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Detonation Synthesis of Carbon-Encapsulated Nickel Nanoparticles
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Ning LUO1, 2, Xiao-Jie LI2, Hong-Lu FEI1, Fei MO2, Cheng-Jiao ZHANG2
Chinese Journal of High Pressure Physics | 2011, 25(2) : 111 - 117
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Chinese Journal of High Pressure Physics | 2011, 25(2): 111-117
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Detonation Synthesis of Carbon-Encapsulated Nickel Nanoparticles
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Ning LUO1, 2, Xiao-Jie LI2, Hong-Lu FEI1, Fei MO2, Cheng-Jiao ZHANG2
Affiliations
  • 1.Institute of Blasting Technology, Liaoning Technical University, Fuxin 123000, China
  • 2.State Key Laboratory of Structural Analysis for Industrial Equipment, Dalian University of Technology, Dalian 116024, China

    • LUO Ning (1980-), male, doctoral candidate, major in explosion effects and synthesis of nano-materials. E-mail:

About Author:

LUO Ning (1980-), male, doctoral candidate, major in explosion effects and synthesis of nano-materials. E-mail:

Published: 2011-04-15
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Carbon-encapsulated nickel nanoparticles (CENNPs) with core-shell structure were synthesized by detonation method using homemade composite explosives with negative oxygen balance. The detonation chemical reaction was initiated by a nonel tube detonator in a closed explosion vessel filled with nitrogen gas. X-ray diffraction (XRD), X-ray fluorescence (XRF), transmission electron microscopy (TEM) with selected area electron diffraction and Raman spectrum techniques were used to characterize the as-obtained detonation products. The XRD and XRF analysis showed that the detonation products mainly consisted of the well-crystallized face-centered cubic nickel nanocrystals, carbon and other microelement. TEM showed that most nanoparticles are made up of a nickel core with the size of 10~25 nm and a carbon shell with the thickness of 1~2 nm. The Raman spectrum analysis indicated that the coating carbon shell is mainly composed of graphite and amorphous carbon. Furthermore, the possible formation mechanism for CENNPs were also discussed.

carbon-encapsulated nickel nanoparticles  /  detonation synthesis  /  X-ray diffraction  /  formation mechanism
罗宁, 李晓杰, 费鸿禄, 莫非, 张程娇. 爆轰法合成碳包覆镍纳米颗粒的研究. 高压物理学报, 2011 , 25 (2) : 111 -117 .
Ning LUO, Xiao-Jie LI, Hong-Lu FEI, Fei MO, Cheng-Jiao ZHANG. Detonation Synthesis of Carbon-Encapsulated Nickel Nanoparticles[J]. Chinese Journal of High Pressure Physics, 2011 , 25 (2) : 111 -117 .
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Funding
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  • National Natural Science Foundation of China(10872044; 10902023; 10972051)
  • National Science Foundation of Liaoning Province of China(2008161)
References
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Year 2011 volume 25 Issue 2
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Article Info
  • Receive Date：2009-11-11
  • Online Date：2026-11-02
  • Published：2011-04-15
Article Data
Affiliations
History
  • Received：2009-11-11
  • Revised：2010-01-15
Funding
National Natural Science Foundation of China(10872044; 10902023; 10972051)
National Science Foundation of Liaoning Province of China(2008161)
Affiliations
    1.Institute of Blasting Technology, Liaoning Technical University, Fuxin 123000, China
    2.State Key Laboratory of Structural Analysis for Industrial Equipment, Dalian University of Technology, Dalian 116024, China
References
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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