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Determination of Lead in Iron-containing Dust by Microwave Digestion Atomic Fluorescence Spectrometry
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Yan-rong Lu, Su-lan Zhang
Rare Earth Steel | 2018, 44(3) : 63 - 66
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Rare Earth Steel | 2018, 44(3): 63-66
• Quality of Variety and Experiment and Research •
Determination of Lead in Iron-containing Dust by Microwave Digestion Atomic Fluorescence Spectrometry
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Yan-rong Lu, Su-lan Zhang
Affiliations
  • Technical Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
Published: 2018-06-25 doi: 10.13647/j.cnki.btgkj.2018.03.016
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After microwave digestion, Pb+2 in the sample was oxidized to Pb+4 by potassium ferricyanide. In the carrying current solution of hydrochloric acid (5+95), potassium borohydride was used as reducing agent and with the characteristics that gaseous hydrides can be produced by the reaction lead and potassium borohydride. The method of hydride generation-atomic fluorescence spectrometry for determining lead in iron containing dust was established. The detection limit of lead in iron containing dust was 0.091 9 μg/L, the upper limit was 0.5%, the relative standard deviation of iron ore standard sample and iron containing dust sample (n = 11) was less than 5.0%, and the standard recovery rate was 97%~104%. The method is fast and simple, which can be used for determining lead in iron containing dust.

microwave digestion  /  hydride generation-atomic fluorescence spectrometry  /  iron containing dust  /  lead
卢艳蓉, 张素兰. 微波消解原子荧光光谱法测定含铁尘泥中铅. 包钢科技, 2018 , 44 (3) : 63 -66 . DOI: 10.13647/j.cnki.btgkj.2018.03.016
Yan-rong Lu, Su-lan Zhang. Determination of Lead in Iron-containing Dust by Microwave Digestion Atomic Fluorescence Spectrometry[J]. Science & Technology of Baotou Steel, 2018 , 44 (3) : 63 -66 . DOI: 10.13647/j.cnki.btgkj.2018.03.016
Year 2018 volume 44 Issue 3
45
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doi: 10.13647/j.cnki.btgkj.2018.03.016
  • Receive Date:2018-01-04
  • Online Date:2026-10-20
  • Published:2018-06-25
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  • Received:2018-01-04
Affiliations
    Technical Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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