Article(id=1217529313067451125, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1217529305693864468, articleNumber=null, orderNo=null, doi=10.19812/j.cnki.jfsq11-5956/ts.20250213007, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=research-article, receivedDate=1739376000000, receivedDateStr=2025-02-13, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1768211208835, onlineDateStr=2026-01-12, pubDate=1752508800000, pubDateStr=2025-07-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1768211208835, onlineIssueDateStr=2026-01-12, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1768211208835, creator=13701087609, updateTime=1768211208835, updator=13701087609, issue=Issue{id=1217529305693864468, tenantId=1146029695717560320, journalId=1149652044408987649, year='2025', volume='16', issue='13', pageStart='1', pageEnd='320', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1768211207077, creator=13701087609, updateTime=1768212057891, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1217532874337730593, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1217529305693864468, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1217532874337730594, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1217529305693864468, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=144, endPage=154, ext={EN=ArticleExt(id=1217529314103444246, articleId=1217529313067451125, tenantId=1146029695717560320, journalId=1149652044408987649, language=EN, title=Determination of the content of 5 kinds of caffeoylquinic acid in
Lonicera japonica Thunb. from Sandao real estate area by quantitative analysis of multi-components by single marker, columnId=1217529307778438039, journalTitle=Journal of Food Safety & Quality, columnName=Highlight: Application of Modern Analysis Instrument in Food Detection, runingTitle=null, highlight=null, articleAbstract=
Objective To establish a method to simultaneously determine the content of 5 kinds of components of Lonicera japonica Thunb. herbs from Sandao real estate area (neochlorogenic acid, chlorogenic acid, isochlorogenic acid A, isochlorogenic acid B and isochlorogenic acid C) by quantitative analysis of multi-components by single marker. Methods Phenomenex Synergi Hydro-RP80A (250 mm×4.6 mm, 4 μm) column was used with acetonitrile (A)-0.1% phosphoric acid aqueous solution (B) as mobile phase, the detection wavelength was 327 nm, the column temperature was 20 ℃, and the flow rate was 0.7 mL/min. The injection volume was 2 µL. Results The linear ranges of neochlorogenic acid, chlorogenic acid, isochlorogenic acid B, isochlorogenic acid A and isochlorogenic acid C were 0.41-16.40, 7.22-289.00, 0.21-8.50, 1.65-66.00 and 0.37-14.80 μg/mL (r≥0.9993), respectively. The average recovery rate was 95.25%-100.42%, and the relative standard deviation (RSD) of precision, repeatability and stability were less than 2.0%. The content of neochlorogenic acid, chlorogenic acid, isochlorogenic acid A, isochlorogenic acid B and isochlorogenic acid C in 25 batches of samples was determined by external standard method, and there was no significant difference between the measured values and the calculated values of quantitative analysis of multi-components by single marker method. Conclusion This method is accurate, reliable and simple for the simultaneous determination of the content of 5 kinds of compounds in Lonicera japonica Thunb., which solves the bottleneck problem of lack of reference substances in the quality control of Lonicera japonica Thunb.. The content of caffeoylquinic acid in Lonicera japonica Thunb. from different origins varies greatly, and it is necessary to further strengthen the processing of Lonicera japonica Thunb.. This study provides an important basis for the identification, quality evaluation and formulation of quality standards of Lonicera japonica Thunb..
, correspAuthors=Zheng-Gang HUA, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Zhen-Zhen QI, Bing-Ya ZHU, Zheng-Gang HUA), CN=ArticleExt(id=1217529315080717152, articleId=1217529313067451125, tenantId=1146029695717560320, journalId=1149652044408987649, language=CN, title=一测多评法测定三大道地产区金银花中5种咖啡酰奎宁酸含量, columnId=1217529307954598811, journalTitle=食品安全质量检测学报, columnName=本期重点：现代分析仪器在食品检测中的应用, runingTitle=null, highlight=null, articleAbstract=
目的 建立一测多评法同时测定三大道地产区金银花药材中新绿原酸、绿原酸、异绿原酸A、异绿原酸B、异绿原酸C 5种成分的含量。方法 采用Phenomenex Synergi Hydro-RP80A (250 mm×4.6 mm, 4 µm)色谱柱, 以乙腈(A)-0.1%磷酸水溶液(B)为流动相, 检测波长327 nm, 柱温20 ℃, 流速0.7 mL/min; 进样量2 µL。结果 新绿原酸、绿原酸、异绿原酸B、异绿原酸A、异绿原酸C的线性范围分别为0.41~16.40、7.22~289.00、0.21~8.50、1.65~66.00、0.37~14.80 μg/mL (r≥0.9993), 平均回收率为95.25%~100.42%, 精密度、重复性、稳定性相对标准偏差(relative standard deviation, RSD)均小于等于2.0%; 利用外标法测25批样品中新绿原酸、绿原酸、异绿原酸A、异绿原酸B、异绿原酸C的含量, 其测定值与一测多评法计算值无显著性差异。结论 本方法同时测定金银花中5个化合物含量准确可靠且方法简便, 解决了金银花质量控制中缺乏对照品这一瓶颈问题。不同产地的金银花中咖啡酰奎宁酸类的含量差别较大。本研究为金银花的鉴别、品质评价、制定质量标准等提供了重要的依据。
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祁珍祯(1989—), 女, 副主任技师, 硕士, 主要研究方向为食品药品检测与分析。E-mail: 15040206892@163.com
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祁珍祯(1989—), 女, 副主任技师, 硕士, 主要研究方向为食品药品检测与分析。E-mail: 15040206892@163.com
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Lonicerae flos, refAbstract=null)], funds=null, companyList=[AuthorCompany(id=1217901252533473743, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, xref=null, ext=[AuthorCompanyExt(id=1217901252541862351, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, companyId=1217901252533473743, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=Liaoning Provincial Center for Disease Control and Prevention, Liaoning Provincial Key Laboratory of Air Haze and Population Health Monitoring, Shenyang 110005, China), AuthorCompanyExt(id=1217901252550250960, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, companyId=1217901252533473743, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=辽宁省疾病预防控制中心, 辽宁省空气雾霾与人群健康监测重点实验室, 沈阳 110005)])], figs=[ArticleFig(id=1217901256400622264, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Fig.1, caption=
Ultraviolet absorption spectra of 5 kinds of reference standards, figureFileSmall=lpEkRRiR18maB/ccDLIhVQ==, figureFileBig=2bpd/5g/jDI5qzlFxczuHA==, tableContent=null), ArticleFig(id=1217901256530645697, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=图1, caption=
5种对照品的紫外线吸收光谱 注: a. 新绿原酸; b. 绿原酸; c. 异绿原酸A; d. 异绿原酸B; e. 异绿原酸C。
, figureFileSmall=lpEkRRiR18maB/ccDLIhVQ==, figureFileBig=2bpd/5g/jDI5qzlFxczuHA==, tableContent=null), ArticleFig(id=1217901256740360914, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Fig.2, caption=
High performance liquid chromatograms of 5 kinds of reference substances Lonicera japonica Thunb. sample solution, figureFileSmall=JYAzhaMK2pY6KRRr2R49Uw==, figureFileBig=F9z7Gb5DS8fd19jYG1d7fw==, tableContent=null), ArticleFig(id=1217901256845218526, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=图2, caption=
5种对照品(a)和金银花样品溶液(b)的高效液相色谱图 注: 1. 新绿原酸; 2. 绿原酸; 3. 异绿原酸B; 4. 异绿原酸A; 5. 异绿原酸C。
, figureFileSmall=JYAzhaMK2pY6KRRr2R49Uw==, figureFileBig=F9z7Gb5DS8fd19jYG1d7fw==, tableContent=null), ArticleFig(id=1217901256958464744, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 1, caption=
Sources of Lonicera japonica Thunb. samples
, figureFileSmall=null, figureFileBig=null, tableContent=
| 样品号 | 产地 | 样品号 | 产地 | 样品号 | 产地 |
| S1 | 山东平邑县1 | S10 | 河南新密市1 | S19 | 山东临沂市6 |
| S2 | 山东平邑县2 | S11 | 河南新密市2 | S20 | 山东临沂市7 |
| S3 | 山东平邑县3 | S12 | 河南新密市3 | S21 | 河南封丘县1 |
| S4 | 山东平邑县4 | S13 | 河南新密市4 | S22 | 河南封丘县2 |
| S5 | 山东平邑县5 | S14 | 山东临沂市1 | S23 | 河南封丘县3 |
| S6 | 河北巨鹿县1 | S15 | 山东临沂市2 | S24 | 河南封丘县4 |
| S7 | 河北巨鹿县2 | S16 | 山东临沂市3 | S25 | 河南封丘县5 |
| S8 | 河北巨鹿县3 | S17 | 山东临沂市4 | | |
| S9 | 河北巨鹿县4 | S18 | 山东临沂市5 | | |
), ArticleFig(id=1217901258371945207, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表1, caption=
金银花样品来源
, figureFileSmall=null, figureFileBig=null, tableContent=
| 样品号 | 产地 | 样品号 | 产地 | 样品号 | 产地 |
| S1 | 山东平邑县1 | S10 | 河南新密市1 | S19 | 山东临沂市6 |
| S2 | 山东平邑县2 | S11 | 河南新密市2 | S20 | 山东临沂市7 |
| S3 | 山东平邑县3 | S12 | 河南新密市3 | S21 | 河南封丘县1 |
| S4 | 山东平邑县4 | S13 | 河南新密市4 | S22 | 河南封丘县2 |
| S5 | 山东平邑县5 | S14 | 山东临沂市1 | S23 | 河南封丘县3 |
| S6 | 河北巨鹿县1 | S15 | 山东临沂市2 | S24 | 河南封丘县4 |
| S7 | 河北巨鹿县2 | S16 | 山东临沂市3 | S25 | 河南封丘县5 |
| S8 | 河北巨鹿县3 | S17 | 山东临沂市4 | | |
| S9 | 河北巨鹿县4 | S18 | 山东临沂市5 | | |
), ArticleFig(id=1217901258694906629, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 2, caption=
Comparison table of peak areas for different extraction solvents
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 甲醇提取峰面积 | 乙醇提取峰面积 | 50%甲醇提取峰面积 | 75%甲醇提取峰面积 | 纯水提取峰面积 |
| 新绿原酸 | 30.82 | 26.35 | 37.84 | 36.57 | 18.25 |
| 绿原酸 | 803.25 | 789.52 | 873.84 | 876.31 | 543.16 |
| 异绿原酸B | 20.48 | 20.83 | 21.41 | 18.25 | 17.35 |
| 异绿原酸A | 563.27 | 594.62 | 606.45 | 601.43 | 487.90 |
| 异绿原酸C | 75.46 | 79.35 | 83.32 | 83.11 | 53.99 |
), ArticleFig(id=1217901258812347150, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表2, caption=
不同提取溶剂峰面积对照表
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 甲醇提取峰面积 | 乙醇提取峰面积 | 50%甲醇提取峰面积 | 75%甲醇提取峰面积 | 纯水提取峰面积 |
| 新绿原酸 | 30.82 | 26.35 | 37.84 | 36.57 | 18.25 |
| 绿原酸 | 803.25 | 789.52 | 873.84 | 876.31 | 543.16 |
| 异绿原酸B | 20.48 | 20.83 | 21.41 | 18.25 | 17.35 |
| 异绿原酸A | 563.27 | 594.62 | 606.45 | 601.43 | 487.90 |
| 异绿原酸C | 75.46 | 79.35 | 83.32 | 83.11 | 53.99 |
), ArticleFig(id=1217901258933981976, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 3, caption=
Comparison table of peak area of different extraction methods and solvent dosage
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 10 mL 50%甲醇提取峰面积 | 20 mL 50%甲醇提取峰面积 | 40 mL 50%甲醇提取峰面积 | 超声提取峰
面积 | 冷浸提提取峰
面积 | 回流提取峰
面积 |
| 新绿原酸 | 30.66 | 37.84 | 38.25 | 37.68 | 33.16 | 38.12 |
| 绿原酸 | 705.32 | 873.84 | 872.42 | 871.85 | 756.09 | 872.94 |
| 异绿原酸B | 16.81 | 21.41 | 20.69 | 20.93 | 16.53 | 21.26 |
| 异绿原酸A | 509.10 | 606.45 | 606.81 | 606.89 | 592.37 | 605.88 |
| 异绿原酸C | 74.56 | 83.32 | 84.02 | 83.66 | 72.15 | 82.98 |
), ArticleFig(id=1217901259072394022, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表3, caption=
不同提取方式及溶剂用量峰面积对照表
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 10 mL 50%甲醇提取峰面积 | 20 mL 50%甲醇提取峰面积 | 40 mL 50%甲醇提取峰面积 | 超声提取峰
面积 | 冷浸提提取峰
面积 | 回流提取峰
面积 |
| 新绿原酸 | 30.66 | 37.84 | 38.25 | 37.68 | 33.16 | 38.12 |
| 绿原酸 | 705.32 | 873.84 | 872.42 | 871.85 | 756.09 | 872.94 |
| 异绿原酸B | 16.81 | 21.41 | 20.69 | 20.93 | 16.53 | 21.26 |
| 异绿原酸A | 509.10 | 606.45 | 606.81 | 606.89 | 592.37 | 605.88 |
| 异绿原酸C | 74.56 | 83.32 | 84.02 | 83.66 | 72.15 | 82.98 |
), ArticleFig(id=1217901259185640242, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 4, caption=
Calibration curves and mass concentration ranges of 5 kinds of components
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 校准曲线 | 相关系数(r) | 质量浓度范围
/(μg/mL) |
| 新绿原酸 | Y=8.0348X+0.5741 | 0.9997 | 0.41~16.40 |
| 绿原酸 | Y=8.2367X+6.4705 | 0.9999 | 7.22~289.00 |
| 异绿原酸B | Y=8.9177X+2.6588 | 0.9995 | 0.21~8.50 |
| 异绿原酸A | Y=10.44X+2.8075 | 0.9993 | 1.65~66.00 |
| 异绿原酸C | Y=8.709X-1.8738 | 0.9998 | 0.37~14.80 |
), ArticleFig(id=1217901259298886461, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表4, caption=
5种成分的校准曲线和质量浓度范围
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 校准曲线 | 相关系数(r) | 质量浓度范围
/(μg/mL) |
| 新绿原酸 | Y=8.0348X+0.5741 | 0.9997 | 0.41~16.40 |
| 绿原酸 | Y=8.2367X+6.4705 | 0.9999 | 7.22~289.00 |
| 异绿原酸B | Y=8.9177X+2.6588 | 0.9995 | 0.21~8.50 |
| 异绿原酸A | Y=10.44X+2.8075 | 0.9993 | 1.65~66.00 |
| 异绿原酸C | Y=8.709X-1.8738 | 0.9998 | 0.37~14.80 |
), ArticleFig(id=1217901259416326982, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 5, caption=
Results of intraday precision and daytime precision
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 低浓度日内精密度 | 中浓度日内精密度 | 高浓度日内精密度 | 日间精密度 |
| 峰面积平均值 | RSDs/% | 峰面积平均值 | RSDs/% | 峰面积平均值 | RSDs/% | 峰面积平均值 | RSDs/% |
| 新绿原酸 | 7.35 | 1.66 | 34.68 | 1.56 | 131.16 | 1.48 | 34.84 | 1.37 |
| 绿原酸 | 306.50 | 1.29 | 1480.50 | 0.11 | 5918.30 | 0.08 | 1480.00 | 0.12 |
| 异绿原酸B | 6.93 | 1.75 | 21.65 | 1.79 | 74.53 | 1.10 | 21.29 | 1.63 |
| 异绿原酸A | 175.80 | 1.38 | 856.90 | 0.98 | 3464.00 | 0.09 | 858.40 | 0.51 |
| 异绿原酸C | 31.28 | 1.81 | 162.20 | 0.94 | 648.10 | 0.21 | 161.80 | 0.79 |
), ArticleFig(id=1217901259542156108, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表5, caption=
日内及日间精密度结果
, figureFileSmall=null, figureFileBig=null, tableContent=
| 成分 | 低浓度日内精密度 | 中浓度日内精密度 | 高浓度日内精密度 | 日间精密度 |
| 峰面积平均值 | RSDs/% | 峰面积平均值 | RSDs/% | 峰面积平均值 | RSDs/% | 峰面积平均值 | RSDs/% |
| 新绿原酸 | 7.35 | 1.66 | 34.68 | 1.56 | 131.16 | 1.48 | 34.84 | 1.37 |
| 绿原酸 | 306.50 | 1.29 | 1480.50 | 0.11 | 5918.30 | 0.08 | 1480.00 | 0.12 |
| 异绿原酸B | 6.93 | 1.75 | 21.65 | 1.79 | 74.53 | 1.10 | 21.29 | 1.63 |
| 异绿原酸A | 175.80 | 1.38 | 856.90 | 0.98 | 3464.00 | 0.09 | 858.40 | 0.51 |
| 异绿原酸C | 31.28 | 1.81 | 162.20 | 0.94 | 648.10 | 0.21 | 161.80 | 0.79 |
), ArticleFig(id=1217901259688956754, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 6, caption=
Influence of various factors on the relative retention value
, figureFileSmall=null, figureFileBig=null, tableContent=
| 仪器 | 色谱柱 | 相对保留值 |
| 新绿原酸 | 绿原酸 | 异绿原酸B | 异绿原酸A | 异绿原酸C |
| Agilent 1260 | Phenomenex Synergi Hydro-RP80A | 0.73 | 1.00 | 2.53 | 2.75 | 2.93 |
| InfinityLab Poroshell 120 EC-C18 | 0.71 | 1.00 | 2.55 | 2.78 | 2.91 |
| Accucore™ XL C18 | 0.72 | 1.00 | 2.56 | 2.76 | 2.87 |
| Waters e2695 | Phenomenex Synergi Hydro-RP80A | 0.71 | 1.00 | 2.52 | 2.68 | 2.89 |
| InfinityLab Poroshell 120 EC-C18 | 0.70 | 1.00 | 2.55 | 2.72 | 2.92 |
| Accucore™ XL C18 | 0.73 | 1.00 | 2.54 | 2.75 | 2.86 |
| 平均值 | | 0.72 | 1.00 | 2.54 | 2.74 | 2.89 |
| RSDs/% | | 1.69 | 0.00 | 0.62 | 1.18 | 0.91 |
), ArticleFig(id=1217901259827368797, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表6, caption=
各种因素对相对保留值的影响
, figureFileSmall=null, figureFileBig=null, tableContent=
| 仪器 | 色谱柱 | 相对保留值 |
| 新绿原酸 | 绿原酸 | 异绿原酸B | 异绿原酸A | 异绿原酸C |
| Agilent 1260 | Phenomenex Synergi Hydro-RP80A | 0.73 | 1.00 | 2.53 | 2.75 | 2.93 |
| InfinityLab Poroshell 120 EC-C18 | 0.71 | 1.00 | 2.55 | 2.78 | 2.91 |
| Accucore™ XL C18 | 0.72 | 1.00 | 2.56 | 2.76 | 2.87 |
| Waters e2695 | Phenomenex Synergi Hydro-RP80A | 0.71 | 1.00 | 2.52 | 2.68 | 2.89 |
| InfinityLab Poroshell 120 EC-C18 | 0.70 | 1.00 | 2.55 | 2.72 | 2.92 |
| Accucore™ XL C18 | 0.73 | 1.00 | 2.54 | 2.75 | 2.86 |
| 平均值 | | 0.72 | 1.00 | 2.54 | 2.74 | 2.89 |
| RSDs/% | | 1.69 | 0.00 | 0.62 | 1.18 | 0.91 |
), ArticleFig(id=1217901259957392225, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 7, caption=
Relative correction factor and its RSDs
, figureFileSmall=null, figureFileBig=null, tableContent=
| 次数 | 新绿
原酸 | 绿原酸 | 异绿
原酸B | 异绿
原酸A | 异绿
原酸C |
| 1 | 0.98 | 1.00 | 1.21 | 1.27 | 1.04 |
| 2 | 0.98 | 1.00 | 1.21 | 1.27 | 1.03 |
| 3 | 0.99 | 1.00 | 1.19 | 1.26 | 1.02 |
| 4 | 0.99 | 1.00 | 1.20 | 1.27 | 1.03 |
| 5 | 0.99 | 1.00 | 1.19 | 1.27 | 1.03 |
| 6 | 0.99 | 1.00 | 1.21 | 1.27 | 1.04 |
| 平均值 | 0.99 | 1.00 | 1.20 | 1.27 | 1.03 |
| RSDs/% | 0.52 | 0.00 | 1.52 | 0.32 | 0.73 |
), ArticleFig(id=1217901260087415657, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表7, caption=
相对校正因子及其RSDs
, figureFileSmall=null, figureFileBig=null, tableContent=
| 次数 | 新绿
原酸 | 绿原酸 | 异绿
原酸B | 异绿
原酸A | 异绿
原酸C |
| 1 | 0.98 | 1.00 | 1.21 | 1.27 | 1.04 |
| 2 | 0.98 | 1.00 | 1.21 | 1.27 | 1.03 |
| 3 | 0.99 | 1.00 | 1.19 | 1.26 | 1.02 |
| 4 | 0.99 | 1.00 | 1.20 | 1.27 | 1.03 |
| 5 | 0.99 | 1.00 | 1.19 | 1.27 | 1.03 |
| 6 | 0.99 | 1.00 | 1.21 | 1.27 | 1.04 |
| 平均值 | 0.99 | 1.00 | 1.20 | 1.27 | 1.03 |
| RSDs/% | 0.52 | 0.00 | 1.52 | 0.32 | 0.73 |
), ArticleFig(id=1217901260217439091, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=EN, label=Table 8, caption=
Comparison of the content of 5 kinds of caffeoylquinic acid in Lonicera japonica Thunb. Samples (%)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 样品号 | 测定方法 | 新绿原酸 | 绿原酸 | 异绿原酸 B | 异绿原酸A | 异绿原酸C |
| S1 | 一测多评法 | 0.1143 | - | 0.0676 | 1.1255 | 0.3009 |
| 外标法 | 0.1154 | 2.1356 | 0.0694 | 1.1307 | 0.2996 |
| RSDs | 0.68 | - | 1.86 | 0.33 | 0.31 |
| S2 | 一测多评法 | 0.1161 | - | 0.0546 | 0.8742 | 0.1880 |
| 外标法 | 0.1172 | 2.2900 | 0.0549 | 0.8765 | 0.1887 |
| RSDs | 0.67 | - | 0.39 | 0.19 | 0.26 |
| S3 | 一测多评法 | 0.1391 | - | 0.0490 | 1.0091 | 0.2142 |
| 外标法 | 0.1408 | 1.9623 | 0.0488 | 1.0138 | 0.2146 |
| RSDs | 0.86 | - | 0.29 | 0.33 | 0.13 |
| S4 | 一测多评法 | 0.1076 | - | 0.0495 | 0.7974 | 0.2472 |
| 外标法 | 0.1086 | 1.9099 | 0.0494 | 0.7457 | 0.2313 |
| RSDs | 0.86 | - | 0.14 | 4.74 | 4.70 |
| S5 | 一测多评法 | 0.1197 | - | 0.0371 | 0.8305 | 0.2008 |
| 外标法 | 0.1209 | 2.1012 | 0.0354 | 0.8329 | 0.2015 |
| RSDs | 0.71 | - | 3.32 | 0.20 | 0.25 |
| S6 | 一测多评法 | 0.1250 | - | 0.0256 | 1.0723 | 0.2011 |
| 外标法 | 0.1262 | 2.5859 | 0.0245 | 1.0756 | 0.2015 |
| RSDs | 0.68 | - | 3.11 | 0.22 | 0.14 |
| S7 | 一测多评法 | 0.0801 | - | 0.0504 | 0.5833 | 0.1801 |
| 外标法 | 0.0805 | 1.9026 | 0.0503 | 0.5840 | 0.1812 |
| RSDs | 0.35 | - | 0.14 | 0.08 | 0.43 |
| S8 | 一测多评法 | 0.1258 | - | 0.0623 | 1.4253 | 0.3425 |
| 外标法 | 0.1271 | 2.1696 | 0.0635 | 1.4332 | 0.3405 |
| RSDs | 0.73 | - | 1.35 | 0.39 | 0.41 |
| S9 | 一测多评法 | 0.0890 | - | 0.0588 | 0.7642 | 0.1579 |
| 外标法 | 0.0896 | 2.0009 | 0.0597 | 0.7664 | 0.1593 |
| RSDs | 0.48 | - | 1.07 | 0.20 | 0.62 |
| S10 | 一测多评法 | 0.0706 | - | 0.0390 | 0.8295 | 0.1628 |
| 外标法 | 0.0707 | 2.2636 | 0.0376 | 0.8316 | 0.1639 |
| RSDs | 0.10 | - | 2.58 | 0.18 | 0.48 |
| S11 | 一测多评法 | 0.1012 | - | 0.0551 | 1.1803 | 0.2623 |
| 外标法 | 0.1019 | 2.6326 | 0.0555 | 1.1843 | 0.2613 |
| RSDs/% | 0.49 | - | 0.51 | 0.24 | 0.27 |
| S12 | 一测多评法 | 0.1233 | - | 0.0486 | 1.0059 | 0.2523 |
| 外标法 | 0.1246 | 2.2548 | 0.0482 | 1.0095 | 0.2518 |
| RSDs | 0.74 | - | 0.58 | 0.25 | 0.14 |
| S13 | 一测多评法 | 0.0862 | - | 0.0321 | 1.2871 | 0.2041 |
| 外标法 | 0.0866 | 2.7784 | 0.0307 | 1.2916 | 0.2044 |
| RSDs | 0.33 | - | 3.15 | 0.25 | 0.10 |
| S14 | 一测多评法 | 0.0901 | - | 0.0595 | 1.1530 | 0.2418 |
| 外标法 | 0.0906 | 2.3354 | 0.0604 | 1.1576 | 0.2415 |
| RSDs | 0.39 | - | 1.06 | 0.28 | 0.09 |
| S15 | 一测多评法 | 0.0791 | - | 0.0497 | 1.2249 | 0.2182 |
| 外标法 | 0.0795 | 1.9765 | 0.0494 | 1.2316 | 0.2185 |
| RSDs | 0.36 | - | 0.43 | 0.39 | 0.10 |
| S16 | 一测多评法 | 0.0912 | - | 0.0426 | 1.1396 | 0.1931 |
| 外标法 | 0.0919 | 2.0855 | 0.0416 | 1.1451 | 0.1937 |
| RSDs | 0.54 | - | 1.68 | 0.34 | 0.22 |
| S17 | 一测多评法 | 0.0968 | - | 0.0409 | 0.8777 | 0.2463 |
| 外标法 | 0.0976 | 2.0160 | 0.0398 | 0.8809 | 0.2461 |
| RSDs | 0.58 | - | 1.93 | 0.26 | 0.06 |
| S18 | 一测多评法 | 0.1142 | - | 0.0620 | 0.8408 | 0.2809 |
| 外标法 | 0.1153 | 2.2413 | 0.0632 | 0.8430 | 0.2799 |
| RSDs | 0.68 | - | 1.36 | 0.18 | 0.25 |
| S19 | 一测多评法 | 0.1106 | - | 0.0501 | 0.9756 | 0.2298 |
| 外标法 | 0.1116 | 2.0887 | 0.0500 | 0.9795 | 0.2299 |
| RSDs | 0.64 | - | 0.14 | 0.28 | 0.03 |
| S20 | 一测多评法 | 0.0900 | - | 0.0594 | 0.8027 | 0.2211 |
| 外标法 | 0.0907 | 1.7333 | 0.0605 | 0.8062 | 0.2217 |
| RSDs | 0.55 | - | 1.30 | 0.31 | 0.19 |
| S21 | 一测多评法 | 0.0696 | - | 0.0500 | 1.2694 | 0.2496 |
| 外标法 | 0.0698 | 2.0144 | 0.0499 | 1.2765 | 0.2493 |
| RSDs | 0.20 | - | 0.14 | 0.39 | 0.09 |
| S22 | 一测多评法 | 0.1098 | - | 0.0554 | 0.8976 | 0.2630 |
| 外标法 | 0.1109 | 2.0111 | 0.0559 | 0.9010 | 0.2625 |
| RSDs | 0.70 | - | 0.64 | 0.27 | 0.13 |
| S23 | 一测多评法 | 0.1058 | - | 0.0724 | 0.9439 | 0.3244 |
| 外标法 | 0.1067 | 2.1920 | 0.0748 | 0.9472 | 0.3226 |
| RSDs | 0.60 | - | 2.31 | 0.25 | 0.39 |
| S24 | 一测多评法 | 0.0627 | - | 0.0320 | 0.6279 | 0.1228 |
| 外标法 | 0.0628 | 1.8482 | 0.0315 | 0.6291 | 0.1248 |
| RSDs | 0.11 | - | 1.11 | 0.14 | 1.14 |
| S25 | 一测多评法 | 0.1007 | - | 0.0354 | 0.9582 | 0.1935 |
| 外标法 | 0.1015 | 2.0017 | 0.0335 | 0.9623 | 0.1943 |
| RSDs | 0.56 | - | 3.90 | 0.30 | 0.29 |
), ArticleFig(id=1217901260368434046, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1217529313067451125, language=CN, label=表8, caption=
金银花样品中5种咖啡酰奎宁酸的含量测定比对(%)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 样品号 | 测定方法 | 新绿原酸 | 绿原酸 | 异绿原酸 B | 异绿原酸A | 异绿原酸C |
| S1 | 一测多评法 | 0.1143 | - | 0.0676 | 1.1255 | 0.3009 |
| 外标法 | 0.1154 | 2.1356 | 0.0694 | 1.1307 | 0.2996 |
| RSDs | 0.68 | - | 1.86 | 0.33 | 0.31 |
| S2 | 一测多评法 | 0.1161 | - | 0.0546 | 0.8742 | 0.1880 |
| 外标法 | 0.1172 | 2.2900 | 0.0549 | 0.8765 | 0.1887 |
| RSDs | 0.67 | - | 0.39 | 0.19 | 0.26 |
| S3 | 一测多评法 | 0.1391 | - | 0.0490 | 1.0091 | 0.2142 |
| 外标法 | 0.1408 | 1.9623 | 0.0488 | 1.0138 | 0.2146 |
| RSDs | 0.86 | - | 0.29 | 0.33 | 0.13 |
| S4 | 一测多评法 | 0.1076 | - | 0.0495 | 0.7974 | 0.2472 |
| 外标法 | 0.1086 | 1.9099 | 0.0494 | 0.7457 | 0.2313 |
| RSDs | 0.86 | - | 0.14 | 4.74 | 4.70 |
| S5 | 一测多评法 | 0.1197 | - | 0.0371 | 0.8305 | 0.2008 |
| 外标法 | 0.1209 | 2.1012 | 0.0354 | 0.8329 | 0.2015 |
| RSDs | 0.71 | - | 3.32 | 0.20 | 0.25 |
| S6 | 一测多评法 | 0.1250 | - | 0.0256 | 1.0723 | 0.2011 |
| 外标法 | 0.1262 | 2.5859 | 0.0245 | 1.0756 | 0.2015 |
| RSDs | 0.68 | - | 3.11 | 0.22 | 0.14 |
| S7 | 一测多评法 | 0.0801 | - | 0.0504 | 0.5833 | 0.1801 |
| 外标法 | 0.0805 | 1.9026 | 0.0503 | 0.5840 | 0.1812 |
| RSDs | 0.35 | - | 0.14 | 0.08 | 0.43 |
| S8 | 一测多评法 | 0.1258 | - | 0.0623 | 1.4253 | 0.3425 |
| 外标法 | 0.1271 | 2.1696 | 0.0635 | 1.4332 | 0.3405 |
| RSDs | 0.73 | - | 1.35 | 0.39 | 0.41 |
| S9 | 一测多评法 | 0.0890 | - | 0.0588 | 0.7642 | 0.1579 |
| 外标法 | 0.0896 | 2.0009 | 0.0597 | 0.7664 | 0.1593 |
| RSDs | 0.48 | - | 1.07 | 0.20 | 0.62 |
| S10 | 一测多评法 | 0.0706 | - | 0.0390 | 0.8295 | 0.1628 |
| 外标法 | 0.0707 | 2.2636 | 0.0376 | 0.8316 | 0.1639 |
| RSDs | 0.10 | - | 2.58 | 0.18 | 0.48 |
| S11 | 一测多评法 | 0.1012 | - | 0.0551 | 1.1803 | 0.2623 |
| 外标法 | 0.1019 | 2.6326 | 0.0555 | 1.1843 | 0.2613 |
| RSDs/% | 0.49 | - | 0.51 | 0.24 | 0.27 |
| S12 | 一测多评法 | 0.1233 | - | 0.0486 | 1.0059 | 0.2523 |
| 外标法 | 0.1246 | 2.2548 | 0.0482 | 1.0095 | 0.2518 |
| RSDs | 0.74 | - | 0.58 | 0.25 | 0.14 |
| S13 | 一测多评法 | 0.0862 | - | 0.0321 | 1.2871 | 0.2041 |
| 外标法 | 0.0866 | 2.7784 | 0.0307 | 1.2916 | 0.2044 |
| RSDs | 0.33 | - | 3.15 | 0.25 | 0.10 |
| S14 | 一测多评法 | 0.0901 | - | 0.0595 | 1.1530 | 0.2418 |
| 外标法 | 0.0906 | 2.3354 | 0.0604 | 1.1576 | 0.2415 |
| RSDs | 0.39 | - | 1.06 | 0.28 | 0.09 |
| S15 | 一测多评法 | 0.0791 | - | 0.0497 | 1.2249 | 0.2182 |
| 外标法 | 0.0795 | 1.9765 | 0.0494 | 1.2316 | 0.2185 |
| RSDs | 0.36 | - | 0.43 | 0.39 | 0.10 |
| S16 | 一测多评法 | 0.0912 | - | 0.0426 | 1.1396 | 0.1931 |
| 外标法 | 0.0919 | 2.0855 | 0.0416 | 1.1451 | 0.1937 |
| RSDs | 0.54 | - | 1.68 | 0.34 | 0.22 |
| S17 | 一测多评法 | 0.0968 | - | 0.0409 | 0.8777 | 0.2463 |
| 外标法 | 0.0976 | 2.0160 | 0.0398 | 0.8809 | 0.2461 |
| RSDs | 0.58 | - | 1.93 | 0.26 | 0.06 |
| S18 | 一测多评法 | 0.1142 | - | 0.0620 | 0.8408 | 0.2809 |
| 外标法 | 0.1153 | 2.2413 | 0.0632 | 0.8430 | 0.2799 |
| RSDs | 0.68 | - | 1.36 | 0.18 | 0.25 |
| S19 | 一测多评法 | 0.1106 | - | 0.0501 | 0.9756 | 0.2298 |
| 外标法 | 0.1116 | 2.0887 | 0.0500 | 0.9795 | 0.2299 |
| RSDs | 0.64 | - | 0.14 | 0.28 | 0.03 |
| S20 | 一测多评法 | 0.0900 | - | 0.0594 | 0.8027 | 0.2211 |
| 外标法 | 0.0907 | 1.7333 | 0.0605 | 0.8062 | 0.2217 |
| RSDs | 0.55 | - | 1.30 | 0.31 | 0.19 |
| S21 | 一测多评法 | 0.0696 | - | 0.0500 | 1.2694 | 0.2496 |
| 外标法 | 0.0698 | 2.0144 | 0.0499 | 1.2765 | 0.2493 |
| RSDs | 0.20 | - | 0.14 | 0.39 | 0.09 |
| S22 | 一测多评法 | 0.1098 | - | 0.0554 | 0.8976 | 0.2630 |
| 外标法 | 0.1109 | 2.0111 | 0.0559 | 0.9010 | 0.2625 |
| RSDs | 0.70 | - | 0.64 | 0.27 | 0.13 |
| S23 | 一测多评法 | 0.1058 | - | 0.0724 | 0.9439 | 0.3244 |
| 外标法 | 0.1067 | 2.1920 | 0.0748 | 0.9472 | 0.3226 |
| RSDs | 0.60 | - | 2.31 | 0.25 | 0.39 |
| S24 | 一测多评法 | 0.0627 | - | 0.0320 | 0.6279 | 0.1228 |
| 外标法 | 0.0628 | 1.8482 | 0.0315 | 0.6291 | 0.1248 |
| RSDs | 0.11 | - | 1.11 | 0.14 | 1.14 |
| S25 | 一测多评法 | 0.1007 | - | 0.0354 | 0.9582 | 0.1935 |
| 外标法 | 0.1015 | 2.0017 | 0.0335 | 0.9623 | 0.1943 |
| RSDs | 0.56 | - | 3.90 | 0.30 | 0.29 |
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