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High-Temperature Quenching Synthesis and Electrochemical Properties of Na11Sn2PS12 Solid Electrolytes
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Wei WENG1, 2, Hongli WAN1, Gaozhan LIU1, Lin SHEN1, 2, Xiayin YAO1, 2
Journal of the Chinese Ceramic Society | 2022, 50(1) : 55 - 61
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Journal of the Chinese Ceramic Society | 2022, 50(1): 55-61
• Research Articles •
High-Temperature Quenching Synthesis and Electrochemical Properties of Na11Sn2PS12 Solid Electrolytes
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Wei WENG1, 2, Hongli WAN1, Gaozhan LIU1, Lin SHEN1, 2, Xiayin YAO1, 2
Affiliations
  • 1.Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, Zhejiang, China
  • 2.Center of Materials Science and Optoelectronics Engineering, University of Chinese Academy of Sciences, Beijing 100049, China

    • WENG Wei (1994-), male, Doctoral candidate. E-mail:

About Author:

WENG Wei (1994-), male, Doctoral candidate. E-mail:

Published: 2022-01-20 doi: 10.14062/j.issn.0454-5648.20210566
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Na11Sn2PS12 solid electrolytes were synthesized by a high-temperature quenching method, and the structures as well as electrochemical performance were investigated. A Na11Sn2PS12 phase with a certain amount of impurity can be obtained in quenching process. The content of impurity phase in the quenching precursors annealed at 430 ℃ decreases and the room-temperature ionic conductivity enhances from 0.34×10-4 S/cm to 6.26×10-4 S/cm. In addition, a prepared Na11Sn2PS12 possesses a low activation energy of 0.27 eV and an electronic conductivity of 2.25×10-8 S/cm, and an electrochemistry stability window between 0.8 V and 2.8 V. Also, Na11Sn2PS12 is used in all-solid-state sodium batteries, showing good electrochemical performances.

sulfide solid electrolytes  /  quaternary sodium ionic conductor  /  high temperature quenching synthesis  /  all-solid-state sodium batteries
翁伟, 万红利, 刘高瞻, 沈麟, 姚霞银. 高温淬火制备Na11Sn2PS12固体电解质及其电化学性能. 硅酸盐学报, 2022 , 50 (1) : 55 -61 . DOI: 10.14062/j.issn.0454-5648.20210566
Wei WENG, Hongli WAN, Gaozhan LIU, Lin SHEN, Xiayin YAO. High-Temperature Quenching Synthesis and Electrochemical Properties of Na11Sn2PS12 Solid Electrolytes[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (1) : 55 -61 . DOI: 10.14062/j.issn.0454-5648.20210566
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Year 2022 volume 50 Issue 1
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doi: 10.14062/j.issn.0454-5648.20210566
  • Receive Date：2021-07-12
  • Online Date：2026-10-22
  • Published：2022-01-20
Article Data
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History
  • Received：2021-07-12
  • Revised：2021-08-20
Funding
Affiliations
    1.Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, Zhejiang, China
    2.Center of Materials Science and Optoelectronics Engineering, University of Chinese Academy of Sciences, Beijing 100049, China

Corresponding:

YAO Xiayin (1982-), male, Ph.D., Professor. E-mail:
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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