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Controllable Preparation and Decorative Effect of Iron-based Crystalline Glazes
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Mei LI1, 2, 3, Weidong LI1, 3, Xiaoke LU1, 3, Changsong XU1, 3
Journal of the Chinese Ceramic Society | 2020, 48(7) : 1134 - 1144
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Journal of the Chinese Ceramic Society | 2020, 48(7): 1134-1144
• Research Articles •
Controllable Preparation and Decorative Effect of Iron-based Crystalline Glazes
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Mei LI1, 2, 3, Weidong LI1, 3, Xiaoke LU1, 3, Changsong XU1, 3
Affiliations
  • 1.Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
  • 2.University of Chinese Academy of Sciences, Beijing 100049, China
  • 3.Key Scientific Research Base of Ancient Ceramics, State Administration for Cultural Heritage, Shanghai 200050, China

    • LI Mei(1995-), female, Master candidate. E-mail:

About Author:

LI Mei(1995-), female, Master candidate. E-mail:

Published: 2020-07-20 doi: 10.14062/j.issn.0454-5648.2020.07.20190684
Outline
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Based on the study of ancient black glazed porcelains, high-fired glazes of SiO2-Al2O3-K2O-MgO-CaO-Fe2O3 system were designed and prepared. Different glaze decoration effects were achieved by changing the firing schedules to modify the crystallization behavior and microstructure of the glazes. The influence of thermal history on the crystal attribute and morphology, glaze appearance and coloring mechanism was investigated by using optical microscopy, field emission scanning electron microscopy, electron backscattered diffraction, X-ray diffraction and Raman spectroscopy, respectively. ε-Fe2O3 crystalline layer was prepared in a slight oxidation atmosphere at about 1 000-1 050 ℃. The results show that α-Fe2O3 crystals precipitated on the glaze surface have a good orientation and a variety of morphologies, which are related to the crystallization position and the direction of the crystallization plane. α-Fe2O3 crystals on the glaze surface show a silvery metallic luster, which belongs to a physical structural color.

crystalline glaze  /  firing schedule  /  crystallization  /  ε-iron oxide  /  α-iron oxide  /  structural color
李玫, 李伟东, 鲁晓珂, 徐嫦松. 铁系结晶釉的可控制备与装饰效果. 硅酸盐学报, 2020 , 48 (7) : 1134 -1144 . DOI: 10.14062/j.issn.0454-5648.2020.07.20190684
Mei LI, Weidong LI, Xiaoke LU, Changsong XU. Controllable Preparation and Decorative Effect of Iron-based Crystalline Glazes[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (7) : 1134 -1144 . DOI: 10.14062/j.issn.0454-5648.2020.07.20190684
Appendix
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Year 2020 volume 48 Issue 7
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Article Info
doi: 10.14062/j.issn.0454-5648.2020.07.20190684
  • Receive Date：2019-10-15
  • Online Date：2026-10-29
  • Published：2020-07-20
Article Data
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History
  • Received：2019-10-15
  • Revised：2019-12-09
Funding
Affiliations
    1.Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
    2.University of Chinese Academy of Sciences, Beijing 100049, China
    3.Key Scientific Research Base of Ancient Ceramics, State Administration for Cultural Heritage, Shanghai 200050, China

Corresponding:

LI Weidong(1966-), female, Ph.D., Professor. E-mail:
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Citations
表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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