Article(id=1153986584929096560, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153986579971429187, articleNumber=null, orderNo=null, doi=10.19812/j.cnki.jfsq11-5956/ts.20241219008, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1734537600000, receivedDateStr=2024-12-19, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1753061441881, onlineDateStr=2025-07-21, pubDate=1740412800000, pubDateStr=2025-02-25, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1753061441881, onlineIssueDateStr=2025-07-21, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1753061441881, creator=13701087609, updateTime=1753061441881, updator=13701087609, issue=Issue{id=1153986579971429187, tenantId=1146029695717560320, journalId=1149652044408987649, year='2025', volume='16', issue='4', pageStart='1', pageEnd='320', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1753061440699, creator=13701087609, updateTime=1758783495950, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1177986619249406427, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153986579971429187, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1177986619249406428, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153986579971429187, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=71, endPage=77, ext={EN=ArticleExt(id=1153986585679876984, articleId=1153986584929096560, tenantId=1146029695717560320, journalId=1149652044408987649, language=EN, title=Simultaneous determination of 12 kinds of nicotine pesticides in fruits by ultra performance liquid chromatography-tandem mass spectrometry coupled with cold induced liquid-liquid extraction, columnId=1153429495274000613, journalTitle=Journal of Food Safety & Quality, columnName=Special Topic: Research and Detection of Pesticide and Veterinary Drug Residue, runingTitle=null, highlight=null, articleAbstract=
Objective To establish a detection method for 12 kinds of nicotine pesticides in fruits by ultra performance liquid chromatography-tandem mass spectrometry coupled with cold induced liquid-liquid extraction. Methods Fruit samples were extracted using acetonitrile, and after salting out, shaking, and centrifugation, they were subjected to freeze induced liquid-liquid extraction using acetonitrile water solution for further enrichment and purification. Combined with ultra performance liquid chromatography mass spectrometry, data was collected using a multi reaction monitoring mode, and quantified using isotope internal standard method. Results The linear range of 12 kinds of nicotine compounds was 1-500 ng/mL, and the method showed good linearity (r2>0.999). The limits of detection were 2.15-3.60 μg/kg, and the method limits of quantification were 7.11-13.01 μg/kg. The recovery rates of 12 kinds of nicotine compounds were 73.1%-126.7%, and the relative standard deviations were 3.5%-13.3%. Conclusion This method is easy to operate, has high precision, and good stability, and is suitable for screening and detecting nicotine like compounds in fruit samples.
, correspAuthors=Ding-Guo JIANG, Sai FAN, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Qiang LIN, Yun-Kui SHEN, Chao YANG, Mei-Li LI, Jia WANG, Ding-Guo JIANG, Sai FAN), CN=ArticleExt(id=1153986607624474879, articleId=1153986584929096560, tenantId=1146029695717560320, journalId=1149652044408987649, language=CN, title=冷冻诱导液液萃取结合超高效液相色谱-串联质谱法同时检测水果中12种烟碱类农药, columnId=1153429495479521513, journalTitle=食品安全质量检测学报, columnName=本期专题：农兽药残留研究与检测, runingTitle=null, highlight=null, articleAbstract=
目的 建立冷冻诱导液液萃取结合超高效液相色谱-串联质谱法同时检测水果中12种烟碱类农药的检测方法。方法 水果样品使用乙腈提取, 经盐析、振荡、离心后, 使用乙腈-水溶液进行冷冻诱导液液萃取, 进一步富集和净化, 结合超高效液相色谱质谱联用仪, 使用多反应监测模式采集数据, 同位素内标法定量。结果 12种烟碱类化合物在1~500 ng/mL线性范围内方法线性良好(r2>0.999), 检出限为2.15~3.60 μg/kg, 方法定量限为7.11~13.01 μg/kg。12种烟碱类化合物加标回收率为73.1%~126.7%, 相对标准偏差为3.5%~13.3%。结论 该方法操作简便、精密度高、稳定性好, 适用于水果样品中烟碱类化合物的筛查检测工作。
, correspAuthors=蒋定国, 范赛, authorNote=null, correspAuthorsNote=
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, authorsList=林强, 申贇魁, 杨超, 李美丽, 王佳, 蒋定国, 范赛)}, authors=[Author(id=1177987118581297652, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=412163050@qq.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1177987118665183734, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, authorId=1177987118581297652, language=EN, stringName=Qiang LIN, firstName=Qiang, middleName=null, lastName=LIN, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
1, address=1. Beijing Yanqing District Center for Disease Control and Prevention, Beijing 102100, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1177987118723903991, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, authorId=1177987118581297652, language=CN, stringName=林强, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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林强(1986—), 男, 硕士, 副主任医师, 主要研究方向为卫生检验方向。E-mail: 412163050@qq.com
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林强(1986—), 男, 硕士, 副主任医师, 主要研究方向为卫生检验方向。E-mail: 412163050@qq.com
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Analytical Chemistry,
2003,
75: 3019-3030., articleTitle=Strategies for the assessment of matrix effect in quantitative bioanalytical methods based on HPLC-MS/MS, refAbstract=null)], funds=[Fund(id=1177987121462784552, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, awardId=BJSP2021101345, language=CN, fundingSource=北京市食品风险监测项目(BJSP2021101345), fundOrder=null, country=null)], companyList=[AuthorCompany(id=1177987118216393192, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, xref=null, ext=[AuthorCompanyExt(id=1177987118224781801, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, companyId=1177987118216393192, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1. Beijing Yanqing District Center for Disease Control and Prevention, Beijing 102100, China), AuthorCompanyExt(id=1177987118233170410, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, companyId=1177987118216393192, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1.北京市延庆区疾病预防控制中心, 北京 102100)]), AuthorCompany(id=1177987118312862187, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, xref=null, ext=[AuthorCompanyExt(id=1177987118321250796, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, companyId=1177987118312862187, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2. China National Center for Food Safety Risk Assessment, Beijing 100021, China), AuthorCompanyExt(id=1177987118333833709, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, companyId=1177987118312862187, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.国家食品安全风险评估中心, 北京 100021)]), AuthorCompany(id=1177987118417719791, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, xref=null, ext=[AuthorCompanyExt(id=1177987118426108400, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, companyId=1177987118417719791, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3. Beijing Center for Disease Prevention and Control, Beijing Center for Preventive Medicine Research, Beijing 100013, China), AuthorCompanyExt(id=1177987118430302705, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, companyId=1177987118417719791, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3.北京市疾病预防控制中心, 北京市预防医学研究中心, 北京 100013)])], figs=[ArticleFig(id=1177987120594563612, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=EN, label=Fig.1, caption=
Recoveries of different extraction solvents (n=6), figureFileSmall=j2l50NzR3kws+sCiA8ATOA==, figureFileBig=dDYalXMHEufulNiKKsp50A==, tableContent=null), ArticleFig(id=1177987120649089565, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=CN, label=图1, caption=
不同提取试剂的加标回收率(n=6), figureFileSmall=j2l50NzR3kws+sCiA8ATOA==, figureFileBig=dDYalXMHEufulNiKKsp50A==, tableContent=null), ArticleFig(id=1177987120699421214, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=EN, label=Fig.2, caption=
Distribution of enrichment factors for 12 kinds of pesticides under different proportions of acetonitrile water solution, figureFileSmall=+X0nSZ+LKeWh7ds/0NZdOQ==, figureFileBig=NEfRhaZVTQ2dawtQ75GSdQ==, tableContent=null), ArticleFig(id=1177987120762335775, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=CN, label=图2, caption=
12种农药在不同比例乙腈水的富集倍数分布, figureFileSmall=+X0nSZ+LKeWh7ds/0NZdOQ==, figureFileBig=NEfRhaZVTQ2dawtQ75GSdQ==, tableContent=null), ArticleFig(id=1177987120821056032, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=EN, label=Fig.3, caption=
MRM chromatograms of 12 kinds of nicotine pesticides, figureFileSmall=yj+2YxoudipSR36s6jYHEw==, figureFileBig=n2IpLXYXMDE5wo8unU2/3Q==, tableContent=null), ArticleFig(id=1177987120871387681, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=CN, label=图3, caption=
12种烟碱类农药的MRM色谱图 注: FCA. 呋虫胺; XDCA. 烯啶虫胺; SCQ. 噻虫嗪; HYCD. 环氧虫啶; SCA. 噻虫胺; PCL. 吡虫啉; LSL. 氯噻啉; FPFNT. 氟吡呋喃酮; FDCAJ. 氟啶虫胺腈; DCM. 啶虫咪; SCL. 噻虫啉; PCD1. 哌虫啶1; PCD2. 哌虫啶2。
, figureFileSmall=yj+2YxoudipSR36s6jYHEw==, figureFileBig=n2IpLXYXMDE5wo8unU2/3Q==, tableContent=null), ArticleFig(id=1177987120934302242, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=EN, label=Table 1, caption=
Mass spectrum parameters of target compound
, figureFileSmall=null, figureFileBig=null, tableContent=
| 物质名称 | 母离子
(m/z) | 子离子
(m/z) | 碰撞能量
/V | 去簇电压
/V |
| 呋虫胺 | 203.1 | 139.0* | 17 | 40 |
| 157.0 | 13 |
| 烯啶虫胺 | 271.1 | 225.1* | 16 | 30 |
| 136.0 | 40 |
| 噻虫嗪 | 292.0 | 211.1* | 18 | 20 |
| 181.1 | 31 |
| 环氧虫啶 | 323.2 | 136.0* | 50 | 40 |
| 151.1 | 30 |
| 277.0 | 20 |
| 噻虫胺 | 250.0 | 169.1* | 19 | 10 |
| 132.0 | 24 |
| 吡虫啉 | 256.1 | 175.1* | 25 | 20 |
| 209.1 | 22 |
| 氯噻啉 | 262.0 | 181.0* | 20 | 20 |
| 132.1 | 40 |
| 啶虫咪 | 223.1 | 136.0* | 28 | 20 |
| 56.2 | 20 |
| 噻虫啉 | 253.0 | 136.0* | 30 | 20 |
| 90.1 | 50 |
| 哌虫啶1 | 367.2 | 321.2* | 18 | 20 |
| 263.1 | 22 |
| 哌虫啶2 | 367.2 | 306.1* | 35 | 20 |
| 137.1 | 31 |
| 氟啶虫胺腈 | 278.0 | 173.9* | 13 | 20 |
| 153.9 | 40 |
| 氟吡呋喃酮 | 289.0 | 136.1* | 25 | 20 |
| 90.0 | 60 |
| 呋虫胺-D3 | 206.0 | 132.0 | 17 | 20 |
| 噻虫胺-D3 | 253.0 | 172.1 | 17 | 10 |
| 烯啶虫胺-D3 | 274.0 | 228.1 | 17 | 10 |
| 吡虫啉-D4 | 260.1 | 213.1 | 21 | 20 |
| 氯噻啉-D4 | 266.0 | 185.0 | 21 | 10 |
| 啶虫咪-D3 | 226.0 | 136.2 | 30 | 10 |
| 噻虫嗪-D3 | 295.0 | 214.2 | 17 | 20 |
| 噻虫啉-D4 | 257.1 | 136.1 | 30 | 20 |
| 氟啶虫胺腈-D3 | 281.2 | 177.1 | 14 | 20 |
), ArticleFig(id=1177987121013994019, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=CN, label=表1, caption=
目标化合物质谱参数
, figureFileSmall=null, figureFileBig=null, tableContent=
| 物质名称 | 母离子
(m/z) | 子离子
(m/z) | 碰撞能量
/V | 去簇电压
/V |
| 呋虫胺 | 203.1 | 139.0* | 17 | 40 |
| 157.0 | 13 |
| 烯啶虫胺 | 271.1 | 225.1* | 16 | 30 |
| 136.0 | 40 |
| 噻虫嗪 | 292.0 | 211.1* | 18 | 20 |
| 181.1 | 31 |
| 环氧虫啶 | 323.2 | 136.0* | 50 | 40 |
| 151.1 | 30 |
| 277.0 | 20 |
| 噻虫胺 | 250.0 | 169.1* | 19 | 10 |
| 132.0 | 24 |
| 吡虫啉 | 256.1 | 175.1* | 25 | 20 |
| 209.1 | 22 |
| 氯噻啉 | 262.0 | 181.0* | 20 | 20 |
| 132.1 | 40 |
| 啶虫咪 | 223.1 | 136.0* | 28 | 20 |
| 56.2 | 20 |
| 噻虫啉 | 253.0 | 136.0* | 30 | 20 |
| 90.1 | 50 |
| 哌虫啶1 | 367.2 | 321.2* | 18 | 20 |
| 263.1 | 22 |
| 哌虫啶2 | 367.2 | 306.1* | 35 | 20 |
| 137.1 | 31 |
| 氟啶虫胺腈 | 278.0 | 173.9* | 13 | 20 |
| 153.9 | 40 |
| 氟吡呋喃酮 | 289.0 | 136.1* | 25 | 20 |
| 90.0 | 60 |
| 呋虫胺-D3 | 206.0 | 132.0 | 17 | 20 |
| 噻虫胺-D3 | 253.0 | 172.1 | 17 | 10 |
| 烯啶虫胺-D3 | 274.0 | 228.1 | 17 | 10 |
| 吡虫啉-D4 | 260.1 | 213.1 | 21 | 20 |
| 氯噻啉-D4 | 266.0 | 185.0 | 21 | 10 |
| 啶虫咪-D3 | 226.0 | 136.2 | 30 | 10 |
| 噻虫嗪-D3 | 295.0 | 214.2 | 17 | 20 |
| 噻虫啉-D4 | 257.1 | 136.1 | 30 | 20 |
| 氟啶虫胺腈-D3 | 281.2 | 177.1 | 14 | 20 |
), ArticleFig(id=1177987121093685796, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=EN, label=Table 2, caption=
Linear range, correlation coefficients, LODs and LOQs of 12 kinds of nicotine pesticides
, figureFileSmall=null, figureFileBig=null, tableContent=
| 化合物 | 线性范围/(μg/L) | 相关系数(r) | LODs/(μg/kg) | LOQs/(μg/kg) | 同位素内标 |
| 呋虫胺 | 1~500 | 0.9961 | 2.50 | 8.28 | 呋虫胺-D3 |
| 烯啶虫胺 | 1~500 | 0.9992 | 3.13 | 10.30 | 烯啶虫胺-D3 |
| 噻虫嗪 | 1~500 | 0.9995 | 2.60 | 8.84 | 噻虫嗪-D3 |
| 环氧虫啶 | 1~500 | 0.9999 | 3.01 | 9.93 | 烯啶虫胺-D3 |
| 噻虫胺 | 1~500 | 0.9992 | 2.15 | 7.10 | 噻虫胺-D3 |
| 吡虫啉 | 1~500 | 0.9975 | 2.20 | 7.36 | 吡虫啉-D4 |
| 氯噻啉 | 1~500 | 0.9991 | 3.10 | 10.36 | 氯噻啉-D4 |
| 啶虫咪 | 1~500 | 0.9992 | 2.25 | 7.43 | 啶虫脒-D3 |
| 噻虫啉 | 1~500 | 0.9961 | 2.30 | 7.79 | 噻虫啉-D4 |
| 哌虫啶1 | 1~500 | 0.9995 | 2.45 | 8.09 | 噻虫啉-D4 |
| 哌虫啶2 | 1~500 | 0.9985 | 3.40 | 11.45 | 噻虫啉-D4 |
| 氟啶虫胺腈 | 1~500 | 0.9992 | 3.60 | 13.01 | 氟啶虫胺腈-D3 |
| 氟吡呋喃酮 | 1~500 | 0.9975 | 2.54 | 8.38 | 氟啶虫胺腈-D3 |
), ArticleFig(id=1177987121164988965, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=CN, label=表2, caption=
12种烟碱类化合物的线性范围、相关系数、LODs和LOQs
, figureFileSmall=null, figureFileBig=null, tableContent=
| 化合物 | 线性范围/(μg/L) | 相关系数(r) | LODs/(μg/kg) | LOQs/(μg/kg) | 同位素内标 |
| 呋虫胺 | 1~500 | 0.9961 | 2.50 | 8.28 | 呋虫胺-D3 |
| 烯啶虫胺 | 1~500 | 0.9992 | 3.13 | 10.30 | 烯啶虫胺-D3 |
| 噻虫嗪 | 1~500 | 0.9995 | 2.60 | 8.84 | 噻虫嗪-D3 |
| 环氧虫啶 | 1~500 | 0.9999 | 3.01 | 9.93 | 烯啶虫胺-D3 |
| 噻虫胺 | 1~500 | 0.9992 | 2.15 | 7.10 | 噻虫胺-D3 |
| 吡虫啉 | 1~500 | 0.9975 | 2.20 | 7.36 | 吡虫啉-D4 |
| 氯噻啉 | 1~500 | 0.9991 | 3.10 | 10.36 | 氯噻啉-D4 |
| 啶虫咪 | 1~500 | 0.9992 | 2.25 | 7.43 | 啶虫脒-D3 |
| 噻虫啉 | 1~500 | 0.9961 | 2.30 | 7.79 | 噻虫啉-D4 |
| 哌虫啶1 | 1~500 | 0.9995 | 2.45 | 8.09 | 噻虫啉-D4 |
| 哌虫啶2 | 1~500 | 0.9985 | 3.40 | 11.45 | 噻虫啉-D4 |
| 氟啶虫胺腈 | 1~500 | 0.9992 | 3.60 | 13.01 | 氟啶虫胺腈-D3 |
| 氟吡呋喃酮 | 1~500 | 0.9975 | 2.54 | 8.38 | 氟啶虫胺腈-D3 |
), ArticleFig(id=1177987121232097830, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=EN, label=Table 3, caption=
Spiked recoveries and RSDs (%, n=6)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 化合物 | 15 µg/kg | 100 µg/kg | 800 µg/kg |
平均
回收率 | RSDs | 平均
回收率 | RSDs | 平均
回收率 | RSDs |
| 呋虫胺 | 83.2 | 11.7 | 93.6 | 8.9 | 101.6 | 3.5 |
| 烯啶虫胺 | 86.7 | 10.9 | 90.5 | 8.5 | 96.7 | 7.6 |
| 噻虫嗪 | 84.9 | 9.9 | 94.9 | 7.1 | 97.9 | 6.8 |
| 环氧虫啶 | 84.3 | 9.7 | 85.6 | 8.0 | 90.7 | 5.4 |
| 噻虫胺 | 85.1 | 11.0 | 91.6 | 7.4 | 94.2 | 3.8 |
| 吡虫啉 | 85.7 | 10.9 | 92.5 | 6.4 | 95.8 | 6.9 |
| 氯噻啉 | 73.1 | 8.7 | 89.0 | 8.5 | 93.5 | 8.1 |
| 啶虫咪 | 88.8 | 10.2 | 93.2 | 8.3 | 98.8 | 5.8 |
| 噻虫啉 | 85.7 | 10.5 | 98.3 | 8.1 | 97.6 | 7.2 |
| 哌虫啶1 | 80.6 | 9.7 | 99.3 | 5.5 | 90.2 | 3.5 |
| 哌虫啶2 | 91.4 | 11.7 | 89.3 | 7.2 | 96.4 | 6.7 |
| 氟啶虫胺腈 | 83.3 | 11.4 | 97.7 | 6.3 | 94.6 | 5.5 |
| 氟吡呋喃酮 | 126.7 | 13.3 | 94.6 | 8.9 | 102.6 | 3.8 |
), ArticleFig(id=1177987121299206695, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153986584929096560, language=CN, label=表3, caption=
加标回收率与RSDs(%, n=6)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 化合物 | 15 µg/kg | 100 µg/kg | 800 µg/kg |
平均
回收率 | RSDs | 平均
回收率 | RSDs | 平均
回收率 | RSDs |
| 呋虫胺 | 83.2 | 11.7 | 93.6 | 8.9 | 101.6 | 3.5 |
| 烯啶虫胺 | 86.7 | 10.9 | 90.5 | 8.5 | 96.7 | 7.6 |
| 噻虫嗪 | 84.9 | 9.9 | 94.9 | 7.1 | 97.9 | 6.8 |
| 环氧虫啶 | 84.3 | 9.7 | 85.6 | 8.0 | 90.7 | 5.4 |
| 噻虫胺 | 85.1 | 11.0 | 91.6 | 7.4 | 94.2 | 3.8 |
| 吡虫啉 | 85.7 | 10.9 | 92.5 | 6.4 | 95.8 | 6.9 |
| 氯噻啉 | 73.1 | 8.7 | 89.0 | 8.5 | 93.5 | 8.1 |
| 啶虫咪 | 88.8 | 10.2 | 93.2 | 8.3 | 98.8 | 5.8 |
| 噻虫啉 | 85.7 | 10.5 | 98.3 | 8.1 | 97.6 | 7.2 |
| 哌虫啶1 | 80.6 | 9.7 | 99.3 | 5.5 | 90.2 | 3.5 |
| 哌虫啶2 | 91.4 | 11.7 | 89.3 | 7.2 | 96.4 | 6.7 |
| 氟啶虫胺腈 | 83.3 | 11.4 | 97.7 | 6.3 | 94.6 | 5.5 |
| 氟吡呋喃酮 | 126.7 | 13.3 | 94.6 | 8.9 | 102.6 | 3.8 |
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