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Determine Silicon Carbide in Warming Agent with Acid Dissolution-Combustion Gas Volumetric Method
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Yan-rong Lu, Su-lan Zhang, Chun-ling Zhou
Rare Earth Steel | 2018, 44(5) : 75 - 78
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Rare Earth Steel | 2018, 44(5): 75-78
• Quality of Variety and Experiment and Research •
Determine Silicon Carbide in Warming Agent with Acid Dissolution-Combustion Gas Volumetric Method
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Yan-rong Lu, Su-lan Zhang, Chun-ling Zhou
Affiliations
  • Technical Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
Published: 2018-10-25 doi: 10.13647/j.cnki.btgkj.2018.05.021
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In the paper, it is introduced the content of silicon carbide in warming agent was determined with the combustion gas volumetric method by burning the sample at about 800 ℃ to remove the free carbon, dissolving carbonate with acid, filtration and washing. The determination conditions such as the temperatures of starting decomposition and complete decomposition for silicon carbide, preheating time and selection of sample weights are discussed as well as the optimum working conditions are found out. The measurement range of content of silicon carbide with this method was 1.00%~45.00%. 11 times of determination were carried out with 4 types of warming agent samples and the relative standard deviation (RSD) were 0.952%, 0.446%, 0.590% and 0.490% respectively. Compared with other methods, the results were the same.

combustion gas volumetric method  /  warming agent  /  silicon carbide  /  decomposition temperature  /  determine
卢艳蓉, 张素兰, 周春玲. 酸溶-燃烧气体容量法测定提温剂中碳化硅. 包钢科技, 2018 , 44 (5) : 75 -78 . DOI: 10.13647/j.cnki.btgkj.2018.05.021
Yan-rong Lu, Su-lan Zhang, Chun-ling Zhou. Determine Silicon Carbide in Warming Agent with Acid Dissolution-Combustion Gas Volumetric Method[J]. Science & Technology of Baotou Steel, 2018 , 44 (5) : 75 -78 . DOI: 10.13647/j.cnki.btgkj.2018.05.021
Year 2018 volume 44 Issue 5
44
8
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doi: 10.13647/j.cnki.btgkj.2018.05.021
  • Receive Date:2018-01-12
  • Online Date:2026-10-20
  • Published:2018-10-25
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  • Received:2018-01-12
Affiliations
    Technical Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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