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Optimization of Electrospinning Process for Preparation of BiFeO3 by Response Surface Methodology
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Yan-mei LI1, Jia-rui ZHANG1, Dai-hong KUANG1, 2, *, Rousuli AWABAIKELI2
Science Technology and Engineering | 2025, 25(2) : 862 - 870
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Science Technology and Engineering | 2025, 25(2): 862-870
Papers·Environmental and Safe Science
Optimization of Electrospinning Process for Preparation of BiFeO3 by Response Surface Methodology
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Yan-mei LI1, Jia-rui ZHANG1, Dai-hong KUANG1, 2, *, Rousuli AWABAIKELI2
Affiliations
  • 1 College of Resources and Environment, Xinjiang Agricultural University, Urumqi 830052, China
  • 2 College of Mathematics and Science, Xinjiang Agricultural University, Urumqi 830052, China
Published: 2025-01-18 doi: 10.12404/j.issn.1671-1815.2308910
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Bismuth ferrite has become an effective semiconductor photocatalyst for the degradation of various wastewaters due to its narrow band gap, high chemical stability, and good visible light response. Pure phase BiFeO3 nanofibers were prepared by electrospinning method. The optimal degradation conditions for Congo Red were obtained through single factor experiments such as calcination temperature, PVP (polyvinyl pyrrolidone)concentration, collection distance, spinning voltage, and pushing speed. Four factors that significantly affect photocatalytic efficiency were selected for response surface analysis experiments with four factors and three levels. After optimization, the optimal PVP concentration was 12.17 wt%, collection distance was 14.07 cm, and spinning voltage was 12.03 kV The pushing speed is 0.74 μm/s, and under this condition, the efficiency of BiFeO3 photocatalytic degradation of Congo red can reach 90.43%. The phase analysis and morphology characterization of bismuth ferrite nanofibers were carried out using X-ray diffraction, scanning electron microscopy, Raman spectroscopy, and Fourier transform infrared spectroscopy. The results show that the pure phase BFO nanofibers prepared by electrospinning has a rough surface and obvious particle sensation, presenting a one-dimensional rod-shaped structure with a size of about 300 nm. This nanorod-shaped structure has a larger specific surface area and more active sites, Can improve the photocatalytic degradation efficiency of BFO.

Bismuth ferrite  /  electrospinning  /  response surface analysis
Yan-mei LI, Jia-rui ZHANG, Dai-hong KUANG, Rousuli AWABAIKELI. Optimization of Electrospinning Process for Preparation of BiFeO3 by Response Surface Methodology[J]. Science Technology and Engineering, 2025 , 25 (2) : 862 -870 . DOI: 10.12404/j.issn.1671-1815.2308910
Year 2025 volume 25 Issue 2
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Article Info
doi: 10.12404/j.issn.1671-1815.2308910
  • Receive Date:2023-11-13
  • Online Date:2025-12-05
  • Published:2025-01-18
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  • Received:2023-11-13
  • Revised:2024-10-18
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    1 College of Resources and Environment, Xinjiang Agricultural University, Urumqi 830052, China
    2 College of Mathematics and Science, Xinjiang Agricultural University, Urumqi 830052, China
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表12种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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