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Determination of 26 kinds of veterinary drug residues in duck meat by ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry
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Si SUN1, Mei YANG1, Tai-Yang LIU1, Wen-Feng LIU1, Zhong-Rong WANG2, *
Journal of Food Safety & Quality | 2025, 16(11) : 186 - 192
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Journal of Food Safety & Quality | 2025, 16(11): 186-192
• Special Topic: Analysis and Monitoring of Toxic and Harmful Substances in Food •
Determination of 26 kinds of veterinary drug residues in duck meat by ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry
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Si SUN1, Mei YANG1, Tai-Yang LIU1, Wen-Feng LIU1, Zhong-Rong WANG2, *
Affiliations
  • 1. Examing and Inspection Center for Agricultural Products Safety and Quality of Qiandongnan Zhou Prefecture, Kaili 556000, China
  • 2. Guizhou Provincial Qiandongnan Center for Animal Disease Control and Prevention, Kaili 556000, China
Published: 2025-06-15 doi: 10.19812/j.cnki.jfsq11-5956/ts.20250120003
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Objective To establish a method for the simultaneous determination of 26 kinds of veterinary drug residues in 3 categories including sulfonamide, quinolones and tetracyclines based on duck meat by ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry. Methods The 0.1% formic acid acetonitrile extraction was used, QuEChERS purification agent was used to remove impurities. After nitrogen blowing in a 45 ℃ water bath to near dryness, the mixture was diluted with 0.1% formic acid water acetonitrile (1:1, V:V) and analyzed qualitatively and quantitatively using ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry. Results The 26 kinds of veterinary drugs showed good linearity in the range of 2.0-300.0 ng/mL (r2≥0.9996), the limits of detection were 0.28-6.02 μg/kg, the limits of quantification were 11.28-15.03 μg/kg. The average recovery rates of 26 kinds of veterinary drugs at different concentration levels (5.0, 50.0, 300.0 μg/kg) were 75.08%-112.35% (n=15), and the relative standard deviations (RSDs) were 1.25%-7.88% (n=15). Conclusion This method features simple pretreatment operations, high efficiency, and low consumption of reagents and materials. It is suitable for the preliminary screening and detection of 26 kinds of veterinary drug residues in 3 categories for large quantities of duck meat samples.

ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry  /  veterinary drug residues  /  quick screening  /  duck meat
Si SUN, Mei YANG, Tai-Yang LIU, Wen-Feng LIU, Zhong-Rong WANG. Determination of 26 kinds of veterinary drug residues in duck meat by ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry[J]. Journal of Food Safety & Quality, 2025 , 16 (11) : 186 -192 . DOI: 10.19812/j.cnki.jfsq11-5956/ts.20250120003
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Year 2025 volume 16 Issue 11
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doi: 10.19812/j.cnki.jfsq11-5956/ts.20250120003
  • Receive Date：2025-01-20
  • Online Date：2025-07-14
  • Published：2025-06-15
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  • Received：2025-01-20
Affiliations
    1. Examing and Inspection Center for Agricultural Products Safety and Quality of Qiandongnan Zhou Prefecture, Kaili 556000, China
    2. Guizhou Provincial Qiandongnan Center for Animal Disease Control and Prevention, Kaili 556000, China
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多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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