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A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus
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Zhong LU1, Xiao-Hong ZHAN1, Da-Hu CAO1, Liang-Ying ZHANG2, Xi YAO2
Chinese Journal of High Pressure Physics | 2008, 22(1) : 99 - 102
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Chinese Journal of High Pressure Physics | 2008, 22(1): 99-102
• Research Note •
A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus
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Zhong LU1, Xiao-Hong ZHAN1, Da-Hu CAO1, Liang-Ying ZHANG2, Xi YAO2
Affiliations
  • 1.Material Science and Engineering Department, Jiangsu Polytechnic University, Changzhou 213164, China
  • 2.Functional Materials Research Laboratory, Tongji University, Shanghai 200000, China
Published: 2008-03-05
Outline
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By a self-made system based on a cubic anvil high-pressure apparatus and an Agilent 4294A accurate impedance analyzer, real time high frequency dielectricity measurement under hydrostatic pressure is realized by the standard four-wire method widely used in ambient pressure dielectric research. The sealing of liquid cell in solid pressure-transmission medium and multi signal lines out through gaskets including four micro-coaxial cables is achieved by the pre-formation of pyrophyllite cube together with gaskets. The testing fixture, 10 mm×10 mm sample, pressure-temperature sensors and as many as 16 signal wires including 4 micro-coaxial cables with an outer diameters of 1.6 mm respectively can be contained simultaneously in a liquid testing cell with a volume of (Ø13×15) mm3. Four-wire impedance spectroscopy can be obtained by this system in a measurement range of room temperature to 300 ℃, ambient pressure to about 3 GPa hydrostatic pressure and testing frequency from 40 Hz to 5 MHz with an experiment error below 3%. The pressure induced ferroelectric-paraelectric phase transition of a BaTiO3 single crystal is observed using this setting up.

BaTiO3  /  hydrostatic pressure  /  four-wire method
陆中, 战晓红, 曹大呼, 张良莹, 姚熹. 一套基于六面顶高压装置的静水压高频介电测试系统. 高压物理学报, 2008 , 22 (1) : 99 -102 .
Zhong LU, Xiao-Hong ZHAN, Da-Hu CAO, Liang-Ying ZHANG, Xi YAO. A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus[J]. Chinese Journal of High Pressure Physics, 2008 , 22 (1) : 99 -102 .
Year 2008 volume 22 Issue 1
21
4
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Article Info
  • Receive Date:2007-02-05
  • Online Date:2026-11-01
  • Published:2008-03-05
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  • Received:2007-02-05
  • Revised:2007-05-25
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Affiliations
    1.Material Science and Engineering Department, Jiangsu Polytechnic University, Changzhou 213164, China
    2.Functional Materials Research Laboratory, Tongji University, Shanghai 200000, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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