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Preparation of C/ZrSiO4 Black Pigment with Phenolic Resin Spheres as a Colorant
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Shanfang LAN1, Qing HU1, Weihui JIANG1, 2, Qianqian ZHAO1, Huidong TANG1, Jianmin LIU2, Fen JIANG1, Guo FENG2
Journal of the Chinese Ceramic Society | 2020, 48(12) : 1927 - 1934
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Journal of the Chinese Ceramic Society | 2020, 48(12): 1927-1934
Preparation of C/ZrSiO4 Black Pigment with Phenolic Resin Spheres as a Colorant
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Shanfang LAN1, Qing HU1, Weihui JIANG1, 2, Qianqian ZHAO1, Huidong TANG1, Jianmin LIU2, Fen JIANG1, Guo FENG2
Affiliations
  • 1.School of Material Science and Engineering, Jingdezhen Ceramic Institute, Jingdezhen 333403, Jiangxi, China
  • 2.National Engineering Research Center for Domestic and Building Ceramics, Jingdezhen 333001, Jiangxi, China

    • LAN Shanfang (1994—), male, Master candidate. E-mail:

About Author:

LAN Shanfang (1994—), male, Master candidate. E-mail:

Published: 2020-12-20 doi: 10.14062/j.issn.0454-5648.20200145
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A black pigment of C/ZrSiO4 was prepared by a non-hydrolytic sol gel method with zirconium tetrachloride, tetraethyl orthosilicate and phenolic resin spheres prepared by the Stöber method as zirconium, silicon and carbon sources, respectively. The morphology, structure and residual carbon rate of the phenolic resin spheres were characterized by scanning electron microscopy, energy disperse spectroscopy, X-ray diffraction, Fourier transform infrared spectroscopy and differential thermal analysis-thermogravimetry. The effects of phenolic resin spheres amount and calcination temperature on the synthesis and color properties of C/ZrSiO4 pigments were also investigated. The results show that the obtained phenolic resin spheres are well-dispersive and the average diameter is 550 nm, and they possess oxygen-containing functional groups on their surfaces and achieve a high residual carbon rate of 48.63%. The L* value of prepared C/ZrSiO4 pigment firstly decreases and then increases with increasing the amount of phenolic resin spheres. When the amount of the phenolic resin spheres is 2% (in mass fraction) and the calcining temperature is 900 ℃, C/ZrSiO4 pigment with a good color performance (L*=39.76, a*=0.53, b*=2.21) can be obtained. Moreover, the colored glaze samples present a good color rendering performance when applying C/ZrSiO4 pigment in ceramic glaze calcined at 1 200 ℃. It is indicated that C/ZrSiO4 pigment could have a promising application in coating, ceramic and glass decoration.

phenolic resin spheres  /  zirconium silicate  /  black pigments  /  non-hydrolyzed sol-gel method
蓝善芳, 胡庆, 江伟辉, 赵迁迁, 汤惠东, 刘健敏, 江峰, 冯果. 酚醛树脂球为碳源制备C/ZrSiO4黑色色料. 硅酸盐学报, 2020 , 48 (12) : 1927 -1934 . DOI: 10.14062/j.issn.0454-5648.20200145
Shanfang LAN, Qing HU, Weihui JIANG, Qianqian ZHAO, Huidong TANG, Jianmin LIU, Fen JIANG, Guo FENG. Preparation of C/ZrSiO4 Black Pigment with Phenolic Resin Spheres as a Colorant[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (12) : 1927 -1934 . DOI: 10.14062/j.issn.0454-5648.20200145
Appendix
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Year 2020 volume 48 Issue 12
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Article Info
doi: 10.14062/j.issn.0454-5648.20200145
  • Receive Date：2020-03-06
  • Online Date：2026-10-30
  • Published：2020-12-20
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History
  • Received：2020-03-06
  • Revised：2020-04-10
Funding
Affiliations
    1.School of Material Science and Engineering, Jingdezhen Ceramic Institute, Jingdezhen 333403, Jiangxi, China
    2.National Engineering Research Center for Domestic and Building Ceramics, Jingdezhen 333001, Jiangxi, China

Corresponding:

JIANG Weihui (1965—), male, Ph.D., Professor. E-mail:
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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