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Effect of Molten Salt on Preparation of Zirconia Nanosheets
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Xuefeng LIU1, Jianmin LIU2, Yage LI1, Zijuan TANG1, Tao WANG1, Guo FENG2, Weihui JIANG1, 2
Journal of the Chinese Ceramic Society | 2020, 48(4) : 514 - 519
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Journal of the Chinese Ceramic Society | 2020, 48(4): 514-519
Effect of Molten Salt on Preparation of Zirconia Nanosheets
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Xuefeng LIU1, Jianmin LIU2, Yage LI1, Zijuan TANG1, Tao WANG1, Guo FENG2, Weihui JIANG1, 2
Affiliations
  • 1.School of Material Science and Engineering, Jingdezhen Ceramic Institute, Jingdezhen 333403, Jiangxi, China
  • 2.National Engineering Research Center for Domestic and Building Ceramics, Jingdezhen 333001, Jiangxi, China

    • LIU Xuefeng (1992-), male, Master candidate. E-mail:

About Author:

LIU Xuefeng (1992-), male, Master candidate. E-mail:

Published: 2020-04-20 doi: 10.14062/j.issn.0454-5648.20190691
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ZrO2 nanosheets were prepared at low temperature by a molten salt method with assistance of solvothermal process using zirconium chloride as zirconium source and ethanol as a solvent. The effects of salt type and content on the growth and morphology of zirconia crystals were investigated. The results show that monoclinic zirconia nanosheets with an average side length of 1.8 μm, a thickness of 70 nm and a width: thickness ratio of more than 10∶1 can be obtained when NaCl and Na3PO4 are used as composite molten salts and the mass ratio of precursor∶NaCl∶Na3PO4 is set to 10∶10∶1. The nanosheet shows single crystal structure with little defects, and the main exposed surface is (001) facet. The formation process in molten salts accords with a self-focusing mechanism, including dissolution, diffusion, adsorption and growth. The large percentage of (001) facet obtained is in reasonable agreement with that based on the theoretical calculation of surface energy.

molten salt method  /  zirconium dioxide nanosheet  /  (001) facet  /  self-focusing
刘雪枫, 刘健敏, 李亚格, 唐紫娟, 王涛, 冯果, 江伟辉. 熔融盐对氧化锆纳米片合成的影响. 硅酸盐学报, 2020 , 48 (4) : 514 -519 . DOI: 10.14062/j.issn.0454-5648.20190691
Xuefeng LIU, Jianmin LIU, Yage LI, Zijuan TANG, Tao WANG, Guo FENG, Weihui JIANG. Effect of Molten Salt on Preparation of Zirconia Nanosheets[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (4) : 514 -519 . DOI: 10.14062/j.issn.0454-5648.20190691
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Year 2020 volume 48 Issue 4
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Article Info
doi: 10.14062/j.issn.0454-5648.20190691
  • Receive Date：2019-10-20
  • Online Date：2026-10-29
  • Published：2020-04-20
Article Data
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History
  • Received：2019-10-20
  • Revised：2019-11-08
Funding
Affiliations
    1.School of Material Science and Engineering, Jingdezhen Ceramic Institute, Jingdezhen 333403, Jiangxi, China
    2.National Engineering Research Center for Domestic and Building Ceramics, Jingdezhen 333001, Jiangxi, China

Corresponding:

JIANG Weihui (1965-), male, Ph.D., Professor. E-mail:
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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