After microwave digestion, Pb+2 in the sample was oxidized to Pb+4 by potassium ferricyanide. In the carrying current solution of hydrochloric acid (5+95), potassium borohydride was used as reducing agent and with the characteristics that gaseous hydrides can be produced by the reaction lead and potassium borohydride. The method of hydride generation-atomic fluorescence spectrometry for determining lead in iron containing dust was established. The detection limit of lead in iron containing dust was 0.091 9 μg/L, the upper limit was 0.5%, the relative standard deviation of iron ore standard sample and iron containing dust sample (n = 11) was less than 5.0%, and the standard recovery rate was 97%~104%. The method is fast and simple, which can be used for determining lead in iron containing dust.
| 科 Family | 属数 Number of genus | 种数 Number of species | 占总种数比例 Percentage of total species (%) | 属 Genus | 种数 Number of species | 占总种数比例 Percentage of total species (%) |
|---|---|---|---|---|---|---|
| 鹅膏菌科Amanitaceae | 2 | 11 | 5.26 | 鹅膏菌属 Amanita | 10 | 4.78 |
| 小菇科 Mycenaceae | 2 | 12 | 5.74 | 丝盖伞属 Inocybe | 5 | 2.39 |
| 多孔菌科 Polyporaceae | 8 | 14 | 6.70 | 蜡蘑属 Laccaria | 5 | 2.39 |
| 红菇科 Russulaceae | 3 | 23 | 11.00 | 小皮伞属 Marasmius | 6 | 2.87 |
| 小菇属 Mycena | 11 | 5.26 | ||||
| 光柄菇属 Pluteus | 5 | 2.39 | ||||
| 红菇属 Russula | 17 | 8.13 | ||||
| 栓菌属 Trametes | 5 | 2.39 |