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Preparation and Luminescent Properties of ZnS∶Mn Nanocrystals Embedded Glass
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Jiancheng WANG1, Beiying ZHOU2, 3, Peng YANG1, Yuye ZHAO1, Lianjun WANG1, 2, Wan JIANG2, 3
Journal of the Chinese Ceramic Society | 2022, 50(4) : 983 - 990
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Journal of the Chinese Ceramic Society | 2022, 50(4): 983-990
• Research Articles •
Preparation and Luminescent Properties of ZnS∶Mn Nanocrystals Embedded Glass
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Jiancheng WANG1, Beiying ZHOU2, 3, Peng YANG1, Yuye ZHAO1, Lianjun WANG1, 2, Wan JIANG2, 3
Affiliations
  • 1.State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, College of Materials Science and Engineering, Donghua University, Shanghai 201620, China
  • 2.Institute of Functional Materials, Donghua University, Shanghai 201620, China
  • 3.Engineering Research Center of Advanced Glasses Manufacturing Technology, Ministry of Education, Donghua University, Shanghai 201620, China

    • WANG Jiancheng (1993-), male, Doctoral candidate. E-mail:

About Author:

WANG Jiancheng (1993-), male, Doctoral candidate. E-mail:

Published: 2022-04-20 doi: 10.14062/j.issn.0454-5648.20211009
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ZnS:Mn nanocrystals embedded glass has attracted much attention due to the excellent luminescence performance in reddish orange range, high stability and non-toxicity. However, high temperature and long annealing time needed in a conventional melt-quenching method readily cause the volatilization, invalidation and agglomeration of nanocrystals, greatly reducing the luminescence performance. In this paper, ZnS∶Mn nanocrystals embedded glass was prepared via spark plasma sintering (SPS) at 980℃ for 10 min, and the samples were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, electron spin resonance, photoluminescence and fluorescence lifetime analysis. The results show that rapidly sintering at a low temperature is beneficial to avoiding the oxidation of Mn2+ and driving Mn2+ into the ZnS lattice to realize the effective doping. Also, the generation of defect-related luminescence is suppressed by regulating the composition of ZnS nanocrystals, thereby further enhancing the Mn2+ transition luminescence. The ion-doped nanocrystals embedded glass prepared by SPS with the superior performance can be used as a promising solid light convertor in high-power LED devices.

nanocrystals  /  nanocrystals embedded glass  /  luminescence properties  /  fluorescence
王建成, 周蓓莹, 杨蓬, 赵玉叶, 王连军, 江莞. ZnS∶Mn纳米晶复合玻璃的制备与光学性能. 硅酸盐学报, 2022 , 50 (4) : 983 -990 . DOI: 10.14062/j.issn.0454-5648.20211009
Jiancheng WANG, Beiying ZHOU, Peng YANG, Yuye ZHAO, Lianjun WANG, Wan JIANG. Preparation and Luminescent Properties of ZnS∶Mn Nanocrystals Embedded Glass[J]. Journal of the Chinese Ceramic Society, 2022 , 50 (4) : 983 -990 . DOI: 10.14062/j.issn.0454-5648.20211009
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Year 2022 volume 50 Issue 4
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Article Info
doi: 10.14062/j.issn.0454-5648.20211009
  • Receive Date：2021-12-27
  • Online Date：2026-10-22
  • Published：2022-04-20
Article Data
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History
  • Received：2021-12-27
  • Revised：2022-01-25
Funding
Affiliations
    1.State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, College of Materials Science and Engineering, Donghua University, Shanghai 201620, China
    2.Institute of Functional Materials, Donghua University, Shanghai 201620, China
    3.Engineering Research Center of Advanced Glasses Manufacturing Technology, Ministry of Education, Donghua University, Shanghai 201620, China

Corresponding:

ZHOU Beiying (1990-), female, Ph.D., Assistant Professor. E-mail:
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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