Home Journals Articles Updates About
CN
image
收藏切换
Simultaneous determination of 12 kinds of nicotine pesticides in fruits by ultra performance liquid chromatography-tandem mass spectrometry coupled with cold induced liquid-liquid extraction
收藏切换
PDF
Qiang LIN1, Yun-Kui SHEN1, Chao YANG1, Mei-Li LI1, Jia WANG1, Ding-Guo JIANG2, *, Sai FAN3, *
Journal of Food Safety & Quality | 2025, 16(4) : 71 - 77
Less
收藏切换
Journal of Food Safety & Quality | 2025, 16(4): 71-77
• Special Topic: Research and Detection of Pesticide and Veterinary Drug Residue •
Simultaneous determination of 12 kinds of nicotine pesticides in fruits by ultra performance liquid chromatography-tandem mass spectrometry coupled with cold induced liquid-liquid extraction
Full
Qiang LIN1, Yun-Kui SHEN1, Chao YANG1, Mei-Li LI1, Jia WANG1, Ding-Guo JIANG2, *, Sai FAN3, *
Affiliations
  • 1. Beijing Yanqing District Center for Disease Control and Prevention, Beijing 102100, China
  • 2. China National Center for Food Safety Risk Assessment, Beijing 100021, China
  • 3. Beijing Center for Disease Prevention and Control, Beijing Center for Preventive Medicine Research, Beijing 100013, China
Published: 2025-02-25 doi: 10.19812/j.cnki.jfsq11-5956/ts.20241219008
Outline
收藏切换

Objective To establish a detection method for 12 kinds of nicotine pesticides in fruits by ultra performance liquid chromatography-tandem mass spectrometry coupled with cold induced liquid-liquid extraction. Methods Fruit samples were extracted using acetonitrile, and after salting out, shaking, and centrifugation, they were subjected to freeze induced liquid-liquid extraction using acetonitrile water solution for further enrichment and purification. Combined with ultra performance liquid chromatography mass spectrometry, data was collected using a multi reaction monitoring mode, and quantified using isotope internal standard method. Results The linear range of 12 kinds of nicotine compounds was 1-500 ng/mL, and the method showed good linearity (r2>0.999). The limits of detection were 2.15-3.60 μg/kg, and the method limits of quantification were 7.11-13.01 μg/kg. The recovery rates of 12 kinds of nicotine compounds were 73.1%-126.7%, and the relative standard deviations were 3.5%-13.3%. Conclusion This method is easy to operate, has high precision, and good stability, and is suitable for screening and detecting nicotine like compounds in fruit samples.

ultra performance liquid chromatography-tandem mass spectrometry  /  fruits  /  nicotine pesticides
Qiang LIN, Yun-Kui SHEN, Chao YANG, Mei-Li LI, Jia WANG, Ding-Guo JIANG, Sai FAN. Simultaneous determination of 12 kinds of nicotine pesticides in fruits by ultra performance liquid chromatography-tandem mass spectrometry coupled with cold induced liquid-liquid extraction[J]. Journal of Food Safety & Quality, 2025 , 16 (4) : 71 -77 . DOI: 10.19812/j.cnki.jfsq11-5956/ts.20241219008
Appendix
Less
Year 2025 volume 16 Issue 4
PDF
273
123
Cite this Article
BibTeX
Article Info
doi: 10.19812/j.cnki.jfsq11-5956/ts.20241219008
  • Receive Date：2024-12-19
  • Online Date：2025-07-21
  • Published：2025-02-25
Article Data
Affiliations
History
  • Received：2024-12-19
Funding
Affiliations
    1. Beijing Yanqing District Center for Disease Control and Prevention, Beijing 102100, China
    2. China National Center for Food Safety Risk Assessment, Beijing 100021, China
    3. Beijing Center for Disease Prevention and Control, Beijing Center for Preventive Medicine Research, Beijing 100013, China
References
Share
https://castjournals.cast.org.cn/joweb/spaq/EN/10.19812/j.cnki.jfsq11-5956/ts.20241219008
Share to
QR

Scan QR to access full text

Cite this article
BibTeX
Citations
表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
关闭全屏
  • BibTeX
  • EndNote
  • RefWorks
  • TxT
Links
Articles
Latest Articles
Most Read
Collections
Updates
Events
News
Multimedia
About
About Us
Contact
No. 86 Xueyuan South Road, Haidian District, Beijing
100081
010-62199257
qkjq@cast.org.cn

Copyright © 2025 China Association for Science and Technology. All rights reserved. For all open access content, the relevant licensing terms apply.
Sponsored by the Office of the Leading Group for Cybersecurity and Informatization of CAST, and supported by Science and Technology Review Publishing House