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Analysis of volatile flavor components in Osmanthus fragrans-aged liqueur at different storage durations by gas chromatography-tandem mass spectrometry
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Shui-Yan LV1, Di-Shu HUANG2, Gao-Jian CHEN2, Yan ZHENG2, Ai-Ping LI3, Li-Chang TANG2, *
Journal of Food Safety & Quality | 2026, 17(18) : 164 - 172
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Journal of Food Safety & Quality | 2026, 17(18): 164-172
• Special Topic: Rapid Detection Technology for Food Safety •
Analysis of volatile flavor components in Osmanthus fragrans-aged liqueur at different storage durations by gas chromatography-tandem mass spectrometry
Full
Shui-Yan LV1, Di-Shu HUANG2, Gao-Jian CHEN2, Yan ZHENG2, Ai-Ping LI3, Li-Chang TANG2, *
Affiliations
  • 1.Yulin Science and Technology Development Experimental Center, Yulin 537000, China
  • 2.Beihai Public Inspection and Testing Center, Beihai 536000, China
  • 3.Guilin Yijiang Jiuye, Co., Ltd., Guilin 541000, China
doi: 10.19812/j.cnki.jfsq11-5956/ts.20260506001
Outline
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Objective

To investigate the effects of different storage durations on the volatile flavor components of Osmanthus fragrans‑aged liqueur by gas chromatography‑tandem mass spectrometry (GC‑MS/MS).

Methods

Taking Chuanshanyan cave‑aged Osmanthus fragrans‑aged liqueur as the research object, 3 groups of samples were selected:initial bottling stage, after 2 years of storage durations and after 3 years of storage durations. GC‑MS/MSwas used to qualitatively detect and compare the volatile flavor components of the Osmanthus fragrans‑aged liqueur at different storage durations.

Results

With increasing storage durations, the total number of volatile flavor compounds in the Osmanthus fragrans‑aged liqueur showed an initial increase followed by a decrease: 29 kinds of compounds were detected at the initial bottling stage, which increased to 32 kinds of after 2 years of storage durations, and further decreased to 27 kinds of after 3 years of storage durations. The number of alcohol species remained stable across all 3 stages, but their content gradually decreased with prolonged storage. The numbers of ester and aldehyde both exhibited an initial increase followed by a decline, with esters decreasing significantly after 3 years of storage, and acids increasing by one species at the 2‑year stage and then remaining stable. Other compounds gradually diminished during storage and completely disappeared after 3 years. During the aging process, unstable and pungent flavor components gradually diminished.

Conclusion

This study reveals the evolution patterns of volatile flavor compounds in Osmanthus fragrans‑aged liqueur during cave aging, clarifies the differential responses of various flavor components to the storage duration, and makes the aroma structure of structure more streamlined and coordinated. It can provide a reference for controlling reasonable storage durations and ensuring stable quality production of this type of characteristic fruit liqueur.

Osmanthus fragrans-aged liqueur  /  storage duration  /  volatile flavor substances  /  gas chromatography‑tandem mass spectrometry
吕水燕, 黄荻舒, 陈高健, 郑燕, 李爱平, 汤丽昌. 气相色谱-串联质谱法分析不同贮藏年限桂花陈酿酒挥发性风味成分. 食品安全质量检测学报, 2026 , 17 (18) : 164 -172 . DOI: 10.19812/j.cnki.jfsq11-5956/ts.20260506001
Shui-Yan LV, Di-Shu HUANG, Gao-Jian CHEN, Yan ZHENG, Ai-Ping LI, Li-Chang TANG. Analysis of volatile flavor components in Osmanthus fragrans-aged liqueur at different storage durations by gas chromatography-tandem mass spectrometry[J]. Journal of Food Safety & Quality, 2026 , 17 (18) : 164 -172 . DOI: 10.19812/j.cnki.jfsq11-5956/ts.20260506001
Year 2026 volume 17 Issue 18
8
2
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Article Info
doi: 10.19812/j.cnki.jfsq11-5956/ts.20260506001
  • Receive Date:2026-05-06
  • Online Date:2026-11-05
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  • Received:2026-05-06
Funding
Affiliations
    1.Yulin Science and Technology Development Experimental Center, Yulin 537000, China
    2.Beihai Public Inspection and Testing Center, Beihai 536000, China
    3.Guilin Yijiang Jiuye, Co., Ltd., Guilin 541000, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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