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Rapid Determination of Chloride Ion Content in Organic Amine
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Jian-ping Xue, Ye-jian Du, Er-feng Sun, Li-xia Hu, Li-xia Zhou, Na Wu
Rare Earth Steel | 2021, 47(1) : 91 - 94
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Rare Earth Steel | 2021, 47(1): 91-94
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Rapid Determination of Chloride Ion Content in Organic Amine
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Jian-ping Xue, Ye-jian Du, Er-feng Sun, Li-xia Hu, Li-xia Zhou, Na Wu
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  • Baotou Huamei Rare Earth High-tech Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
Published: 2021-02-25 doi: 10.13647/j.cnki.btgkj.2021.01.027
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In this experiment, the mercuric thiocyanate ethanol solution is as color-substrate solution and the chlorine ion content in organic amine is determined with spectrophotometry at the wave length of 460 nm. Such conditions as the amount of chromogenic agent, chromogenic time and amount of acid added are optimized by the experiment as well as the elimination test of interfering ion is carried out. The detection limit of this method is 0.034 2 μg/mL, adding standard recovery is 93.10%~104.60% and RSD≤1.75%. The method is fast, accurate as well as with high sensitivity and precision, which is suitable for determining the chloride ion content in organic amine.

organic amine  /  chloride ion  /  accompanying ion  /  spectrophotometry
薛建萍, 都业俭, 孙二凤, 胡丽霞, 周丽霞, 吴娜. 快速测定有机胺中氯离子含量. 包钢科技, 2021 , 47 (1) : 91 -94 . DOI: 10.13647/j.cnki.btgkj.2021.01.027
Jian-ping Xue, Ye-jian Du, Er-feng Sun, Li-xia Hu, Li-xia Zhou, Na Wu. Rapid Determination of Chloride Ion Content in Organic Amine[J]. Science & Technology of Baotou Steel, 2021 , 47 (1) : 91 -94 . DOI: 10.13647/j.cnki.btgkj.2021.01.027
Year 2021 volume 47 Issue 1
71
8
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doi: 10.13647/j.cnki.btgkj.2021.01.027
  • Receive Date:2020-09-11
  • Online Date:2026-10-20
  • Published:2021-02-25
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  • Received:2020-09-11
Affiliations
    Baotou Huamei Rare Earth High-tech Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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