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Optimisation of Ammonium Sulphate Crystallization Based on Response Surface Methodology
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Rui LI1, Yonghua JIANG1, Yanling ZHANG1, Kunqing CHEN1, Bangfu HUANG2, Lu LI2
Journal of the Chinese Ceramic Society | 2022, 50(3) : 782 - 790
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Journal of the Chinese Ceramic Society | 2022, 50(3): 782-790
• Research Articles •
Optimisation of Ammonium Sulphate Crystallization Based on Response Surface Methodology
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Rui LI1, Yonghua JIANG1, Yanling ZHANG1, Kunqing CHEN1, Bangfu HUANG2, Lu LI2
Affiliations
  • 1.Yunnan Tianlang Energy Saving & Environmental Protection Group Co., Ltd., Anning 650302, Yunnan, China
  • 2.Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China
  • LI Rui (1973-), male, Undergraduate, Senior Engineer. E-mail:

About Author:

LI Rui (1973-), male, Undergraduate, Senior Engineer. E-mail:

Published: 2022-03-20 doi: 10.14062/j.issn.0454-5648.20210478
Outline
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The influences of pH value, Fe3+ mass concentration, and stirring rate and their interactions on the ammonium sulfate crystallization were investigated via cooling crystallization and sieving based on a response surface methodology. An average particle size quadratic orthogonal model and a variation coefficient 2FI orthogonal model were proposed. The interactions among the various factors were analyzed. The results show that pH value (A) > stirring rate (C) > Fe3+ ions concentration (B) is a decreased order for the parameter effects on the average particle size and variation coefficient. Their interactions have a decreased effect order (i.e., AC >BC > AB) on the average particle size and variation coefficient. When pH value is 5.5, stirring rate is 150 r/min, and Fe3+ ions concentration is 0.3 g/L, the average particle size and variation coefficient of the ideal crystals is 0.985 mm and 793.719, respectively.

response surface methodology  /  pH value  /  ferric ions concentration  /  stirring rate  /  ammonium sulfate  /  crystallization  /  interaction
李锐, 姜永华, 张燕玲, 陈昆庆, 黄帮福, 李露. 基于响应曲面法优化硫酸铵结晶. 硅酸盐学报, 2022 , 50 (3) : 782 -790 . DOI: 10.14062/j.issn.0454-5648.20210478
Rui LI, Yonghua JIANG, Yanling ZHANG, Kunqing CHEN, Bangfu HUANG, Lu LI. Optimisation of Ammonium Sulphate Crystallization Based on Response Surface Methodology[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (3) : 782 -790 . DOI: 10.14062/j.issn.0454-5648.20210478
Year 2022 volume 50 Issue 3
15
1
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Article Info
doi: 10.14062/j.issn.0454-5648.20210478
  • Receive Date:2021-06-11
  • Online Date:2026-10-22
  • Published:2022-03-20
Article Data
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History
  • Received:2021-06-11
  • Revised:2021-07-28
Funding
Affiliations
    1.Yunnan Tianlang Energy Saving & Environmental Protection Group Co., Ltd., Anning 650302, Yunnan, China
    2.Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093, China

Corresponding:

Huang Bangfu (1983-), male, Ph.D., Associate Professor. E-mail:
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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