Article(id=1152996333897110335, tenantId=1146029695717560320, journalId=1146119944283992078, issueId=1152996332307473145, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1752825347637, onlineDateStr=2025-07-18, pubDate=1738944000000, pubDateStr=2025-02-08, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1752825347637, onlineIssueDateStr=2025-07-18, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1752825347637, creator=13701087609, updateTime=1752825347637, updator=13701087609, issue=Issue{id=1152996332307473145, tenantId=1146029695717560320, journalId=1146119944283992078, year='2025', volume='3', issue='3', pageStart='1', pageEnd='162', issueExtLink='null', onlineDate='null', pubDate='1738944000000', pubDateStr='2025-02-08', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1752825347258, creator='13701087609', updateTime=1753700656126, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1156667643827446407, tenantId=1146029695717560320, journalId=1146119944283992078, issueId=1152996332307473145, language=EN, specialIssueTitle=, coverIllustrator=, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1156667643827446408, tenantId=1146029695717560320, journalId=1146119944283992078, issueId=1152996332307473145, language=CN, specialIssueTitle=, coverIllustrator=, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=12, endPage=16, ext={CN=ArticleExt(id=1152996334387843906, articleId=1152996333897110335, tenantId=1146029695717560320, journalId=1146119944283992078, language=CN, title=电感耦合等离子体发射光谱仪测定尿中砷含量, columnId=1151957373175820401, journalTitle=实验室检测, columnName=创新应用, runingTitle=null, highlight=null, articleAbstract=
目的 探讨和评估使用电感耦合等离子体原子发射光谱仪(ICPOES)来测定尿液样本中砷含量的可行性。方法 通过优化仪器条件、建立工作曲线、测定空白样品、测定标准质控样、定期对加标样测定,确定了该方法的灵敏度、准确度、重复性和检测限等关键参数,以期验证该方法在实际应用中的可靠性和有效性。结果 该方法的灵敏度为156.44,检出限为0.0015 mg/L, 定量限为0.0051 mg/L,标准质控样的检测结果均在控制范围内,加标回收率在90.14%~115.10%之间,同一浓度样品的日內和日间RSD值均未超过8%。结论 该方法能有效监测尿样中砷的微量水平,为砷相关健康风险评价提供依据。
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30(01): 43-45., articleTitle=江西省职业接触砷生物限值研制, refAbstract=null), Reference(id=1154353660835385870, tenantId=1146029695717560320, journalId=1146119944283992078, articleId=1152996333897110335, doi=null, pmid=null, pmcid=null, year=2022, volume=null, issue=null, pageStart=null, pageEnd=null, url=null, language=null, rfNumber=[13], rfOrder=12, authorNames=徐菁, journalName=null, refType=null, unstructuredReference=徐菁. 滇鸡血藤基原植物內南五味子及其近缘物种化学成分和活性的比较研究[D]. 北京: 北京协和医学院,
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| 仪器检测条件和优化参数 | 值 |
| 仪器功率(W) | 1200 |
| 等离子气体(L/min) | 15.00 |
| 雾化器(L/min) | 0.50 |
| 辅助器(L/min) | 0.50 |
| 泵速(mL/min) | 1.00 |
| 检测波长(nm) | 193.696 |
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仪器检测和优化条件参数, figureFileSmall=null, figureFileBig=null, tableContent=
| 仪器检测条件和优化参数 | 值 |
| 仪器功率(W) | 1200 |
| 等离子气体(L/min) | 15.00 |
| 雾化器(L/min) | 0.50 |
| 辅助器(L/min) | 0.50 |
| 泵速(mL/min) | 1.00 |
| 检测波长(nm) | 193.696 |
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| 管号 | 砷含量为 标准使用液体积(mL) | 空白尿液体积(mL) | 定容体积(mL) | 砷含量 (μg/L) | 强度 |
| 1 | 0.25 | 5.00 | 50.00 | 5.00 | 190 |
| 2 | 0.50 | 5.00 | 50.00 | 10.00 | 228 |
| 3 | 1.00 | 5.00 | 50.00 | 20.00 | 300 |
| 4 | 1.50 | 5.00 | 50.00 | 30.00 | 380 |
| 5 | 2.00 | 5.00 | 50.00 | 40.00 | 456 |
| 6 | 2.50 | 5.00 | 50.00 | 50.00 | 545 |
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| 管号 | 砷含量为 标准使用液体积(mL) | 空白尿液体积(mL) | 定容体积(mL) | 砷含量 (μg/L) | 强度 |
| 1 | 0.25 | 5.00 | 50.00 | 5.00 | 190 |
| 2 | 0.50 | 5.00 | 50.00 | 10.00 | 228 |
| 3 | 1.00 | 5.00 | 50.00 | 20.00 | 300 |
| 4 | 1.50 | 5.00 | 50.00 | 30.00 | 380 |
| 5 | 2.00 | 5.00 | 50.00 | 40.00 | 456 |
| 6 | 2.50 | 5.00 | 50.00 | 50.00 | 545 |
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| 空白样品编号 | 强度 | 最小值 | 最大值 | 均值 | 标准偏差 | 检测限 LOD(mg/L) | 定量限 |
| 空白 1 | 173 | | | | | | |
| 空白 2 | 185 | | | | | | |
| 空白 3 | 179 | | | | | | |
| 空白 4 | 171 | | | | | | |
| 空白 5 | 177 | | | | | | |
| 空白 6 | 191 | 171 | 197 | 180.64 | 7.941 | 0.0015 | 0.0051 |
| 空白 7 | 173 | | | | | | |
| 空白 8 | 179 | | | | | | |
| 空白 9 | 179 | | | | | | |
| 空白 10 | 197 | | | | | | |
| 空白 11 | 183 | | | | | | |
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样品空白检测结果统计及检测限表, figureFileSmall=null, figureFileBig=null, tableContent=
| 空白样品编号 | 强度 | 最小值 | 最大值 | 均值 | 标准偏差 | 检测限 LOD(mg/L) | 定量限 |
| 空白 1 | 173 | | | | | | |
| 空白 2 | 185 | | | | | | |
| 空白 3 | 179 | | | | | | |
| 空白 4 | 171 | | | | | | |
| 空白 5 | 177 | | | | | | |
| 空白 6 | 191 | 171 | 197 | 180.64 | 7.941 | 0.0015 | 0.0051 |
| 空白 7 | 173 | | | | | | |
| 空白 8 | 179 | | | | | | |
| 空白 9 | 179 | | | | | | |
| 空白 10 | 197 | | | | | | |
| 空白 11 | 183 | | | | | | |
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| 检测时间 | 质控样名称 | 批号 | 测定值 | 质控样参考值范围 |
| 第一天 | GDOHNYBZ025-1 | 20230323 | 114.20 | ${115.69} \pm {12.62}$ |
| GDOHNYBZ025-2 | 20230323 | 209.18 | ${201.38} \pm {12.62}$ |
| 第二天 | GDOHNYBZ025-1 | 20230323 | 116.08 | ${115.69} \pm {12.62}$ |
| GDOHNYBZ025-2 | 20230323 | 205.66 | ${201.38} \pm {12.62}$ |
| 第三天 | GDOHNYBZ025-1 | 20230323 | 115.76 | ${115.69} \pm {12.62}$ |
| GDOHNYBZ025-2 | 20230323 | 204.72 | ${201.38} \pm {12.62}$ |
), ArticleFig(id=1154353659258327529, tenantId=1146029695717560320, journalId=1146119944283992078, articleId=1152996333897110335, language=CN, label=表 4, caption=
质控样测定结果汇总表, figureFileSmall=null, figureFileBig=null, tableContent=
| 检测时间 | 质控样名称 | 批号 | 测定值 | 质控样参考值范围 |
| 第一天 | GDOHNYBZ025-1 | 20230323 | 114.20 | ${115.69} \pm {12.62}$ |
| GDOHNYBZ025-2 | 20230323 | 209.18 | ${201.38} \pm {12.62}$ |
| 第二天 | GDOHNYBZ025-1 | 20230323 | 116.08 | ${115.69} \pm {12.62}$ |
| GDOHNYBZ025-2 | 20230323 | 205.66 | ${201.38} \pm {12.62}$ |
| 第三天 | GDOHNYBZ025-1 | 20230323 | 115.76 | ${115.69} \pm {12.62}$ |
| GDOHNYBZ025-2 | 20230323 | 204.72 | ${201.38} \pm {12.62}$ |
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| 检测时间 | 加标量 | 平均值回收率 | 最小值回收率 | 最大值回收率 | 相对标准偏差 |
| 第一天 | 5 | 101.80% | 95.18% | 107.30% | 0.92% |
| 20 | 103.57% | 95.91% | 113.36% | 0.26% |
| 40 | 97.48% | 93.48% | 105.46% | 0.10% |
| 第二天 | 5 | 101.73% | 93.84% | 109.08% | 1.17% |
| 20 | 104.63% | 95.20% | 111.80% | 0.32% |
| 40 | 102.73% | 94.90% | 110.25% | 0.13% |
| 第三天 | 5 | 101.28% | 90.14% | 115.10% | 1.95% |
| 20 | 97.78% | 92.70% | 105.20% | 0.23% |
| 40 | 101.31% | 95.97% | 102.48% | 0.06% |
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加标回收结果统计表, figureFileSmall=null, figureFileBig=null, tableContent=
| 检测时间 | 加标量 | 平均值回收率 | 最小值回收率 | 最大值回收率 | 相对标准偏差 |
| 第一天 | 5 | 101.80% | 95.18% | 107.30% | 0.92% |
| 20 | 103.57% | 95.91% | 113.36% | 0.26% |
| 40 | 97.48% | 93.48% | 105.46% | 0.10% |
| 第二天 | 5 | 101.73% | 93.84% | 109.08% | 1.17% |
| 20 | 104.63% | 95.20% | 111.80% | 0.32% |
| 40 | 102.73% | 94.90% | 110.25% | 0.13% |
| 第三天 | 5 | 101.28% | 90.14% | 115.10% | 1.95% |
| 20 | 97.78% | 92.70% | 105.20% | 0.23% |
| 40 | 101.31% | 95.97% | 102.48% | 0.06% |
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| 检测日期 | 加标浓度 | 测定结果平均值 | 最小值 (μg/L) | 最大值 | 标准偏差 | 日内 RSD |
| 第一天 | 5.00 | 5.09 | 4.76 | 5.37 | 0.2307845 | 4.53% |
| 20.00 | 20.39 | 19.18 | 21.08 | 0.6635887 | 3.25% |
| 40.00 | 39.26 | 38.05 | 42.18 | 1.5677978 | 3.99% |
| 第二天 | 5.00 | 5.097 | 4.69 | 5.45 | 0.2935723 | 5.77% |
| 20.00 | 20.93 | 19.04 | 22.36 | 1.2920488 | 6.17% |
| 40.00 | 40.597 | 37.96 | 43.50 | 1.8331657 | 4.52% |
| 第三天 | 5.00 | 5.000 | 4.51 | 5.56 | 0.393405 | 7.87% |
| 20.00 | 19.81 | 19.00 | 21.04 | 0.7400113 | 3.74% |
| 40.00 | 40.88 | 40.56 | 40.99 | 0.1636358 | 0.40% |
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| 检测日期 | 加标浓度 | 测定结果平均值 | 最小值 (μg/L) | 最大值 | 标准偏差 | 日内 RSD |
| 第一天 | 5.00 | 5.09 | 4.76 | 5.37 | 0.2307845 | 4.53% |
| 20.00 | 20.39 | 19.18 | 21.08 | 0.6635887 | 3.25% |
| 40.00 | 39.26 | 38.05 | 42.18 | 1.5677978 | 3.99% |
| 第二天 | 5.00 | 5.097 | 4.69 | 5.45 | 0.2935723 | 5.77% |
| 20.00 | 20.93 | 19.04 | 22.36 | 1.2920488 | 6.17% |
| 40.00 | 40.597 | 37.96 | 43.50 | 1.8331657 | 4.52% |
| 第三天 | 5.00 | 5.000 | 4.51 | 5.56 | 0.393405 | 7.87% |
| 20.00 | 19.81 | 19.00 | 21.04 | 0.7400113 | 3.74% |
| 40.00 | 40.88 | 40.56 | 40.99 | 0.1636358 | 0.40% |
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