Article(id=1151437196701037180, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1151437189243089177, articleNumber=null, orderNo=null, doi=10.19812/j.cnki.jfsq11-5956/ts.20250120003, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1737302400000, receivedDateStr=2025-01-20, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1752453620361, onlineDateStr=2025-07-14, pubDate=1749916800000, pubDateStr=2025-06-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1752453620361, onlineIssueDateStr=2025-07-14, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1752453620361, creator=13701087609, updateTime=1752453620361, updator=13701087609, issue=Issue{id=1151437189243089177, tenantId=1146029695717560320, journalId=1149652044408987649, year='2025', volume='16', issue='11', pageStart='1', pageEnd='320', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1752453618584, creator=13701087609, updateTime=1767768054466, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1215670588966883492, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1151437189243089177, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1215670588966883493, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1151437189243089177, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=186, endPage=192, ext={EN=ArticleExt(id=1151895323640689201, articleId=1151437196701037180, tenantId=1146029695717560320, journalId=1149652044408987649, language=EN, title=Determination of 26 kinds of veterinary drug residues in duck meat by ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry, columnId=1151895322692776479, journalTitle=Journal of Food Safety & Quality, columnName=Special Topic: Analysis and Monitoring of Toxic and Harmful Substances in Food, runingTitle=null, highlight=null, articleAbstract=
Objective To establish a method for the simultaneous determination of 26 kinds of veterinary drug residues in 3 categories including sulfonamide, quinolones and tetracyclines based on duck meat by ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry. Methods The 0.1% formic acid acetonitrile extraction was used, QuEChERS purification agent was used to remove impurities. After nitrogen blowing in a 45 ℃ water bath to near dryness, the mixture was diluted with 0.1% formic acid water acetonitrile (1:1, V:V) and analyzed qualitatively and quantitatively using ultra performance liquid chromatography-tandem triple quadrupole mass spectrometry. Results The 26 kinds of veterinary drugs showed good linearity in the range of 2.0-300.0 ng/mL (r2≥0.9996), the limits of detection were 0.28-6.02 μg/kg, the limits of quantification were 11.28-15.03 μg/kg. The average recovery rates of 26 kinds of veterinary drugs at different concentration levels (5.0, 50.0, 300.0 μg/kg) were 75.08%-112.35% (n=15), and the relative standard deviations (RSDs) were 1.25%-7.88% (n=15). Conclusion This method features simple pretreatment operations, high efficiency, and low consumption of reagents and materials. It is suitable for the preliminary screening and detection of 26 kinds of veterinary drug residues in 3 categories for large quantities of duck meat samples.
, correspAuthors=Zhong-Rong WANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Si SUN, Mei YANG, Tai-Yang LIU, Wen-Feng LIU, Zhong-Rong WANG), CN=ArticleExt(id=1151895333384057644, articleId=1151437196701037180, tenantId=1146029695717560320, journalId=1149652044408987649, language=CN, title=超高效液相色谱-串联三重四极杆质谱法测定鸭肉中26种兽药残留, columnId=1151895322898297380, journalTitle=食品安全质量检测学报, columnName=本期专题：食品中有毒有害物质分析与监测, runingTitle=null, highlight=null, articleAbstract=
目的 建立超高效液相色谱-串联三重四极杆质谱法同时测定鸭肉中磺胺类、四环素类、氟喹诺酮类, 共3类26种兽药残留的分析方法。方法 采用0.1%的甲酸-乙腈提取, QuEChERS净化剂除杂, 经45 ℃水浴氮吹至近干后0.1%甲酸水-乙腈(1:1, V:V)定容, 通过超高效液相色谱-串联三重四极杆质谱仪进行定性及定量检测分析。结果 26种兽药在2.0~300.0 ng/mL质量浓度范围内线性关系良好(r2≥0.9996), 检出限为0.28~6.02 μg/kg, 定量限为11.28~15.03 μg/kg。在不同浓度添加水平(5.0、50.0、300.0 μg/kg)下26种兽药的平均回收率为75.08%~112.35% (n=15), 相对标准偏差(relative standard deviations, RSDs)为1.25%~7.88% (n=15)。结论 该方法前处理操作简便, 效率高, 试剂耗材用量小, 适用于大批量鸭肉样品中此3类26种兽药残留的初筛检测。
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57(5): 77-80., articleTitle=食品安全国家标准食品中41个兽药最大残留限量解读, refAbstract=null), Reference(id=1167030702685041071, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, doi=null, pmid=null, pmcid=null, year=2023, volume=57, issue=5, pageStart=77, pageEnd=80, url=null, language=null, rfNumber=[31], rfOrder=61, authorNames=ZHANG YJ, HAO LH, ZHANG L, journalName=Chinese Journal of Veterinary Drug, refType=null, unstructuredReference=
ZHANG YJ,
HAO LH,
ZHANG L,
et al. Decipherment of the national food safety standard maximum residue limits for 41 veterinary drugs in foods[J].
Chinese Journal of Veterinary Drug,
2023,
57(5): 77-80., articleTitle=Decipherment of the national food safety standard maximum residue limits for 41 veterinary drugs in foods, refAbstract=null), Reference(id=1167030702768927153, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, doi=null, pmid=null, pmcid=null, year=2024, volume=58, issue=1, pageStart=29, pageEnd=36, url=null, language=null, rfNumber=[32], rfOrder=62, authorNames=叶妮, 王亦琳, 陈超超, journalName=中国兽药杂志, refType=null, unstructuredReference=叶妮, 王亦琳, 陈超超, 等. 我国限制使用的兽药在食品动物中的残留概况[J].
中国兽药杂志,
2024,
58(1): 29-36., articleTitle=我国限制使用的兽药在食品动物中的残留概况, refAbstract=null), Reference(id=1167030702836036018, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, doi=null, pmid=null, pmcid=null, year=2024, volume=58, issue=1, pageStart=29, pageEnd=36, url=null, language=null, rfNumber=[32], rfOrder=63, authorNames=YE N, WANG YL, CHEN CC, journalName=Chinese Journal of Veterinary Drug, refType=null, unstructuredReference=
YE N,
WANG YL,
CHEN CC,
et al. Overview of residues of restricted veterinary drugs in food animals in China[J].
Chinese Journal of Veterinary Drug,
2024,
58(1): 29-36., articleTitle=Overview of residues of restricted veterinary drugs in food animals in China, refAbstract=null)], funds=null, companyList=[AuthorCompany(id=1167030695894462756, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, xref=1., ext=[AuthorCompanyExt(id=1167030695898657061, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, companyId=1167030695894462756, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
1. Examing and Inspection Center for Agricultural Products Safety and Quality of Qiandongnan Zhou Prefecture, Kaili 556000, China), AuthorCompanyExt(id=1167030695907045670, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, companyId=1167030695894462756, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
1. 黔东州农产品质量安全检测中心, 凯里 556000)]), AuthorCompany(id=1167030695995126056, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, xref=2., ext=[AuthorCompanyExt(id=1167030696003514665, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, companyId=1167030695995126056, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
2. Guizhou Provincial Qiandongnan Center for Animal Disease Control and Prevention, Kaili 556000, China), AuthorCompanyExt(id=1167030696020291882, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, companyId=1167030695995126056, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
2. 黔东南州动物疫病预防控制中心, 凯里 556000)])], figs=[ArticleFig(id=1167030697718985053, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=EN, label=Fig.1, caption=
Recovery rates of 26 kinds of veterinary drug residues under different extraction reagents conditions, figureFileSmall=MKJGWDbsc232ZAD4PXjN3Q==, figureFileBig=ogjkixXYRmEJ2DARFkSq/w==, tableContent=null), ArticleFig(id=1167030697773511007, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=CN, label=图1, caption=
不同提取试剂条件下26种兽药残留的回收率, figureFileSmall=MKJGWDbsc232ZAD4PXjN3Q==, figureFileBig=ogjkixXYRmEJ2DARFkSq/w==, tableContent=null), ArticleFig(id=1167030697836425569, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=EN, label=Fig.2, caption=
Recovery rates of 26 kinds of veterinary drug residues under different purification reagents conditions, figureFileSmall=PzpSDtkC/qs34FkeC1tGvw==, figureFileBig=q9FXGLmj6PWpdLtP9eZaGA==, tableContent=null), ArticleFig(id=1167030697907728739, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=CN, label=图2, caption=
不同净化试剂条件下26种兽药残留的回收率, figureFileSmall=PzpSDtkC/qs34FkeC1tGvw==, figureFileBig=q9FXGLmj6PWpdLtP9eZaGA==, tableContent=null), ArticleFig(id=1167030697974837605, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=EN, label=Table 1, caption=
Liquid phase elution gradient of 26 kinds of veterinary drug residue
, figureFileSmall=null, figureFileBig=null, tableContent=
| 时间/min | 流速/(mL/min) | A/% | B/% |
| 0.00 | 0.3 | 95 | 5 |
| 2.00 | 0.3 | 85 | 15 |
| 5.00 | 0.3 | 60 | 40 |
| 7.00 | 0.3 | 5 | 95 |
| 7.10 | 0.3 | 95 | 5 |
| 9.00 | 0.3 | 95 | 5 |
), ArticleFig(id=1167030698041946471, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=CN, label=表1, caption=
26种兽药残留液相洗脱梯度
, figureFileSmall=null, figureFileBig=null, tableContent=
| 时间/min | 流速/(mL/min) | A/% | B/% |
| 0.00 | 0.3 | 95 | 5 |
| 2.00 | 0.3 | 85 | 15 |
| 5.00 | 0.3 | 60 | 40 |
| 7.00 | 0.3 | 5 | 95 |
| 7.10 | 0.3 | 95 | 5 |
| 9.00 | 0.3 | 95 | 5 |
), ArticleFig(id=1167030698117443944, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=EN, label=Table 2, caption=
Mass spectral parameters of 26 kinds of veterinary drug
, figureFileSmall=null, figureFileBig=null, tableContent=
| 检测指标名称 | 定性离子
对(m/z) | 定量离子
对(m/z) | 锥孔
电压/V | 碰撞
能量/eV |
| 土霉素 | 461.1>426.2 | 461.1>426.2 | 23 | 20 |
| 461.1>443.2 | 13 |
| 金霉素 | 479.1>444.2 | 479.1>444.2 | 27 | 23 |
| 479.1>462.2 | 19 |
| 四环素 | 445.1>410.2 | 445.1>410.2 | 25 | 19 |
| 445.1>427.2 | 13 |
| 多西环素 | 455.1>410.2 | 455.1>428.2 | 24 | 16 |
| 455.1>428.2 | 26 |
| 氟甲喹 | 262.0>202.0 | 262.0>244.0 | 26 | 32 |
| 262.0>244.0 | 18 |
| 恩诺沙星 | 360.2>245.0 | 360.2>316.1 | 34 | 26 |
| 360.2>316.1 | 20 |
| 达氟沙星 | 358.2>96.0 | 358.2>340.2 | 30 | 25 |
| 358.2>340.2 | 23 |
| 培氟沙星 | 334.1>290.1 | 334.1>316.1 | 34 | 18 |
| 334.1>316.1 | 20 |
| 环丙沙星 | 332.1>231.1 | 332.1>231.1 | 31 | 38 |
| 332.1>314.1 | 22 |
| 诺氟沙星 | 320.1>233.0 | 320.1>302.0 | 33 | 25 |
| 320.1>302.0 | 19 |
| 氧氟沙星 | 362.1>261.1 | 362.1>318.1 | 30 | 26 |
| 362.1>318.1 | 20 |
| 洛美沙星 | 352.1>265.1 | 352.1>265.1 | 31 | 22 |
| 352.1>308.1 | 16 |
| 沙拉沙星 | 386.2>299.1 | 386.2>299.1 | 33 | 27 |
| 386.2>342.1 | 20 |
| 磺胺甲噻二唑 | 271.0>92.0 | 271.0>92.0 | 19 | 30 |
| 271.0>156.0 | 15 |
| 磺胺醋酰 | 215.0>156.0 | 215.0>156.0 | 30 | 18 |
| 215.0>108.0 | 28 |
| 磺胺二甲异噁唑 | 268.0>92.0 | 268.0>156.0 | 22 | 28 |
| 268.0>156.0 | 16 |
| 磺胺甲基嘧啶 | 265.0>92.0 | 265.0>156.0 | 24 | 28 |
| 265.0>156.0 | 15 |
| 磺胺二甲嘧啶 | 279.0>92.0 | 279.0>186.0 | 30 | 28 |
| 279.0>186.0 | 16 |
| 磺胺甲氧哒嗪 | 281.0>92.0 | 281.1>156.0 | 26 | 30 |
| 281.0>156.0 | 17 |
| 磺胺甲基异恶唑 | 254.0>156.0 | 254.0>156.0 | 27 | 23 |
| 254.0>147.0 | 22 |
| 磺胺苯吡唑 | 315.0>92.0 | 315.0>158.0 | 30 | 42 |
| 315.0>158.0 | 28 |
| 磺胺嘧啶 | 251.1>92.0 | 251.0>156.0 | 25 | 27 |
| 251.0>156.0 | 15 |
| 磺胺吡啶 | 250.0>108.0 | 250.0>156.0 | 27 | 30 |
| 250.0>156.0 | 26 |
| 磺胺噻唑 | 256.0>92.0 | 256.0>156.0 | 26 | 25 |
| 256.0>156.0 | 15 |
| 磺胺间甲氧嘧啶 | 281.0>92..0 | 281.0>156.0 | 28 | 31 |
| 281.0>156.0 | 22 |
| 磺胺氯哒嗪 | 285.0>92.0 | 285.0>156.0 | 22 | 28 |
| 285.0>156.0 | 15 |
), ArticleFig(id=1167030698197135721, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=CN, label=表2, caption=
26种兽药检测的质谱参数
, figureFileSmall=null, figureFileBig=null, tableContent=
| 检测指标名称 | 定性离子
对(m/z) | 定量离子
对(m/z) | 锥孔
电压/V | 碰撞
能量/eV |
| 土霉素 | 461.1>426.2 | 461.1>426.2 | 23 | 20 |
| 461.1>443.2 | 13 |
| 金霉素 | 479.1>444.2 | 479.1>444.2 | 27 | 23 |
| 479.1>462.2 | 19 |
| 四环素 | 445.1>410.2 | 445.1>410.2 | 25 | 19 |
| 445.1>427.2 | 13 |
| 多西环素 | 455.1>410.2 | 455.1>428.2 | 24 | 16 |
| 455.1>428.2 | 26 |
| 氟甲喹 | 262.0>202.0 | 262.0>244.0 | 26 | 32 |
| 262.0>244.0 | 18 |
| 恩诺沙星 | 360.2>245.0 | 360.2>316.1 | 34 | 26 |
| 360.2>316.1 | 20 |
| 达氟沙星 | 358.2>96.0 | 358.2>340.2 | 30 | 25 |
| 358.2>340.2 | 23 |
| 培氟沙星 | 334.1>290.1 | 334.1>316.1 | 34 | 18 |
| 334.1>316.1 | 20 |
| 环丙沙星 | 332.1>231.1 | 332.1>231.1 | 31 | 38 |
| 332.1>314.1 | 22 |
| 诺氟沙星 | 320.1>233.0 | 320.1>302.0 | 33 | 25 |
| 320.1>302.0 | 19 |
| 氧氟沙星 | 362.1>261.1 | 362.1>318.1 | 30 | 26 |
| 362.1>318.1 | 20 |
| 洛美沙星 | 352.1>265.1 | 352.1>265.1 | 31 | 22 |
| 352.1>308.1 | 16 |
| 沙拉沙星 | 386.2>299.1 | 386.2>299.1 | 33 | 27 |
| 386.2>342.1 | 20 |
| 磺胺甲噻二唑 | 271.0>92.0 | 271.0>92.0 | 19 | 30 |
| 271.0>156.0 | 15 |
| 磺胺醋酰 | 215.0>156.0 | 215.0>156.0 | 30 | 18 |
| 215.0>108.0 | 28 |
| 磺胺二甲异噁唑 | 268.0>92.0 | 268.0>156.0 | 22 | 28 |
| 268.0>156.0 | 16 |
| 磺胺甲基嘧啶 | 265.0>92.0 | 265.0>156.0 | 24 | 28 |
| 265.0>156.0 | 15 |
| 磺胺二甲嘧啶 | 279.0>92.0 | 279.0>186.0 | 30 | 28 |
| 279.0>186.0 | 16 |
| 磺胺甲氧哒嗪 | 281.0>92.0 | 281.1>156.0 | 26 | 30 |
| 281.0>156.0 | 17 |
| 磺胺甲基异恶唑 | 254.0>156.0 | 254.0>156.0 | 27 | 23 |
| 254.0>147.0 | 22 |
| 磺胺苯吡唑 | 315.0>92.0 | 315.0>158.0 | 30 | 42 |
| 315.0>158.0 | 28 |
| 磺胺嘧啶 | 251.1>92.0 | 251.0>156.0 | 25 | 27 |
| 251.0>156.0 | 15 |
| 磺胺吡啶 | 250.0>108.0 | 250.0>156.0 | 27 | 30 |
| 250.0>156.0 | 26 |
| 磺胺噻唑 | 256.0>92.0 | 256.0>156.0 | 26 | 25 |
| 256.0>156.0 | 15 |
| 磺胺间甲氧嘧啶 | 281.0>92..0 | 281.0>156.0 | 28 | 31 |
| 281.0>156.0 | 22 |
| 磺胺氯哒嗪 | 285.0>92.0 | 285.0>156.0 | 22 | 28 |
| 285.0>156.0 | 15 |
), ArticleFig(id=1167030698327159146, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=EN, label=Table 3, caption=
Regression equations and correlation coefficients of 26 kinds of veterinary drugs
, figureFileSmall=null, figureFileBig=null, tableContent=
| 药物名称 | 回归方程 | 相关系数
(r2) | 定量方法 |
| 土霉素 | Y=99188.4X+350.021 | 0.9998 | 外标法 |
| 金霉素 | Y=788882X-3118.788 | 0.9999 | 外标法 |
| 四环素 | Y=15 259.2X+45.362 | 0.9998 | 外标法 |
| 多西环素 | Y=13966.8X+728.001 | 0.9998 | 外标法 |
| 氟甲喹 | Y=3692.44X+852.005 | 0.9998 | 外标法 |
| 恩诺沙星 | Y=956.288X+277.888 | 0.9996 | 外标法 |
| 达氟沙星 | Y=429.002X+218.445 | 0.9998 | 外标法 |
| 培氟沙星 | Y=422.217X-87.8806 | 0.9997 | 外标法 |
| 环丙沙星 | Y=59.997 4X-47.2269 | 0.9997 | 外标法 |
| 诺氟沙星 | Y=296.869X+182.022 | 0.9997 | 外标法 |
| 氧氟沙星 | Y=9985.286X+485.774 | 0.9997 | 外标法 |
| 洛美沙星 | Y=926.858X+10885.69 | 0.9999 | 外标法 |
| 沙拉沙星 | Y=412.336X+215.999 | 0.9998 | 外标法 |
| 磺胺甲噻二唑 | Y=79.702 9X+213.089 | 0.9998 | 外标法 |
| 磺胺醋酰 | Y=169.77X-152.109 | 0.9997 | 外标法 |
| 磺胺二甲异噁唑 | Y=158.5221X+78.8599 | 0.9999 | 外标法 |
| 磺胺甲基嘧啶 | Y=222.498X-102.40 | 0.9999 | 外标法 |
| 磺胺二甲嘧啶 | Y=119.889X-37.7175 | 0.9996 | 外标法 |
| 磺胺甲氧哒嗪 | Y=218.688X+38.2526 | 0.9996 | 外标法 |
| 磺胺甲基异恶唑 | Y=303.632X-139.005 | 0.9997 | 外标法 |
| 磺胺苯吡唑 | Y=298.7X-96.9991 | 0.9997 | 外标法 |
| 磺胺嘧啶 | Y=278.900X-495.766 | 0.9998 | 外标法 |
| 磺胺吡啶 | Y=208.318X-308.766 | 0.9998 | 外标法 |
| 磺胺噻唑 | Y=759522X+112.980 | 0.9998 | 外标法 |
| 磺胺间甲氧嘧啶 | Y=219.56X-188.462 | 0.9999 | 外标法 |
| 磺胺氯哒嗪 | Y=128.758X-118.566 | 0.9998 | 外标法 |
), ArticleFig(id=1167030698461376875, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=CN, label=表3, caption=
26种兽药的回归方程和相关系数
, figureFileSmall=null, figureFileBig=null, tableContent=
| 药物名称 | 回归方程 | 相关系数
(r2) | 定量方法 |
| 土霉素 | Y=99188.4X+350.021 | 0.9998 | 外标法 |
| 金霉素 | Y=788882X-3118.788 | 0.9999 | 外标法 |
| 四环素 | Y=15 259.2X+45.362 | 0.9998 | 外标法 |
| 多西环素 | Y=13966.8X+728.001 | 0.9998 | 外标法 |
| 氟甲喹 | Y=3692.44X+852.005 | 0.9998 | 外标法 |
| 恩诺沙星 | Y=956.288X+277.888 | 0.9996 | 外标法 |
| 达氟沙星 | Y=429.002X+218.445 | 0.9998 | 外标法 |
| 培氟沙星 | Y=422.217X-87.8806 | 0.9997 | 外标法 |
| 环丙沙星 | Y=59.997 4X-47.2269 | 0.9997 | 外标法 |
| 诺氟沙星 | Y=296.869X+182.022 | 0.9997 | 外标法 |
| 氧氟沙星 | Y=9985.286X+485.774 | 0.9997 | 外标法 |
| 洛美沙星 | Y=926.858X+10885.69 | 0.9999 | 外标法 |
| 沙拉沙星 | Y=412.336X+215.999 | 0.9998 | 外标法 |
| 磺胺甲噻二唑 | Y=79.702 9X+213.089 | 0.9998 | 外标法 |
| 磺胺醋酰 | Y=169.77X-152.109 | 0.9997 | 外标法 |
| 磺胺二甲异噁唑 | Y=158.5221X+78.8599 | 0.9999 | 外标法 |
| 磺胺甲基嘧啶 | Y=222.498X-102.40 | 0.9999 | 外标法 |
| 磺胺二甲嘧啶 | Y=119.889X-37.7175 | 0.9996 | 外标法 |
| 磺胺甲氧哒嗪 | Y=218.688X+38.2526 | 0.9996 | 外标法 |
| 磺胺甲基异恶唑 | Y=303.632X-139.005 | 0.9997 | 外标法 |
| 磺胺苯吡唑 | Y=298.7X-96.9991 | 0.9997 | 外标法 |
| 磺胺嘧啶 | Y=278.900X-495.766 | 0.9998 | 外标法 |
| 磺胺吡啶 | Y=208.318X-308.766 | 0.9998 | 外标法 |
| 磺胺噻唑 | Y=759522X+112.980 | 0.9998 | 外标法 |
| 磺胺间甲氧嘧啶 | Y=219.56X-188.462 | 0.9999 | 外标法 |
| 磺胺氯哒嗪 | Y=128.758X-118.566 | 0.9998 | 外标法 |
), ArticleFig(id=1167030698528485740, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=EN, label=Table 4, caption=
Recovery rates and precisions of 26 kinds of veterinary drugs added to duck meat
, figureFileSmall=null, figureFileBig=null, tableContent=
| 药物 | 添加浓度/(μg/kg) | 平均回收率/% | RSDs/% |
| 金霉素 | 5.0 | 79.02 | 3.88 |
| 50.0 | 88.05 | 2.21 |
| 300.0 | 87.23 | 1.25 |
| 土霉素 | 5.0 | 90.03 | 2.03 |
| 50.0 | 95.01 | 1.89 |
| 300.0 | 90.23 | 2.52 |
| 四环素 | 5.0 | 98.05 | 1.76 |
| 50.0 | 98.88 | 1.80 |
| 300.0 | 97.77 | 1.82 |
| 多西环素 | 5.0 | 99.78 | 1.96 |
| 50.0 | 100.03 | 2.01 |
| 300.0 | 99.85 | 2.36 |
| 氟甲喹 | 5.0 | 88.77 | 1.88 |
| 50.0 | 88.23 | 1.85 |
| 300.0 | 87.69 | 2.33 |
| 恩诺沙星 | 5.0 | 92.05 | 3.20 |
| 50.0 | 96.23 | 3.21 |
| 300.0 | 99.85 | 5.14 |
| 达氟沙星 | 5.0 | 89.88 | 3.56 |
| 50.0 | 88.55 | 2.89 |
| 300.0 | 87.59 | 3.02 |
| 培氟沙星 | 5.0 | 99.69 | 1.26 |
| 50.0 | 105.23 | 1.27 |
| 300.0 | 106.02 | 2.01 |
| 环丙沙星 | 5.0 | 101.11 | 1.95 |
| 50.0 | 99.88 | 1.96 |
| 300.0 | 98.56 | 3.01 |
| 诺氟沙星 | 5.0 | 97.23 | 3.05 |
| 50.0 | 97.02 | 3.06 |
| 300.0 | 95.66 | 2.35 |
| 氧氟沙星 | 5.0 | 75.08 | 2.65 |
| 50.0 | 77.23 | 2.88 |
| 300.0 | 78.89 | 3.01 |
| 洛美沙星 | 5.0 | 90.23 | 2.59 |
| 50.0 | 91.22 | 4.62 |
| 300.0 | 95.24 | 4.88 |
| 沙拉沙星 | 5.0 | 88.23 | 4.23 |
| 50.0 | 88.90 | 3.58 |
| 300.0 | 85.62 | 4.23 |
| 磺胺甲噻二唑 | 5.0 | 95.02 | 7.88 |
| 50.0 | 94.23 | 5.63 |
| 300.0 | 93.88 | 5.98 |
| 磺胺醋酰 | 5.0 | 99.68 | 1.85 |
| 50.0 | 98.56 | 1.88 |
| 300.0 | 100.02 | 2.36 |
| 磺胺二甲异恶唑 | 5.0 | 100.03 | 2.58 |
| 50.0 | 110.02 | 2.69 |
| 300.0 | 107.52 | 2.57 |
| 磺胺甲基嘧啶 | 5.0 | 108.63 | 1.89 |
| 50.0 | 99.56 | 1.99 |
| 300.0 | 99.84 | 2.03 |
| 磺胺二甲嘧啶 | 5.0 | 98.88 | 1.95 |
| 50.0 | 99.56 | 3.06 |
| 300.0 | 99.48 | 1.88 |
| 磺胺甲氧哒嗪 | 5.0 | 105.05 | 2.01 |
| 50.0 | 109.56 | 1.96 |
| 300.0 | 112.35 | 1.85 |
| 磺胺甲基异恶唑 | 5.0 | 88.56 | 2.23 |
| 50.0 | 87.26 | 3.01 |
| 300.0 | 89.26 | 3.08 |
| 磺胺苯吡唑 | 5.0 | 95.18 | 2.56 |
| 50.0 | 98.87 | 2.45 |
| 300.0 | 98.99 | 2.31 |
| 磺胺嘧啶 | 5.0 | 96.12 | 1.89 |
| 50.0 | 95.99 | 1.92 |
| 300.0 | 97.56 | 1.98 |
| 磺胺吡啶 | 5.0 | 102.03 | 2.01 |
| 50.0 | 100.06 | 1.89 |
| 300.0 | 100.02 | 1.85 |
| 磺胺噻唑 | 5.0 | 88.56 | 1.95 |
| 50.0 | 89.57 | 1.98 |
| 300.0 | 90.03 | 1.95 |
| 磺胺间甲氧嘧啶 | 5.0 | 99.85 | 5.24 |
| 50.0 | 98.77 | 5.21 |
| 300.0 | 98.25 | 5.23 |
| 磺胺氯哒嗪 | 5.0 | 99.03 | 1.29 |
| 50.0 | 99.26 | 1.60 |
| 300.0 | 99.85 | 2.31 |
), ArticleFig(id=1167030698603983213, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1151437196701037180, language=CN, label=表4, caption=
鸭肉中添加26种兽药回收率和精确度
, figureFileSmall=null, figureFileBig=null, tableContent=
| 药物 | 添加浓度/(μg/kg) | 平均回收率/% | RSDs/% |
| 金霉素 | 5.0 | 79.02 | 3.88 |
| 50.0 | 88.05 | 2.21 |
| 300.0 | 87.23 | 1.25 |
| 土霉素 | 5.0 | 90.03 | 2.03 |
| 50.0 | 95.01 | 1.89 |
| 300.0 | 90.23 | 2.52 |
| 四环素 | 5.0 | 98.05 | 1.76 |
| 50.0 | 98.88 | 1.80 |
| 300.0 | 97.77 | 1.82 |
| 多西环素 | 5.0 | 99.78 | 1.96 |
| 50.0 | 100.03 | 2.01 |
| 300.0 | 99.85 | 2.36 |
| 氟甲喹 | 5.0 | 88.77 | 1.88 |
| 50.0 | 88.23 | 1.85 |
| 300.0 | 87.69 | 2.33 |
| 恩诺沙星 | 5.0 | 92.05 | 3.20 |
| 50.0 | 96.23 | 3.21 |
| 300.0 | 99.85 | 5.14 |
| 达氟沙星 | 5.0 | 89.88 | 3.56 |
| 50.0 | 88.55 | 2.89 |
| 300.0 | 87.59 | 3.02 |
| 培氟沙星 | 5.0 | 99.69 | 1.26 |
| 50.0 | 105.23 | 1.27 |
| 300.0 | 106.02 | 2.01 |
| 环丙沙星 | 5.0 | 101.11 | 1.95 |
| 50.0 | 99.88 | 1.96 |
| 300.0 | 98.56 | 3.01 |
| 诺氟沙星 | 5.0 | 97.23 | 3.05 |
| 50.0 | 97.02 | 3.06 |
| 300.0 | 95.66 | 2.35 |
| 氧氟沙星 | 5.0 | 75.08 | 2.65 |
| 50.0 | 77.23 | 2.88 |
| 300.0 | 78.89 | 3.01 |
| 洛美沙星 | 5.0 | 90.23 | 2.59 |
| 50.0 | 91.22 | 4.62 |
| 300.0 | 95.24 | 4.88 |
| 沙拉沙星 | 5.0 | 88.23 | 4.23 |
| 50.0 | 88.90 | 3.58 |
| 300.0 | 85.62 | 4.23 |
| 磺胺甲噻二唑 | 5.0 | 95.02 | 7.88 |
| 50.0 | 94.23 | 5.63 |
| 300.0 | 93.88 | 5.98 |
| 磺胺醋酰 | 5.0 | 99.68 | 1.85 |
| 50.0 | 98.56 | 1.88 |
| 300.0 | 100.02 | 2.36 |
| 磺胺二甲异恶唑 | 5.0 | 100.03 | 2.58 |
| 50.0 | 110.02 | 2.69 |
| 300.0 | 107.52 | 2.57 |
| 磺胺甲基嘧啶 | 5.0 | 108.63 | 1.89 |
| 50.0 | 99.56 | 1.99 |
| 300.0 | 99.84 | 2.03 |
| 磺胺二甲嘧啶 | 5.0 | 98.88 | 1.95 |
| 50.0 | 99.56 | 3.06 |
| 300.0 | 99.48 | 1.88 |
| 磺胺甲氧哒嗪 | 5.0 | 105.05 | 2.01 |
| 50.0 | 109.56 | 1.96 |
| 300.0 | 112.35 | 1.85 |
| 磺胺甲基异恶唑 | 5.0 | 88.56 | 2.23 |
| 50.0 | 87.26 | 3.01 |
| 300.0 | 89.26 | 3.08 |
| 磺胺苯吡唑 | 5.0 | 95.18 | 2.56 |
| 50.0 | 98.87 | 2.45 |
| 300.0 | 98.99 | 2.31 |
| 磺胺嘧啶 | 5.0 | 96.12 | 1.89 |
| 50.0 | 95.99 | 1.92 |
| 300.0 | 97.56 | 1.98 |
| 磺胺吡啶 | 5.0 | 102.03 | 2.01 |
| 50.0 | 100.06 | 1.89 |
| 300.0 | 100.02 | 1.85 |
| 磺胺噻唑 | 5.0 | 88.56 | 1.95 |
| 50.0 | 89.57 | 1.98 |
| 300.0 | 90.03 | 1.95 |
| 磺胺间甲氧嘧啶 | 5.0 | 99.85 | 5.24 |
| 50.0 | 98.77 | 5.21 |
| 300.0 | 98.25 | 5.23 |
| 磺胺氯哒嗪 | 5.0 | 99.03 | 1.29 |
| 50.0 | 99.26 | 1.60 |
| 300.0 | 99.85 | 2.31 |
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