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Chemical Synthesis and Characterization of Flaky h-BCN by HPHT
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Da-Peng YANG, Ying-Ai LI, Yong-Hui DU, Zuo-Peng SU, Xiao-Rui JI, Xu-Xin YANG, Xi-Liang GONG, Tie-Chen ZHANG
Chinese Journal of High Pressure Physics | 2007, 21(3) : 295 - 298
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Chinese Journal of High Pressure Physics | 2007, 21(3): 295-298
Chemical Synthesis and Characterization of Flaky h-BCN by HPHT
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Da-Peng YANG, Ying-Ai LI, Yong-Hui DU, Zuo-Peng SU, Xiao-Rui JI, Xu-Xin YANG, Xi-Liang GONG, Tie-Chen ZHANG
Affiliations
  • National Laboratory of Superhard Materials, Jilin University, Changchun 130023, China
Published: 2007-09-05
Outline
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Hexagonal boron carbonitrogen (h-BCN) crystal was synthesized from the mixture of boron powder and CNH compound prepared by pyrolysis of Melamine (C3H3N3) under high temperature (1 400~1 500 ℃) and high pressure (5.0~5.5 GPa). X-ray photoelectron spectroscopy and Fourier transform infrared spectroscopy were used to determine the product chemical composition and characterization. The results show that the product has composition of B0.18C0.66N0.16(near BC4N) and atomic-level hybrid. X-ray diffraction analysis indicates that the powder has hexagonal network structure. Scanning electron microscopy result suggests that h-BCN crystal morphology are mainly hexagonal flaky and the diameter is about 1 μm, thickness 200 nm.

HTHP synthesis  /  BCN flake  /  characterization
杨大鹏, 李英爱, 杜勇慧, 苏作鹏, 吉晓瑞, 杨旭昕, 宫希亮, 张铁臣. 片状h-BCN化合物的高温高压化学合成与表征. 高压物理学报, 2007 , 21 (3) : 295 -298 .
Da-Peng YANG, Ying-Ai LI, Yong-Hui DU, Zuo-Peng SU, Xiao-Rui JI, Xu-Xin YANG, Xi-Liang GONG, Tie-Chen ZHANG. Chemical Synthesis and Characterization of Flaky h-BCN by HPHT[J]. Chinese Journal of High Pressure Physics, 2007 , 21 (3) : 295 -298 .
Year 2007 volume 21 Issue 3
20
4
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Article Info
  • Receive Date:2006-10-24
  • Online Date:2026-11-01
  • Published:2007-09-05
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  • Received:2006-10-24
  • Revised:2007-01-17
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    National Laboratory of Superhard Materials, Jilin University, Changchun 130023, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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