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Effect of Oscillatory Pressure Sintering Process on Microstructure and Properties of Boron Nitride Ceramics with High Performance
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Yao HAN1, Zhipeng XIE2, Haiyan LI3, Heng DONG1, Bingqing ZHANG1
Journal of the Chinese Ceramic Society | 2021, 49(12) : 2549 - 2555
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Journal of the Chinese Ceramic Society | 2021, 49(12): 2549-2555
• Special Topic on Engineering Ceramic Material •
Effect of Oscillatory Pressure Sintering Process on Microstructure and Properties of Boron Nitride Ceramics with High Performance
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Yao HAN1, Zhipeng XIE2, Haiyan LI3, Heng DONG1, Bingqing ZHANG1
Affiliations
  • 1.Aerospace Institute of Advanced Materials & Processing Technology, Beijing 100074, China
  • 2.State Key Laboratory of New Ceramics and Fine Processing, Tsinghua University, Beijing 100084, China
  • 3.China Building Material Test & Certification Group Co., Ltd, Beijing 100024, China
Published: 2021-12-20 doi: 10.14062/j.issn.0454-5648.20210555
Outline
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High h-BN ceramics were prepared by an oscillatory pressure sintering technique (OPS), and the effect of oscillatory pressure on the sintering densification and grain growth of h-BN ceramics was investigated. Boron nitride ceramics were also prepared by a hot pressing sintering process (HP). The density, microstructure, fracture reliability, degree of grain orientation, mechanical and thermal properties of boron nitride ceramics at different sintering processes were analyzed. The results show that the fracture surface of OPS specimens is denser, and the grain orientation becomes clear, compared with those of HP specimens. A high proportion of parallel-arranged BN grains can effectively improve the densification of BN ceramics. The maximum hardness, fracture toughness and flexural strength of OPS specimens are 0.31GPa, 1.09MPa·m1/2 and 74.4MPa, respectively, which are greatly improved, compared with HP specimens at the same sintering parameters. According to the data of grain orientation determined by X-ray diffraction patterns, the application of oscillatory pressure obviously promotes the densification and sintering of boron nitride ceramics, thus improving the fracture reliability and thermal conductivity.

boron nitride  /  oscillatory pressure sintering  /  mechanical properties  /  thermal conductivity  /  microstructure
韩耀, 谢志鹏, 李海燕, 董衡, 张冰清. 新型振荡压力烧结工艺对高性能氮化硼陶瓷微观结构和性能的影响. 硅酸盐学报, 2021 , 49 (12) : 2549 -2555 . DOI: 10.14062/j.issn.0454-5648.20210555
Yao HAN, Zhipeng XIE, Haiyan LI, Heng DONG, Bingqing ZHANG. Effect of Oscillatory Pressure Sintering Process on Microstructure and Properties of Boron Nitride Ceramics with High Performance[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (12) : 2549 -2555 . DOI: 10.14062/j.issn.0454-5648.20210555
Year 2021 volume 49 Issue 12
40
9
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Article Info
doi: 10.14062/j.issn.0454-5648.20210555
  • Receive Date:2021-07-08
  • Online Date:2026-10-30
  • Published:2021-12-20
Article Data
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History
  • Received:2021-07-08
  • Revised:2021-08-14
Funding
Affiliations
    1.Aerospace Institute of Advanced Materials & Processing Technology, Beijing 100074, China
    2.State Key Laboratory of New Ceramics and Fine Processing, Tsinghua University, Beijing 100084, China
    3.China Building Material Test & Certification Group Co., Ltd, Beijing 100024, China

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HAN Yao (1990-), male, Ph.D, Senior Engineer. E-mail:
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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