Article(id=1261728983180296282, tenantId=1146029695717560320, journalId=1146119944283992078, issueId=1261728796072358112, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1778749231380, onlineDateStr=2026-05-14, pubDate=1774195200000, pubDateStr=2026-03-23, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1778749231380, onlineIssueDateStr=2026-05-14, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1778749231380, creator=13701087609, updateTime=1778749231380, updator=13701087609, issue=Issue{id=1261728796072358112, tenantId=1146029695717560320, journalId=1146119944283992078, year='2026', volume='4', issue='6', pageStart='1', pageEnd='234', issueExtLink='null', onlineDate='null', pubDate='1774195200000', pubDateStr='2026-03-23', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1778749186771, creator='13701087609', updateTime=1778750183088, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1261732975067148479, tenantId=1146029695717560320, journalId=1146119944283992078, issueId=1261728796072358112, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1261732975071342784, tenantId=1146029695717560320, journalId=1146119944283992078, issueId=1261728796072358112, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=223, endPage=227, ext={CN=ArticleExt(id=1261728988205072516, articleId=1261728983180296282, tenantId=1146029695717560320, journalId=1146119944283992078, language=CN, title=高效液相色谱法测定藜芦制剂中白藜芦醇、藜芦托素、藜芦胺含量, columnId=1261728976733594600, journalTitle=实验室检测, columnName=分析与检测, runingTitle=null, highlight=null, articleAbstract=
目的 采用高效液相色谱法建立一种同时测定藜芦制剂中白藜芦醇、藜芦托素、藜芦胺含量的分析方法。
方法 采用高效液相色谱仪,InertSustain C18色谱柱(250 mm×4.6 mm,5 μm),以乙腈/0.1 mol/L乙酸铵水溶液为流动相梯度洗脱,在波长225 nm下,对制剂中白藜芦醇、藜芦托素、藜芦胺有效成分进行分离和定量分析。
结果 白藜芦醇、藜芦托素、藜芦胺线性相关系数分别为0.9998、0.9992和0.9984,标准偏差分别为0.00026%、0.00238%和0.00202%,平均回收率分别为100.16%、102.74%和99.55%。
结论 建立的方法线性关系良好、精密度好、准确度高,可用于藜芦制剂的检测。
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