Article(id=1153433750634483817, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153433737141412332, articleNumber=null, orderNo=null, doi=10.19812/j.cnki.jfsq11-5956/ts.20250116002, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1736956800000, receivedDateStr=2025-01-16, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1752929635914, onlineDateStr=2025-07-19, pubDate=1745510400000, pubDateStr=2025-04-25, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1752929635914, onlineIssueDateStr=2025-07-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1752929635914, creator=13701087609, updateTime=1752929635914, updator=13701087609, issue=Issue{id=1153433737141412332, tenantId=1146029695717560320, journalId=1149652044408987649, year='2025', volume='16', issue='8', pageStart='1', pageEnd='316', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1752929632696, creator=13701087609, updateTime=1757293087150, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1171735391666225233, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153433737141412332, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1171735391666225234, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153433737141412332, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=107, endPage=114, ext={EN=ArticleExt(id=1153433752018604173, articleId=1153433750634483817, tenantId=1146029695717560320, journalId=1149652044408987649, language=EN, title=Rapid screening of 302 kinds of illegal additives in traditional Chinese veterinary medicine by ultra performance liquid chromatography-quadrupole time of flight high resolution-mass spectrometry, columnId=1151895322692776479, journalTitle=Journal of Food Safety & Quality, columnName=Special Topic: Analysis and Monitoring of Toxic and Harmful Substances in Food, runingTitle=null, highlight=null, articleAbstract=
Objective To establish a method based on ultra performance liquid chromatography-quadrupole time of flight high resolution-mass spectrometry (UPLC-Q-TOF-MS) use as a rapid screening method for the illegal addition of 302 kinds of drugs in Chinese veterinary medicine. Methods A high-resolution mass spectrometry database containing information such as the names, molecular formulas, and exact mass numbers of 302 kinds of drugs was established. Samples were extracted with methanol and then analyzed by UPLC-Q-TOF-MS. A sample was considered as a suspected positive if the retention time deviation was less than 0.2 min, the mass error was less than 5 ppm, the isotopic ratio deviation was less than 5%, and the library matching score of the main characteristic fragment ions was greater than 80. Results The method exhibited good selectivity, with a minimum detection concentration as low as 50 ng/mL for the target substances (100 ng/mL for tetracyclines, penicillins, estrogens, and nonsteroidal anti-inflammatory drugs; 200 ng/mL for aminoglycosides). This enabled the efficient screening of 302 kinds of illegally added drugs. In the screening of actual samples, 7 batches of suspected positive samples were detected. Conclusion This approach is applicable for the screening of illegal additives in various veterinary Chinese medicines, providing effective technical support for the quality control of veterinary Chinese medicines.
, correspAuthors=Yan-Ning YANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Jing-Yuan GUAN, Yan-Ning YANG, Da-Ke ZHOU, Xue-Ming LONG, Can ZHOU, Gang ZHANG, Rui-Qi ZHANG, Ju-Fang HU, Shi-Qi LI), CN=ArticleExt(id=1153433773237588772, articleId=1153433750634483817, tenantId=1146029695717560320, journalId=1149652044408987649, language=CN, title=基于超高效液相色谱-四极杆-飞行时间高分辨质谱法快速筛查中兽药中302种药物非法添加, columnId=1151895322898297380, journalTitle=食品安全质量检测学报, columnName=本期专题：食品中有毒有害物质分析与监测, runingTitle=null, highlight=null, articleAbstract=
目的 建立一种基于超高效液相色谱-四极杆-飞行时间高分辨质谱法(ultra performance liquid chromatography-quadrupole time of flight high resolution-mass spectrometry, UPLC-Q-TOF-MS)用于中兽药中的302种药物非法添加的快速筛查方法。方法 建立了包含302种药物名称、分子式、精确质量数等信息的高分辨质谱数据库。样品经甲醇提取后, 经过UPLC-Q-TOF-MS进行数据采集并分析, 当保留时间与数据库绝对偏差<0.2 min, 质量误差<5 ppm, 同位素比值偏差<5%, 且主要特征碎片离子的库比对分数>80时, 认为检出疑似阳性样品。结果 该方法选择性较好, 目标物最低检出质量浓度低至50 ng/mL(四环素类、青霉素类、雌激素类、及非甾体抗炎药检出质量浓度100 ng/mL; 氨基糖苷类检出质量浓度200 ng/mL), 实现了302种非法添加药物的高效筛查。实际样品筛查时, 检出了7批疑似阳性样品。结论 本研究建立的筛查手段具有快速、广谱的特点, 适用于多种中兽药中的非法添加药物的初步筛查, 为中兽药质量控制提供了有效技术支持。
, correspAuthors=杨彦宁, authorNote=null, correspAuthorsNote=
* 杨彦宁(1986—), 女, 硕士, 农艺师, 主要研究方向为兽药饲料畜禽产品药物残留检测及相关技术研究。E-mail:
87200877@qq.com , copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=T79ZnkdEMPu0YxFayk5W8w==, magXml=qo98wjlk63tdxRihAGtB8A==, pdfUrl=null, pdf=cvg+vC4fWhPRQy/2Bwh4dA==, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=Xu40DreaivW7yGndj90LSA==, mapNumber=null, authorCompany=null, fund=null, authors=
关静渊(1996—), 女, 硕士, 兽医师, 主要研究方向为兽医药理学与兽药饲料畜禽产品药物残留检测及相关技术研究。E-mail: 894060595@qq.com
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关静渊(1996—), 女, 硕士, 兽医师, 主要研究方向为兽医药理学与兽药饲料畜禽产品药物残留检测及相关技术研究。E-mail: 894060595@qq.com
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关静渊(1996—), 女, 硕士, 兽医师, 主要研究方向为兽医药理学与兽药饲料畜禽产品药物残留检测及相关技术研究。E-mail: 894060595@qq.com
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Chromatogram of spectinomycin hydrochloride pentahydrate, figureFileSmall=6tU+wBJPHb+1uvsHr+bVsQ==, figureFileBig=utj7295unamq3f4+mWFE5Q==, tableContent=null), ArticleFig(id=1171733883767792514, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=CN, label=图1, caption=
盐酸大观霉素五水合物色谱图, figureFileSmall=6tU+wBJPHb+1uvsHr+bVsQ==, figureFileBig=utj7295unamq3f4+mWFE5Q==, tableContent=null), ArticleFig(id=1171733883843289987, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=EN, label=Fig.2, caption=
Chromatographic profile of budesonide, figureFileSmall=GA3krk7Ew9Iwf8jg8BVunA==, figureFileBig=KqC/tiHtJtwca7Rtd+6w2A==, tableContent=null), ArticleFig(id=1171733883990090628, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=CN, label=图2, caption=
布地奈德色谱图, figureFileSmall=GA3krk7Ew9Iwf8jg8BVunA==, figureFileBig=KqC/tiHtJtwca7Rtd+6w2A==, tableContent=null), ArticleFig(id=1171733884136891269, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=EN, label=Fig.3, caption=
Structures and chromatograms of formoterol fumarate dihydrate and phenylethanolamine A, figureFileSmall=xgzB31EN8tExyB75t93HQw==, figureFileBig=WrWfgzErcSUhh/WJ6Ss9QQ==, tableContent=null), ArticleFig(id=1171733884212388743, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=CN, label=图3, caption=
富马酸福莫特罗二水合物与苯乙醇胺A的结构图与色谱图 注: A. 富马酸福莫特罗二水合物; B. 苯乙醇胺A; C. 色谱图。
, figureFileSmall=xgzB31EN8tExyB75t93HQw==, figureFileBig=WrWfgzErcSUhh/WJ6Ss9QQ==, tableContent=null), ArticleFig(id=1171733884283691913, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=EN, label=Fig.4, caption=
Comparison of characteristic fragment ions of atropine and scopolamine in the fertility-promoting intrauterine infusion liquid with reference standards, figureFileSmall=MtYMcj/faP/CckpAr8t20w==, figureFileBig=vu8tr1USr6WdvV91+02ufQ==, tableContent=null), ArticleFig(id=1171733884350800778, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=CN, label=图4, caption=
促孕灌注液中阿托品和东莨菪碱与对照品特征碎片离子比对图 注: A. 阿托品; B. 东莨菪碱。
, figureFileSmall=MtYMcj/faP/CckpAr8t20w==, figureFileBig=vu8tr1USr6WdvV91+02ufQ==, tableContent=null), ArticleFig(id=1171733884409521036, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=EN, label=Table 1, caption=
Gradient elution of mobile phase
, figureFileSmall=null, figureFileBig=null, tableContent=
| 时间/min | 流动相A/% | 流动相B/% |
| 0 | 95 | 5 |
| 3 | 70 | 30 |
| 8 | 50 | 50 |
| 17 | 5 | 95 |
| 19 | 5 | 95 |
| 19.5 | 95 | 5 |
), ArticleFig(id=1171733884510184334, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=CN, label=表1, caption=
流动相的梯度洗脱
, figureFileSmall=null, figureFileBig=null, tableContent=
| 时间/min | 流动相A/% | 流动相B/% |
| 0 | 95 | 5 |
| 3 | 70 | 30 |
| 8 | 50 | 50 |
| 17 | 5 | 95 |
| 19 | 5 | 95 |
| 19.5 | 95 | 5 |
), ArticleFig(id=1171733884644402064, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=EN, label=Table 2, caption=
Database information of selected compounds (positive ion mode)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 类别 | 中文名称 | 提取离子质荷比 | 保留时间/min | 中文名称 | 提取离子质荷比 | 保留时间/min |
| 喹噁啉类 | 喹烯酮 | 307.1083 | 12.18 | 喹乙醇 | 264.0984 | 5.9 |
| 林可酰胺类 | 盐酸林可霉素 | 407.2220 | 6.34 | 盐酸吡利霉素 | 411.1728 | 8.39 |
| 大环内酯类 | 白霉素 | — | — | 泰乐菌素 | — | — |
| 白霉素A1 | 786.4669 | 13.59 | 泰乐菌素A | 916.5291 | 11.29 |
| 白霉素A5* | 772.4516 | 12.74 | 泰乐菌素B* | 772.4515 | 10.22 |
| 白霉素A7 | 758.4364 | 11.88 | 泰乐菌素C | 902.5124 | 10.77 |
| 白霉素A8 | 786.4319 | 11.76 | 泰乐菌素D | 918.5473 | 10.7 |
| 白霉素A9 | 744.4201 | 11.11 | 螺旋霉素 | — | — |
| 白霉素A13 | 800.4823 | 14.46 | 螺旋霉素Ⅰ | 843.5253 | 8.94 |
| 麦迪霉素A1 | 814.4622 | 13.39 | 螺旋霉素III | 899.5509 | 10.01 |
| 维吉尼霉素 | — | — | 红霉素 | 734.4720 | 10.99 |
| 维吉尼霉素M1 | 526.2576 | 12.07 | 罗红霉素 | 837.5347 | 12.83 |
| 维吉尼霉素S1 | 824.3652 | 14.23 | 泰妙菌素 | 494.3311 | 12.73 |
| 乙酰氨基阿维菌素B1a | 914.5300 | 16.65 | 伊维菌素B1a# | 892.5459 | 18.09 |
| β2-受体激动剂 | 盐酸利托君 | 288.1606 | 6.87 | 盐酸莱克多巴胺* | 302.1766 | 7.68 |
| 富马酸福莫特罗二水合物 | 345.1824 | 8.47 | 盐酸苯氧丙酚胺* | 302.1759 | 9.49 |
| 盐酸克仑特罗 | 277.0877 | 8.93 | 苯乙醇胺A | 345.1814 | 11.9 |
| 硝基呋喃类 | 呋喃他酮 | 325.1158 | 7.02 | 呋喃唑酮* | 226.0463 | 8.81 |
| M胆碱受体阻断药 | 东莨菪碱 | 304.1551 | 6.91 | 阿托品 | 290.1754 | 7.63 |
| 氟喹诺酮类 | 环丙沙星 | 332.1420 | 7.86 | 诺氟沙星 | 320.1421 | 7.67 |
| 磺胺类 | 磺胺氯哒嗪* | 285.0221 | 8.84 | 磺胺氯吡嗪* | 285.0223 | 10.1 |
| 磺胺邻二甲氧嘧啶* | 311.0816 | 9.13 | 磺胺间二甲氧嘧啶* | 311.0815 | 10.37 |
| 磺胺对甲氧嘧啶* | 281.0716 | 8.16 | 磺胺间甲氧嘧啶* | 281.0715 | 8.53 |
| 磺胺二甲嘧啶* | 279.0919 | 7.83 | 磺胺二甲异嘧啶* | 279.0918 | 6.59 |
| 磺胺甲氧哒嗪* | 281.0708 | 7.97 | 磺胺异噁唑* | 268.0765 | 9.56 |
| 磺胺二甲唑* | 268.0753 | 7.55 | 磺胺嘧啶 | 251.0609 | 6.95 |
| 非甾体抗炎药 | 双氯芬酸* | 296.0256 | 14.34 | 依托度酸 | 288.1608 | 14 |
| 吡罗昔康* | 332.0707 | 11.65 | 甲氯芬那酸* | 296.0258 | 15.24 |
| 氟尼辛葡甲胺 | 297.0849 | 13.25 | 异丙氨基比林 | 246.1603 | 6.83 |
| 硝基咪唑类 | 甲硝唑 | 172.0722 | 6.25 | 洛硝哒唑 | 201.0632 | 6.76 |
| 氨基糖苷类 | 硫酸新霉素 | — | — | 硫酸庆大霉素 | — | — |
| 新霉素B | 615.3246 | 7.62 | 硫酸庆大霉素C1 | 478.3256 | 2.65 |
| 新霉胺 | 323.1928 | 13.69 | 硫酸庆大霉素C2 | 464.3100 | 2.65 |
| 盐酸大观霉素五水合物 | 351.1719 | 3.18 | 硫酸庆大霉素C3 | 450.2942 | 2.64 |
| 糖皮质激素类 | 布地奈德 | — | — | 可的松* | 361.2027 | 10.2 |
| 布地奈德 22R* | 431.2450 | 13.01 | 倍他米松* | 393.2090 | 10.88 |
| 布地奈德 22S* | 431.2449 | 13.2 | 地塞米松* | 393.2090 | 10.94 |
| 醋酸双氟拉松* | 495.2202 | 14.73 | 泼尼松龙* | 361.2029 | 9.85 |
| 甲基泼尼松龙 | 375.2184 | 10.67 | 氟轻松* | 495.2198 | 14.58 |
| 性激素类 | 雌酮* | 271.1703 | 13.38 | 双烯雌酚 | 267.1396 | 13.61 |
| α-群勃龙* | 271.1695 | 11.8 | 甲睾酮 | 303.2324 | 13.35 |
| 玉米赤霉酮类 | 玉米烯酮 | 319.1556 | 14.19 | | | |
| 伏马菌素类 | 伏马菌素B1 | 722.3982 | 10.13 | 伏马菌素B2 | 706.4037 | 11.5 |
| 抗病毒类 | 盐酸金刚乙胺* | 180.1753 | 9.16 | 盐酸美金刚* | 180.1753 | 9.51 |
| 离子载体类抗球虫药 | 莫能菌素钠盐 | 693.4215 | 18.46 | 盐霉素钠 | 773.4838 | 17.01 |
| 苯并咪唑类 | 阿苯达唑 | 266.0963 | 11.05 | 阿苯达唑亚砜 | 282.0918 | 7.73 |
| 阿苯达唑砜 | 298.0869 | 9.2 | 芬苯达唑砜* | 332.0715 | 10.85 |
| 头孢菌素类 | 头孢拉定 | 350.1191 | 6.9 | 头孢克洛 | 368.0487 | 6.14 |
| 头孢他啶 | 547.1094 | 6.06 | 头孢匹罗 | 515.1196 | 6.29 |
| 青霉素类 | 阿莫西林三水物 | 366.1135 | 5.78 | 氨苄青霉素三水合物 | 350.1182 | 6.71 |
| 四环素类 | 盐酸金霉素* | 479.1248 | 8.72 | 盐酸四环素 | 445.1635 | 7.61 |
| 多西环素盐酸盐半乙醇半水合物 | 445.1634 | 7.99 | 差向金霉素盐酸盐* | 479.1244 | 8.38 |
| 抗菌增效剂 | 甲氧苄啶 | 291.1452 | 7.29 | | | |
), ArticleFig(id=1171733884791202706, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=CN, label=表2, caption=
部分化合物数据库信息(正离子模式)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 类别 | 中文名称 | 提取离子质荷比 | 保留时间/min | 中文名称 | 提取离子质荷比 | 保留时间/min |
| 喹噁啉类 | 喹烯酮 | 307.1083 | 12.18 | 喹乙醇 | 264.0984 | 5.9 |
| 林可酰胺类 | 盐酸林可霉素 | 407.2220 | 6.34 | 盐酸吡利霉素 | 411.1728 | 8.39 |
| 大环内酯类 | 白霉素 | — | — | 泰乐菌素 | — | — |
| 白霉素A1 | 786.4669 | 13.59 | 泰乐菌素A | 916.5291 | 11.29 |
| 白霉素A5* | 772.4516 | 12.74 | 泰乐菌素B* | 772.4515 | 10.22 |
| 白霉素A7 | 758.4364 | 11.88 | 泰乐菌素C | 902.5124 | 10.77 |
| 白霉素A8 | 786.4319 | 11.76 | 泰乐菌素D | 918.5473 | 10.7 |
| 白霉素A9 | 744.4201 | 11.11 | 螺旋霉素 | — | — |
| 白霉素A13 | 800.4823 | 14.46 | 螺旋霉素Ⅰ | 843.5253 | 8.94 |
| 麦迪霉素A1 | 814.4622 | 13.39 | 螺旋霉素III | 899.5509 | 10.01 |
| 维吉尼霉素 | — | — | 红霉素 | 734.4720 | 10.99 |
| 维吉尼霉素M1 | 526.2576 | 12.07 | 罗红霉素 | 837.5347 | 12.83 |
| 维吉尼霉素S1 | 824.3652 | 14.23 | 泰妙菌素 | 494.3311 | 12.73 |
| 乙酰氨基阿维菌素B1a | 914.5300 | 16.65 | 伊维菌素B1a# | 892.5459 | 18.09 |
| β2-受体激动剂 | 盐酸利托君 | 288.1606 | 6.87 | 盐酸莱克多巴胺* | 302.1766 | 7.68 |
| 富马酸福莫特罗二水合物 | 345.1824 | 8.47 | 盐酸苯氧丙酚胺* | 302.1759 | 9.49 |
| 盐酸克仑特罗 | 277.0877 | 8.93 | 苯乙醇胺A | 345.1814 | 11.9 |
| 硝基呋喃类 | 呋喃他酮 | 325.1158 | 7.02 | 呋喃唑酮* | 226.0463 | 8.81 |
| M胆碱受体阻断药 | 东莨菪碱 | 304.1551 | 6.91 | 阿托品 | 290.1754 | 7.63 |
| 氟喹诺酮类 | 环丙沙星 | 332.1420 | 7.86 | 诺氟沙星 | 320.1421 | 7.67 |
| 磺胺类 | 磺胺氯哒嗪* | 285.0221 | 8.84 | 磺胺氯吡嗪* | 285.0223 | 10.1 |
| 磺胺邻二甲氧嘧啶* | 311.0816 | 9.13 | 磺胺间二甲氧嘧啶* | 311.0815 | 10.37 |
| 磺胺对甲氧嘧啶* | 281.0716 | 8.16 | 磺胺间甲氧嘧啶* | 281.0715 | 8.53 |
| 磺胺二甲嘧啶* | 279.0919 | 7.83 | 磺胺二甲异嘧啶* | 279.0918 | 6.59 |
| 磺胺甲氧哒嗪* | 281.0708 | 7.97 | 磺胺异噁唑* | 268.0765 | 9.56 |
| 磺胺二甲唑* | 268.0753 | 7.55 | 磺胺嘧啶 | 251.0609 | 6.95 |
| 非甾体抗炎药 | 双氯芬酸* | 296.0256 | 14.34 | 依托度酸 | 288.1608 | 14 |
| 吡罗昔康* | 332.0707 | 11.65 | 甲氯芬那酸* | 296.0258 | 15.24 |
| 氟尼辛葡甲胺 | 297.0849 | 13.25 | 异丙氨基比林 | 246.1603 | 6.83 |
| 硝基咪唑类 | 甲硝唑 | 172.0722 | 6.25 | 洛硝哒唑 | 201.0632 | 6.76 |
| 氨基糖苷类 | 硫酸新霉素 | — | — | 硫酸庆大霉素 | — | — |
| 新霉素B | 615.3246 | 7.62 | 硫酸庆大霉素C1 | 478.3256 | 2.65 |
| 新霉胺 | 323.1928 | 13.69 | 硫酸庆大霉素C2 | 464.3100 | 2.65 |
| 盐酸大观霉素五水合物 | 351.1719 | 3.18 | 硫酸庆大霉素C3 | 450.2942 | 2.64 |
| 糖皮质激素类 | 布地奈德 | — | — | 可的松* | 361.2027 | 10.2 |
| 布地奈德 22R* | 431.2450 | 13.01 | 倍他米松* | 393.2090 | 10.88 |
| 布地奈德 22S* | 431.2449 | 13.2 | 地塞米松* | 393.2090 | 10.94 |
| 醋酸双氟拉松* | 495.2202 | 14.73 | 泼尼松龙* | 361.2029 | 9.85 |
| 甲基泼尼松龙 | 375.2184 | 10.67 | 氟轻松* | 495.2198 | 14.58 |
| 性激素类 | 雌酮* | 271.1703 | 13.38 | 双烯雌酚 | 267.1396 | 13.61 |
| α-群勃龙* | 271.1695 | 11.8 | 甲睾酮 | 303.2324 | 13.35 |
| 玉米赤霉酮类 | 玉米烯酮 | 319.1556 | 14.19 | | | |
| 伏马菌素类 | 伏马菌素B1 | 722.3982 | 10.13 | 伏马菌素B2 | 706.4037 | 11.5 |
| 抗病毒类 | 盐酸金刚乙胺* | 180.1753 | 9.16 | 盐酸美金刚* | 180.1753 | 9.51 |
| 离子载体类抗球虫药 | 莫能菌素钠盐 | 693.4215 | 18.46 | 盐霉素钠 | 773.4838 | 17.01 |
| 苯并咪唑类 | 阿苯达唑 | 266.0963 | 11.05 | 阿苯达唑亚砜 | 282.0918 | 7.73 |
| 阿苯达唑砜 | 298.0869 | 9.2 | 芬苯达唑砜* | 332.0715 | 10.85 |
| 头孢菌素类 | 头孢拉定 | 350.1191 | 6.9 | 头孢克洛 | 368.0487 | 6.14 |
| 头孢他啶 | 547.1094 | 6.06 | 头孢匹罗 | 515.1196 | 6.29 |
| 青霉素类 | 阿莫西林三水物 | 366.1135 | 5.78 | 氨苄青霉素三水合物 | 350.1182 | 6.71 |
| 四环素类 | 盐酸金霉素* | 479.1248 | 8.72 | 盐酸四环素 | 445.1635 | 7.61 |
| 多西环素盐酸盐半乙醇半水合物 | 445.1634 | 7.99 | 差向金霉素盐酸盐* | 479.1244 | 8.38 |
| 抗菌增效剂 | 甲氧苄啶 | 291.1452 | 7.29 | | | |
), ArticleFig(id=1171733884975752085, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=EN, label=Table 3, caption=
Database information of compounds (negative ion mode)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 类别 | 中文名称 | 提取离子质荷比 | 保留时间/min | 中文名称 | 提取离子质荷比 | 保留时间/min |
| 基因重组药物 | 多拉菌素 | 897.5017 | 17.44 | | | |
| 磺胺类 | 磺胺硝苯 | 334.0505 | 11.92 | | | |
| 氨基糖苷类 | 阿米卡星 | 584.2789 | 2.63 | | | |
| 雌激素类 | 己烷雌酚* | 269.1553 | 13.82 | 己烯雌酚 | 267.1398 | 14.48 |
| 袢利尿剂 | 呋塞米 | 329.0006 | 11.01 | | | |
| 非甾体抗炎药 | 卡洛芬 | 272.0489 | 14.29 | 菲诺洛芬 | 241.0872 | 13.78 |
| 抗寄生虫类 | 碘醚柳胺 | 623.8128 | 19.62 | 地克珠利 | 404.9727 | 14.77 |
| 尼卡巴嗪 | 301.0583 | 14.6 | 硝米特 | 210.0157 | 8.95 |
| 二硝托胺* | 224.0314 | 9.22 | | | |
| 呋喃类 | 呋喃苯烯酸钠 | 258.0407 | 13.03 | | | |
| 玉米赤霉酮类 | α-玉米赤霉醇* | 321.1707 | 12.77 | β-玉米赤霉醇* | 321.1707 | 12.77 |
| α-玉米赤霉烯醇* | 319.1550 | 12.11 | β-玉米赤霉烯醇* | 319.1550 | 13.12 |
| 玉米赤霉酮* | 319.1550 | 14.06 | | | |
| β-内酰胺酶抑制剂 | 舒巴坦 | 232.0286 | 6.39 | | | |
), ArticleFig(id=1171733885084803991, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153433750634483817, language=CN, label=表3, caption=
化合物数据库信息(负离子模式)
, figureFileSmall=null, figureFileBig=null, tableContent=
| 类别 | 中文名称 | 提取离子质荷比 | 保留时间/min | 中文名称 | 提取离子质荷比 | 保留时间/min |
| 基因重组药物 | 多拉菌素 | 897.5017 | 17.44 | | | |
| 磺胺类 | 磺胺硝苯 | 334.0505 | 11.92 | | | |
| 氨基糖苷类 | 阿米卡星 | 584.2789 | 2.63 | | | |
| 雌激素类 | 己烷雌酚* | 269.1553 | 13.82 | 己烯雌酚 | 267.1398 | 14.48 |
| 袢利尿剂 | 呋塞米 | 329.0006 | 11.01 | | | |
| 非甾体抗炎药 | 卡洛芬 | 272.0489 | 14.29 | 菲诺洛芬 | 241.0872 | 13.78 |
| 抗寄生虫类 | 碘醚柳胺 | 623.8128 | 19.62 | 地克珠利 | 404.9727 | 14.77 |
| 尼卡巴嗪 | 301.0583 | 14.6 | 硝米特 | 210.0157 | 8.95 |
| 二硝托胺* | 224.0314 | 9.22 | | | |
| 呋喃类 | 呋喃苯烯酸钠 | 258.0407 | 13.03 | | | |
| 玉米赤霉酮类 | α-玉米赤霉醇* | 321.1707 | 12.77 | β-玉米赤霉醇* | 321.1707 | 12.77 |
| α-玉米赤霉烯醇* | 319.1550 | 12.11 | β-玉米赤霉烯醇* | 319.1550 | 13.12 |
| 玉米赤霉酮* | 319.1550 | 14.06 | | | |
| β-内酰胺酶抑制剂 | 舒巴坦 | 232.0286 | 6.39 | | | |
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