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目的

建立小儿化积颗粒中山楂、牵牛子、槟榔的质量控制方法。

方法

采用薄层色谱法(thin-layer chromatography, TLC)定性鉴别山楂、牵牛子、槟榔,优化展开剂及供试品制备条件;通过高效液相色谱法(high performance liquid chromatography, HPLC)测定熊果酸、牵牛子苷和槟榔碱,考察色谱条件、线性关系、精密度及稳定性。

结果

TLC结果显示山楂、牵牛子、槟榔特征斑点明显,阴性无干扰。HPLC测定表明:熊果酸(0.5~20.0 μg/mL,r=0.9998)、牵牛子苷(1.0~40.0 μg/mL,r=0.9999)、槟榔碱(0.2~8.0 μg/mL,r=0.9997)线性关系良好。精密度相对标准偏差(relative standard deviation, RSD)≤1.2%,24 h稳定性RSD≤1.8%,3批样品含量稳定。

结论

所建立的TLC和HPLC方法专属性强、准确性高,适用于小儿化积颗粒的质量控制。

, correspAuthors=王伟, authorNote=null, correspAuthorsNote=

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王伟,制药工程师,主要研究方向为药品质量控制与检测技术研究。E-mail
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刘萍,高级工程师,主要研究方向为药品质量控制与检测技术研究。E-mail

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小儿化积颗粒中山楂、牵牛子、槟榔的质量标准研究
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刘萍 , 吴多富 , 王伟 *
实验室检测 | 创新应用 2026,4(6): 77-80
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实验室检测 | 创新应用 2026, 4(6): 77-80
小儿化积颗粒中山楂、牵牛子、槟榔的质量标准研究
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刘萍 , 吴多富, 王伟*
作者信息
  • 海南葫芦娃药业集团股份有限公司,海口 570312
  • 刘萍,高级工程师,主要研究方向为药品质量控制与检测技术研究。E-mail

通讯作者:

*

王伟,制药工程师,主要研究方向为药品质量控制与检测技术研究。E-mail
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出版时间: 2026-03-23
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目的

建立小儿化积颗粒中山楂、牵牛子、槟榔的质量控制方法。

方法

采用薄层色谱法(thin-layer chromatography, TLC)定性鉴别山楂、牵牛子、槟榔,优化展开剂及供试品制备条件;通过高效液相色谱法(high performance liquid chromatography, HPLC)测定熊果酸、牵牛子苷和槟榔碱,考察色谱条件、线性关系、精密度及稳定性。

结果

TLC结果显示山楂、牵牛子、槟榔特征斑点明显,阴性无干扰。HPLC测定表明:熊果酸(0.5~20.0 μg/mL,r=0.9998)、牵牛子苷(1.0~40.0 μg/mL,r=0.9999)、槟榔碱(0.2~8.0 μg/mL,r=0.9997)线性关系良好。精密度相对标准偏差(relative standard deviation, RSD)≤1.2%,24 h稳定性RSD≤1.8%,3批样品含量稳定。

结论

所建立的TLC和HPLC方法专属性强、准确性高,适用于小儿化积颗粒的质量控制。

小儿化积颗粒  /  山楂  /  牵牛子  /  槟榔  /  质量标准  /  薄层色谱法  /  高效液相色谱法
刘萍, 吴多富, 王伟. 小儿化积颗粒中山楂、牵牛子、槟榔的质量标准研究. 实验室检测, 2026 , 4 (6) : 77 -80 .
2026年第4卷第6期
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  • 首发时间:2026-05-14
  • 出版时间:2026-03-23
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    海南葫芦娃药业集团股份有限公司,海口 570312

通讯作者:

*

王伟,制药工程师,主要研究方向为药品质量控制与检测技术研究。E-mail
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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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