 1.0 | 95.8 | 4.62 | | 91.4 | 1.82 | | 87.6 | 1.65 | | 90.2 | 1.80 | | 86.4 | 3.98 |
| 2.0 | 96.3 | 3.99 | | 99.5 | 1.18 | | 99.2 | 1.48 | | 98.7 | 1.55 | | 91.5 | 6.20 |
| 10.0 | 98.5 | 3.63 | | 96.3 | 1.95 | | 93.7 | 3.14 | | 93.4 | 2.67 | | 104.4 | 3.08 |
| 苯线磷亚砜 | 0.3 | 92.3 | 8.42 | | 89.8 | 2.46 | | 89.3 | 5.67 | | 91.9 | 2.60 | | 91.1 | 6.79 |
| 0.6 | 102.1 | 5.92 | | 103.3 | 2.05 | | 94.3 | 2.02 | | 98.0 | 1.23 | | 93.4 | 6.43 |
| 3.0 | 97.5 | 2.17 | | 96.1 | 2.79 | | 95.1 | 3.04 | | 96.0 | 2.92 | | 99.4 | 4.75 |
| 水胺硫磷 | 15.0 | 90.0 | 2.20 | | 92.9 | 4.13 | | 90.2 | 5.55 | | 93.5 | 2.30 | | 94.8 | 4.62 |
| 30.0 | 91.3 | 1.40 | | 101.2 | 7.04 | | 98.8 | 6.01 | | 99.8 | 1.59 | | 90.3 | 3.99 |
| 150.0 | 95.4 | 2.80 | | 104.3 | 4.01 | | 104.7 | 4.88 | | 98.2 | 2.39 | | 98.5 | 3.63 |
| 甲拌磷 | 1.0 | 96.8 | 2.38 | | 91.3 | 2.83 | | 90.9 | 2.82 | | 91.2 | 2.83 | | 93.4 | 5.11 |
| 2.0 | 98.9 | 2.09 | | 97.1 | 2.75 | | 98.3 | 2.85 | | 96.7 | 2.40 | | 90.2 | 2.00 |
| 10.0 | 99.8 | 1.47 | | 90.6 | 3.02 | | 99.3 | 2.60 | | 99.2 | 2.98 | | 99.5 | 2.27 |
| 甲拌磷砜 | 1.5 | 99.3 | 2.01 | | 95.4 | 2.04 | | 99.7 | 2.10 | | 93.2 | 2.88 | | 96.2 | 3.34 |
| 3.0 | 95.0 | 2.78 | | 90.6 | 2.85 | | 98.5 | 2.06 | | 92.2 | 1.79 | | 98.3 | 1.87 |
| 15.0 | 95.2 | 3.31 | | 93.1 | 1.54 | | 100.3 | 1.66 | | 99.6 | 2.02 | | 94.6 | 1.22 |
| 甲拌磷亚砜 | 1.0 | 92.4 | 7.23 | | 91.0 | 4.37 | | 93.9 | 2.91 | | 88.5 | 4.36 | | 92.0 | 2.41 |
| 2.0 | 93.2 | 1.98 | | 92.8 | 6.04 | | 96.5 | 1.35 | | 96.0 | 1.34 | | 93.2 | 1.34 |
| 10.0 | 90.6 | 3.18 | | 98.3 | 3.03 | | 96.5 | 2.77 | | 96.4 | 2.94 | | 97.7 | 2.73 |
| 胺苯磺隆 | 0.1 | 93.1 | 8.62 | | 90.2 | 2.46 | | 91.3 | 5.67 | | 91.9 | 2.60 | | 90.8 | 6.79 |
| 0.2 | 92.1 | 5.92 | | 93.3 | 2.05 | | 94.3 | 2.02 | | 98.0 | 1.23 | | 93.4 | 6.43 |
| 1.0 | 97.5 | 2.17 | | 96.1 | 2.79 | | 95.1 | 3.04 | | 96.0 | 2.92 | | 99.4 | 4.75 |
| 硫线磷 | 0.15 | 93.0 | 7.23 | | 102.8 | 4.37 | | 93.9 | 2.91 | | 92.3 | 4.36 | | 92.0 | 2.41 |
| 0.3 | 92.8 | 1.98 | | 102.8 | 6.04 | | 96.5 | 1.35 | | 96.0 | 1.34 | | 99.2 | 1.34 |
| 1.5 | 102.6 | 3.18 | | 98.3 | 3.03 | | 96.5 | 2.77 | | 96.4 | 2.94 | | 97.7 | 2.73 |
| 克百威 | 0.1 | 95.3 | 3.00 | | 89.5 | 2.28 | | 96.0 | 1.88 | | 90.8 | 3.80 | | 100.7 | 2.55 |
| 0.2 | 93.4 | 3.99 | | 88.9 | 3.38 | | 97.1 | 2.35 | | 97.6 | 6.46 | | 93.8 | 4.65 |
| 1.0 | 99.5 | 1.04 | | 91.1 | 4.18 | | 94.0 | 3.09 | | 99.2 | 3.98 | | 94.1 | 0.36 |
| 3-羟基克百威 | 1.0 | 101.0 | 1.85 | | 101.1 | 2.31 | | 98.5 | 2.83 | | 101.3 | 2.56 | | 97.2 | 1.61 |
| 2.0 | 110.4 | 3.72 | | 100.5 | 2.39 | | 100.8 | 6.08 | | 98.9 | 3.20 | | 107.2 | 2.56 |
| 10.0 | 111.0 | 6.01 | | 99.5 | 2.20 | | 97.3 | 2.75 | | 99.8 | 1.34 | | 97.5 | 6.88 |
| 地虫硫磷 | 1.5 | 102.2 | 1.54 | | 99.6 | 3.12 | | 92.5 | 0.84 | | 96.3 | 1.64 | | 102.2 | 1.07 |
| 3.0 | 98.4 | 1.87 | | 99.7 | 3.53 | | 97.1 | 3.93 | | 101.0 | 1.74 | | 98.3 | 2.48 |
| 15.0 | 105.0 | 5.13 | | 98.2 | 1.75 | | 97.1 | 3.04 | | 99.0 | 4.85 | | 96.1 | 2.94 |
| 氯唑磷 | 1.0 | 108.9 | 2.91 | | 100.8 | 2.99 | | 95.8 | 2.12 | | 99.5 | 3.66 | | 102.5 | 3.35 |
| 2.0 | 98.3 | 7.06 | | 100.5 | 2.76 | | 103.8 | 5.37 | | 101.8 | 2.74 | | 99.7 | 1.49 |
| 10.0 | 99.3 | 1.69 | | 96.8 | 0.88 | | 98.6 | 5.72 | | 100.5 | 0.90 | | 96.6 | 1.40 |
| 氯磺隆 | 0.5 | 98.3 | 4.78 | | 90.6 | 4.15 | | 96.7 | 4.87 | | 100.1 | 6.66 | | 96.8 | 4.16 |
| 1.0 | 96.9 | 4.09 | | 108.1 | 2.36 | | 95.2 | 5.68 | | 97.5 | 1.48 | | 93.0 | 3.94 |
| 5.0 | 101.7 | 1.46 | | 93.4 | 1.98 | | 102.1 | 3.15 | | 103.4 | 0.88 | | 100.4 | 3.70 |
| 硫环磷 | 0.15 | 93.9 | 5.60 | | 101.9 | 2.19 | | 102.8 | 3.04 | | 104.5 | 5.39 | | 91.1 | 2.53 |
| 0.3 | 109.0 | 3.30 | | 99.9 | 1.49 | | 99.8 | 1.57 | | 90.8 | 1.76 | | 99.9 | 1.89 |
| 1.5 | 113.1 | 6.50 | | 94.5 | 1.64 | | 94.0 | 0.85 | | 99.5 | 2.21 | | 102.3 | 3.51 |
| 甲磺隆 | 0.1 | 94.5 | 6.56 | | 92.8 | 4.37 | | 93.9 | 2.91 | | 90.5 | 4.36 | | 90.5 | 4.11 |
| 0.2 | 93.1 | 1.41 | | 91.0 | 6.04 | | 96.5 | 1.35 | | 96.0 | 1.34 | | 92.7 | 0.95 |
| 1.0 | 99.5 | 2.53 | | 98.3 | 3.03 | | 96.5 | 2.77 | | 93.4 | 2.94 | | 95.3 | 2.76 |
| 涕灭威 | 1.0 | 97.0 | 7.07 | | 98.7 | 8.52 | | 102.3 | 3.82 | | 100.7 | 2.35 | | 96.0 | 3.12 |
| 2.0 | 93.0 | 6.76 | | 99.2 | 1.48 | | 91.1 | 1.68 | | 98.0 | 5.63 | | 90.2 | 2.44 |
| 10.0 | 94.5 | 5.97 | | 93.5 | 1.98 | | 94.0 | 0.65 | | 100.1 | 5.30 | | 101.4 | 2.34 |
| 涕灭威砜 | 1.5 | 90.4 | 8.33 | | 94.0 | 7.33 | | 93.3 | 7.71 | | 90.2 | 7.45 | | 94.5 | 6.16 |
| 3.0 | 92.9 | 6.05 | | 95.7 | 6.73 | | 96.4 | 7.32 | | 96.8 | 5.53 | | 95.0 | 6.47 |
| 15.0 | 91.7 | 5.76 | | 97.9 | 5.97 | | 97.9 | 6.38 | | 100.8 | 4.56 | | 93.6 | 5.53 |
| 涕灭威亚砜 | 1.5 | 95.3 | 6.86 | | 91.5 | 5.61 | | 94.5 | 7.31 | | 90.9 | 7.06 | | 91.1 | 6.53 |
| 3.0 | 90.3 | 5.58 | | 93.0 | 6.69 | | 91.4 | 5.72 | | 93.1 | 6.35 | | 98.2 | 6.45 |
| 15.0 | 97.4 | 5.18 | | 101.2 | 5.47 | | 93.0 | 6.16 | | 98.7 | 5.71 | | 94.2 | 4.60 |
| 磷胺 | 0.15 | 95.5 | 7.29 | | 94.6 | 4.72 | | 92.0 | 5.08 | | 90.6 | 5.74 | | 90.9 | 6.57 |
| 0.3 | 99.2 | 6.29 | | 92.3 | 5.74 | | 93.4 | 6.28 | | 94.3 | 5.10 | | 92.2 | 6.39 |
| 1.5 | 94.3 | 5.84 | | 94.9 | 5.28 | | 94.6 | 5.00 | | 97.1 | 5.53 | | 98.2 | 7.06 |
| 甲基异柳磷 | 1.0 | 97.0 | 2.03 | | 96.0 | 3.33 | | 91.5 | 2.07 | | 99.0 | 3.10 | | 95.0 | 4..09 |
| 2.0 | 95.7 | 1.05 | | 94.7 | 2.02 | | 98.2 | 1.88 | | 101.0 | 2.11 | | 97.8 | 4.11 |
| 10.0 | 99.4 | 3.11 | | 96.1 | 1.06 | | 96.3 | 2.62 | | 97.8 | 2.08 | | 97.0 | 2.17 |
| 甲胺磷 | 1.5 | 95.9 | 2.33 | | 91.6 | 3.14 | | 95.3 | 3.83 | | 90.5 | 4.11 | | 95.7 | 7.78 |
| 3.0 | 102.5 | 2.22 | | 96.4 | 1.58 | | 97.2 | 1.03 | | 96.7 | 0.95 | | 92.5 | 3.87 |
| 15.0 | 94.5 | 4.80 | | 96.7 | 3.60 | | 91.4 | 6.71 | | 95.3 | 2.76 | | 92.0 | 8.03 |
| 特丁硫磷砜 | 1.0 | 96.2 | 3.02 | | 94.4 | 3.10 | | 96.8 | 6.70 | | 95.3 | 8.74 | | 93.0 | 3.15 |
| 2.0 | 92.4 | 1.91 | | 93.8 | 1.96 | | 97.5 | 1.92 | | 98.8 | 1.95 | | 92.4 | 1.59 |
| 10.0 | 92.8 | 3.45 | | 93.7 | 4.75 | | 99.3 | 3.18 | | 99.7 | 3.95 | | 95.1 | 5.14 |
| 特丁硫磷亚砜 | 0.3 | 93.0 | 0.39 | | 92.9 | 2.08 | | 96.9 | 5.36 | | 95.1 | 0.88 | | 94.3 | 6.13 |
| 0.6 | 95.0 | 1.02 | | 97.7 | 1.97 | | 96.8 | 3.74 | | 96.3 | 2.63 | | 98.0 | 3.42 |
| 3.0 | 92.9 | 2.05 | | 93.2 | 3.05 | | 94.3 | 3.90 | | 98.5 | 1.06 | | 91.5 | 3.41 |
| 久效磷 | 0.3 | 98.9 | 5.08 | | 96.8 | 2.20 | | 97.5 | 1.34 | | 95.1 | 3.52 | | 96.5 | 5.09 |
| 0.6 | 92.0 | 1.93 | | 98.5 | 0.99 | | 96.6 | 3.32 | | 94.4 | 5.02 | | 97.2 | 1.49 |
| 3.0 | 95.4 | 2.08 | | 97.3 | 1.47 | | 90.2 | 1.17 | | 95.6 | 5.82 | | 94.9 | 3.38 |
| 杀虫脒 | 1.5 | 93.4 | 4.86 | | 97.2 | 1.65 | | 96.3 | 6.35 | | 98.1 | 4.21 | | 96.2 | 5.50 |
| 3.0 | 96.8 | 1.39 | | 94.6 | 3.23 | | 95.7 | 3.66 | | 98.3 | 4.02 | | 105.0 | 2.40 |
| 15.0 | 93.4 | 2.04 | | 97.2 | 2.68 | | 99.2 | 2.85 | | 93.6 | 3.17 | | 96.5 | 3.17 |
), ArticleFig(id=1320880640120181457, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, label=表5, caption=
5种参类保健食品原料中30种农残量的回收率和准确度（n=6）
, figureFileSmall=null, figureFileBig=null, tableContent=
| 农药 | 添加水平
（µg/kg） | 高丽红参 | | 丹参 | | 玄参 | | 党参 | | 太子参 |
|---|
平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） | | 平均回收率
（%） | RSD
（%） |
|---|
| 甲基硫环磷 | 0.3 | 96.8 | 1.06 | | 99.6 | 2.23 | | 99.8 | 6.85 | | 97.7 | 6.10 | | 97.5 | 2.41 |
| 0.6 | 99.8 | 1.76 | | 99.1 | 3.47 | | 95.6 | 3.91 | | 96.8 | 2.39 | | 101.2 | 2.45 |
| 3.0 | 97.4 | 4.69 | | 93.9 | 2.74 | | 95.7 | 4.38 | | 97.7 | 2.65 | | 99.2 | 3.89 |
| 内吸磷 | 15.0 | 90.2 | 1.80 | | 94.9 | 5.19 | | 91.5 | 2.21 | | 97.6 | 2.61 | | 96.7 | 1.65 |
| 30.0 | 98.7 | 1.55 | | 95.5 | 2.17 | | 98.2 | 6.16 | | 100.9 | 1.39 | | 99.2 | 1.48 |
| 150.0 | 93.4 | 2.67 | | 105.0 | 4.33 | | 94.3 | 3.19 | | 97.4 | 5.12 | | 93.7 | 3.14 |
| 蝇毒磷 | 1.5 | 95.8 | 1.82 | | 93.5 | 1.45 | | 103.2 | 1.56 | | 99.6 | 2.00 | | 96.9 | 1.76 |
| 3.0 | 101.3 | 2.53 | | 103.4 | 3.94 | | 103.3 | 3.45 | | 101.5 | 2.18 | | 103.1 | 6.85 |
| 15.0 | 97.7 | 4.89 | | 98.3 | 4.09 | | 99.2 | 3.50 | | 98.4 | 4.32 | | 97.9 | 3.75 |
| 灭线磷 | 0.3 | 99.9 | 3.40 | | 95.8 | 3.28 | | 96.8 | 1.53 | | 102.8 | 3.68 | | 98.3 | 1.95 |
| 0.6 | 94.5 | 7.19 | | 98.0 | 4.09 | | 101.9 | 2.44 | | 101.5 | 2.52 | | 100.4 | 2.25 |
| 3.0 | 97.4 | 5.26 | | 95.5 | 6.64 | | 97.9 | 4.70 | | 98.2 | 4.76 | | 97.0 | 5.47 |
| 苯线磷 | 0.1 | 100.2 | 3.22 | | 90.6 | 2.15 | | 94.3 | 5.83 | | 90.5 | 5.74 | | 94.2 | 5.32 |
| 0.2 | 103.5 | 5.33 | | 96.2 | 2.11 | | 96.9 | 4.03 | | 98.2 | 2.41 | | 95.3 | 6.01 |
| 1.0 | 98.3 | 7.52 | | 90.4 | 5.41 | | 101.2 | 7.71 | | 100.8 | 2.66 | | 97.5 | 7.12 |
| 苯线磷砜 | 1.0 | 95.8 | 4.62 | | 91.4 | 1.82 | | 87.6 | 1.65 | | 90.2 | 1.80 | | 86.4 | 3.98 |
| 2.0 | 96.3 | 3.99 | | 99.5 | 1.18 | | 99.2 | 1.48 | | 98.7 | 1.55 | | 91.5 | 6.20 |
| 10.0 | 98.5 | 3.63 | | 96.3 | 1.95 | | 93.7 | 3.14 | | 93.4 | 2.67 | | 104.4 | 3.08 |
| 苯线磷亚砜 | 0.3 | 92.3 | 8.42 | | 89.8 | 2.46 | | 89.3 | 5.67 | | 91.9 | 2.60 | | 91.1 | 6.79 |
| 0.6 | 102.1 | 5.92 | | 103.3 | 2.05 | | 94.3 | 2.02 | | 98.0 | 1.23 | | 93.4 | 6.43 |
| 3.0 | 97.5 | 2.17 | | 96.1 | 2.79 | | 95.1 | 3.04 | | 96.0 | 2.92 | | 99.4 | 4.75 |
| 水胺硫磷 | 15.0 | 90.0 | 2.20 | | 92.9 | 4.13 | | 90.2 | 5.55 | | 93.5 | 2.30 | | 94.8 | 4.62 |
| 30.0 | 91.3 | 1.40 | | 101.2 | 7.04 | | 98.8 | 6.01 | | 99.8 | 1.59 | | 90.3 | 3.99 |
| 150.0 | 95.4 | 2.80 | | 104.3 | 4.01 | | 104.7 | 4.88 | | 98.2 | 2.39 | | 98.5 | 3.63 |
| 甲拌磷 | 1.0 | 96.8 | 2.38 | | 91.3 | 2.83 | | 90.9 | 2.82 | | 91.2 | 2.83 | | 93.4 | 5.11 |
| 2.0 | 98.9 | 2.09 | | 97.1 | 2.75 | | 98.3 | 2.85 | | 96.7 | 2.40 | | 90.2 | 2.00 |
| 10.0 | 99.8 | 1.47 | | 90.6 | 3.02 | | 99.3 | 2.60 | | 99.2 | 2.98 | | 99.5 | 2.27 |
| 甲拌磷砜 | 1.5 | 99.3 | 2.01 | | 95.4 | 2.04 | | 99.7 | 2.10 | | 93.2 | 2.88 | | 96.2 | 3.34 |
| 3.0 | 95.0 | 2.78 | | 90.6 | 2.85 | | 98.5 | 2.06 | | 92.2 | 1.79 | | 98.3 | 1.87 |
| 15.0 | 95.2 | 3.31 | | 93.1 | 1.54 | | 100.3 | 1.66 | | 99.6 | 2.02 | | 94.6 | 1.22 |
| 甲拌磷亚砜 | 1.0 | 92.4 | 7.23 | | 91.0 | 4.37 | | 93.9 | 2.91 | | 88.5 | 4.36 | | 92.0 | 2.41 |
| 2.0 | 93.2 | 1.98 | | 92.8 | 6.04 | | 96.5 | 1.35 | | 96.0 | 1.34 | | 93.2 | 1.34 |
| 10.0 | 90.6 | 3.18 | | 98.3 | 3.03 | | 96.5 | 2.77 | | 96.4 | 2.94 | | 97.7 | 2.73 |
| 胺苯磺隆 | 0.1 | 93.1 | 8.62 | | 90.2 | 2.46 | | 91.3 | 5.67 | | 91.9 | 2.60 | | 90.8 | 6.79 |
| 0.2 | 92.1 | 5.92 | | 93.3 | 2.05 | | 94.3 | 2.02 | | 98.0 | 1.23 | | 93.4 | 6.43 |
| 1.0 | 97.5 | 2.17 | | 96.1 | 2.79 | | 95.1 | 3.04 | | 96.0 | 2.92 | | 99.4 | 4.75 |
| 硫线磷 | 0.15 | 93.0 | 7.23 | | 102.8 | 4.37 | | 93.9 | 2.91 | | 92.3 | 4.36 | | 92.0 | 2.41 |
| 0.3 | 92.8 | 1.98 | | 102.8 | 6.04 | | 96.5 | 1.35 | | 96.0 | 1.34 | | 99.2 | 1.34 |
| 1.5 | 102.6 | 3.18 | | 98.3 | 3.03 | | 96.5 | 2.77 | | 96.4 | 2.94 | | 97.7 | 2.73 |
| 克百威 | 0.1 | 95.3 | 3.00 | | 89.5 | 2.28 | | 96.0 | 1.88 | | 90.8 | 3.80 | | 100.7 | 2.55 |
| 0.2 | 93.4 | 3.99 | | 88.9 | 3.38 | | 97.1 | 2.35 | | 97.6 | 6.46 | | 93.8 | 4.65 |
| 1.0 | 99.5 | 1.04 | | 91.1 | 4.18 | | 94.0 | 3.09 | | 99.2 | 3.98 | | 94.1 | 0.36 |
| 3-羟基克百威 | 1.0 | 101.0 | 1.85 | | 101.1 | 2.31 | | 98.5 | 2.83 | | 101.3 | 2.56 | | 97.2 | 1.61 |
| 2.0 | 110.4 | 3.72 | | 100.5 | 2.39 | | 100.8 | 6.08 | | 98.9 | 3.20 | | 107.2 | 2.56 |
| 10.0 | 111.0 | 6.01 | | 99.5 | 2.20 | | 97.3 | 2.75 | | 99.8 | 1.34 | | 97.5 | 6.88 |
| 地虫硫磷 | 1.5 | 102.2 | 1.54 | | 99.6 | 3.12 | | 92.5 | 0.84 | | 96.3 | 1.64 | | 102.2 | 1.07 |
| 3.0 | 98.4 | 1.87 | | 99.7 | 3.53 | | 97.1 | 3.93 | | 101.0 | 1.74 | | 98.3 | 2.48 |
| 15.0 | 105.0 | 5.13 | | 98.2 | 1.75 | | 97.1 | 3.04 | | 99.0 | 4.85 | | 96.1 | 2.94 |
| 氯唑磷 | 1.0 | 108.9 | 2.91 | | 100.8 | 2.99 | | 95.8 | 2.12 | | 99.5 | 3.66 | | 102.5 | 3.35 |
| 2.0 | 98.3 | 7.06 | | 100.5 | 2.76 | | 103.8 | 5.37 | | 101.8 | 2.74 | | 99.7 | 1.49 |
| 10.0 | 99.3 | 1.69 | | 96.8 | 0.88 | | 98.6 | 5.72 | | 100.5 | 0.90 | | 96.6 | 1.40 |
| 氯磺隆 | 0.5 | 98.3 | 4.78 | | 90.6 | 4.15 | | 96.7 | 4.87 | | 100.1 | 6.66 | | 96.8 | 4.16 |
| 1.0 | 96.9 | 4.09 | | 108.1 | 2.36 | | 95.2 | 5.68 | | 97.5 | 1.48 | | 93.0 | 3.94 |
| 5.0 | 101.7 | 1.46 | | 93.4 | 1.98 | | 102.1 | 3.15 | | 103.4 | 0.88 | | 100.4 | 3.70 |
| 硫环磷 | 0.15 | 93.9 | 5.60 | | 101.9 | 2.19 | | 102.8 | 3.04 | | 104.5 | 5.39 | | 91.1 | 2.53 |
| 0.3 | 109.0 | 3.30 | | 99.9 | 1.49 | | 99.8 | 1.57 | | 90.8 | 1.76 | | 99.9 | 1.89 |
| 1.5 | 113.1 | 6.50 | | 94.5 | 1.64 | | 94.0 | 0.85 | | 99.5 | 2.21 | | 102.3 | 3.51 |
| 甲磺隆 | 0.1 | 94.5 | 6.56 | | 92.8 | 4.37 | | 93.9 | 2.91 | | 90.5 | 4.36 | | 90.5 | 4.11 |
| 0.2 | 93.1 | 1.41 | | 91.0 | 6.04 | | 96.5 | 1.35 | | 96.0 | 1.34 | | 92.7 | 0.95 |
| 1.0 | 99.5 | 2.53 | | 98.3 | 3.03 | | 96.5 | 2.77 | | 93.4 | 2.94 | | 95.3 | 2.76 |
| 涕灭威 | 1.0 | 97.0 | 7.07 | | 98.7 | 8.52 | | 102.3 | 3.82 | | 100.7 | 2.35 | | 96.0 | 3.12 |
| 2.0 | 93.0 | 6.76 | | 99.2 | 1.48 | | 91.1 | 1.68 | | 98.0 | 5.63 | | 90.2 | 2.44 |
| 10.0 | 94.5 | 5.97 | | 93.5 | 1.98 | | 94.0 | 0.65 | | 100.1 | 5.30 | | 101.4 | 2.34 |
| 涕灭威砜 | 1.5 | 90.4 | 8.33 | | 94.0 | 7.33 | | 93.3 | 7.71 | | 90.2 | 7.45 | | 94.5 | 6.16 |
| 3.0 | 92.9 | 6.05 | | 95.7 | 6.73 | | 96.4 | 7.32 | | 96.8 | 5.53 | | 95.0 | 6.47 |
| 15.0 | 91.7 | 5.76 | | 97.9 | 5.97 | | 97.9 | 6.38 | | 100.8 | 4.56 | | 93.6 | 5.53 |
| 涕灭威亚砜 | 1.5 | 95.3 | 6.86 | | 91.5 | 5.61 | | 94.5 | 7.31 | | 90.9 | 7.06 | | 91.1 | 6.53 |
| 3.0 | 90.3 | 5.58 | | 93.0 | 6.69 | | 91.4 | 5.72 | | 93.1 | 6.35 | | 98.2 | 6.45 |
| 15.0 | 97.4 | 5.18 | | 101.2 | 5.47 | | 93.0 | 6.16 | | 98.7 | 5.71 | | 94.2 | 4.60 |
| 磷胺 | 0.15 | 95.5 | 7.29 | | 94.6 | 4.72 | | 92.0 | 5.08 | | 90.6 | 5.74 | | 90.9 | 6.57 |
| 0.3 | 99.2 | 6.29 | | 92.3 | 5.74 | | 93.4 | 6.28 | | 94.3 | 5.10 | | 92.2 | 6.39 |
| 1.5 | 94.3 | 5.84 | | 94.9 | 5.28 | | 94.6 | 5.00 | | 97.1 | 5.53 | | 98.2 | 7.06 |
| 甲基异柳磷 | 1.0 | 97.0 | 2.03 | | 96.0 | 3.33 | | 91.5 | 2.07 | | 99.0 | 3.10 | | 95.0 | 4..09 |
| 2.0 | 95.7 | 1.05 | | 94.7 | 2.02 | | 98.2 | 1.88 | | 101.0 | 2.11 | | 97.8 | 4.11 |
| 10.0 | 99.4 | 3.11 | | 96.1 | 1.06 | | 96.3 | 2.62 | | 97.8 | 2.08 | | 97.0 | 2.17 |
| 甲胺磷 | 1.5 | 95.9 | 2.33 | | 91.6 | 3.14 | | 95.3 | 3.83 | | 90.5 | 4.11 | | 95.7 | 7.78 |
| 3.0 | 102.5 | 2.22 | | 96.4 | 1.58 | | 97.2 | 1.03 | | 96.7 | 0.95 | | 92.5 | 3.87 |
| 15.0 | 94.5 | 4.80 | | 96.7 | 3.60 | | 91.4 | 6.71 | | 95.3 | 2.76 | | 92.0 | 8.03 |
| 特丁硫磷砜 | 1.0 | 96.2 | 3.02 | | 94.4 | 3.10 | | 96.8 | 6.70 | | 95.3 | 8.74 | | 93.0 | 3.15 |
| 2.0 | 92.4 | 1.91 | | 93.8 | 1.96 | | 97.5 | 1.92 | | 98.8 | 1.95 | | 92.4 | 1.59 |
| 10.0 | 92.8 | 3.45 | | 93.7 | 4.75 | | 99.3 | 3.18 | | 99.7 | 3.95 | | 95.1 | 5.14 |
| 特丁硫磷亚砜 | 0.3 | 93.0 | 0.39 | | 92.9 | 2.08 | | 96.9 | 5.36 | | 95.1 | 0.88 | | 94.3 | 6.13 |
| 0.6 | 95.0 | 1.02 | | 97.7 | 1.97 | | 96.8 | 3.74 | | 96.3 | 2.63 | | 98.0 | 3.42 |
| 3.0 | 92.9 | 2.05 | | 93.2 | 3.05 | | 94.3 | 3.90 | | 98.5 | 1.06 | | 91.5 | 3.41 |
| 久效磷 | 0.3 | 98.9 | 5.08 | | 96.8 | 2.20 | | 97.5 | 1.34 | | 95.1 | 3.52 | | 96.5 | 5.09 |
| 0.6 | 92.0 | 1.93 | | 98.5 | 0.99 | | 96.6 | 3.32 | | 94.4 | 5.02 | | 97.2 | 1.49 |
| 3.0 | 95.4 | 2.08 | | 97.3 | 1.47 | | 90.2 | 1.17 | | 95.6 | 5.82 | | 94.9 | 3.38 |
| 杀虫脒 | 1.5 | 93.4 | 4.86 | | 97.2 | 1.65 | | 96.3 | 6.35 | | 98.1 | 4.21 | | 96.2 | 5.50 |
| 3.0 | 96.8 | 1.39 | | 94.6 | 3.23 | | 95.7 | 3.66 | | 98.3 | 4.02 | | 105.0 | 2.40 |
| 15.0 | 93.4 | 2.04 | | 97.2 | 2.68 | | 99.2 | 2.85 | | 93.6 | 3.17 | | 96.5 | 3.17 |
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Detection results of 30 pesticide residues in 5 kinds of ginseng health food ingredients
, figureFileSmall=null, figureFileBig=null, tableContent=
| 样品名称 | 农药残留量（µg/kg） |
|---|
| 甲拌磷砜 | 甲拌磷亚砜 | 标准值 | 克百威 | 氯磺隆 | 标准值 |
|---|
| 丹参 | 1# | 279.8 | / | ≤20 | / | / | ≤50 |
| 2# | 871.8 | / | / | / |
| 3# | 91.44 | / | / | / |
| 4# | 87.29 | / | / | / |
| 5# | 87.72 | / | / | / |
| 太子参 | 1# | / | / | 38.11 | / |
| 高丽红参 | 1# | / | / | / | 362.5 |
| 2# | / | / | / | 293.3 |
), ArticleFig(id=1320880640304730835, tenantId=1146029695717560320, journalId=1260987677001138203, articleId=1320880633191191201, language=CN, label=表6, caption=
5种参类保健食品原料中30种农残量的阳性样品检出结果
, figureFileSmall=null, figureFileBig=null, tableContent=
| 样品名称 | 农药残留量（µg/kg） |
|---|
| 甲拌磷砜 | 甲拌磷亚砜 | 标准值 | 克百威 | 氯磺隆 | 标准值 |
|---|
| 丹参 | 1# | 279.8 | / | ≤20 | / | / | ≤50 |
| 2# | 871.8 | / | / | / |
| 3# | 91.44 | / | / | / |
| 4# | 87.29 | / | / | / |
| 5# | 87.72 | / | / | / |
| 太子参 | 1# | / | / | 38.11 | / |
| 高丽红参 | 1# | / | / | / | 362.5 |
| 2# | / | / | / | 293.3 |
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