Article(id=1153429499095015961, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153429493357203682, articleNumber=null, orderNo=null, doi=10.19812/j.cnki.jfsq11-5956/ts.20240812004, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1723392000000, receivedDateStr=2024-08-12, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1752928622268, onlineDateStr=2025-07-19, pubDate=1741968000000, pubDateStr=2025-03-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1752928622268, onlineIssueDateStr=2025-07-19, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1752928622268, creator=13701087609, updateTime=1752928622268, updator=13701087609, issue=Issue{id=1153429493357203682, tenantId=1146029695717560320, journalId=1149652044408987649, year='2025', volume='16', issue='5', pageStart='1', pageEnd='326', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1752928620900, creator=13701087609, updateTime=1758690311058, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1177595773500932351, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153429493357203682, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1177595773500932352, tenantId=1146029695717560320, journalId=1149652044408987649, issueId=1153429493357203682, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=16, endPage=23, ext={EN=ArticleExt(id=1153429499770298907, articleId=1153429499095015961, tenantId=1146029695717560320, journalId=1149652044408987649, language=EN, title=Determination of 25 kinds of illegal additives in candy by dispersive solid phase microextraction extraction-ultra performance liquid chromatography-tandem mass spectrometry, columnId=1153429494888129034, journalTitle=Journal of Food Safety & Quality, columnName=Highlight: Guangzhou Inspection Testing and Certification Group Co., Ltd., runingTitle=null, highlight=null, articleAbstract=

Objective To establish a method for the determination of 25 kinds of illegal additives in candy by dispersive solid phase microextraction extraction coupled with ultra performance liquid chromatography-tandem mass spectrometry. Methods The samples were extracted with 50% methanol water, purified by dispersive solid phase microextraction extraction and separated by ACQUITY UPLC TSS T3 column. The samples were then eluted with ammonium formate aqueous solution and ammonium acetonitrile as mobile phase by gradient elution. The samples were determined by ultra performance liquid chromatography-tandem mass spectrometry and quantified by external standard method. Results The results showed that the 25 kinds of illegal additives had good linearity in the range of 2.00 to 50.00 µg/L with a correlation coefficient (r²) greater than 0.99, recoveries were between 65.1% and 99.3%, relative standard deviations were 1.1% to 5.0%, and limit of detection was 0.05 mg/kg and limit of quantification was 0.10 mg/kg. The method was applied to the detection of 105 batches of samples, in which one batch of compressed candy was found to contain xinlisita, and two batches of candy were found to contain dipropylphenidate. Conclusion The method is purified by dispersive solid phase microextraction extraction and detected by ultra performance liquid chromatography-tandem mass spectrometry. The method has good accuracy and high sensitivity, and can meet the detection requirements of 25 kinds of illegal additives in candy.

, correspAuthors=Jia-Le HUANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Yang CHEN, Xiao-Qing YAO, Min-Heng HE, Xiao-Jia LIN, Hui-Lin CHEN, Jia-Le HUANG), CN=ArticleExt(id=1153429522310489049, articleId=1153429499095015961, tenantId=1146029695717560320, journalId=1149652044408987649, language=CN, title=磁性分散固相微萃取-超高效液相色谱-串联质谱法测定糖果中25种非法添加物, columnId=1153429495039123980, journalTitle=食品安全质量检测学报, columnName=本期重点：广州检验检测认证集团有限公司, runingTitle=null, highlight=null, articleAbstract=

目的 建立磁性分散固相微萃取-超高效液相色谱-串联质谱法测定糖果中25种非法添加物。方法 样品采用50%甲醇水提取, 经磁性分散固相微萃取净化后由ACQUITY UPLC TSS T3色谱柱分离, 以甲酸铵水溶液-酸铵乙腈为流动相进行梯度洗脱, 经超高效液相色谱-串联质谱法测定, 外标法定量。结果 25种非法添加物在2.00~50.00 µg/L范围内线性关系良好, 相关系数(r²)>0.99, 回收率65.1%~99.3%, 相对标准偏差为1.1%~5.0%, 检出限0.05 mg/kg, 定量限0.10 mg/kg。应用该方法对105批次样品进行检测, 其中有1批次压片糖果中检出新利司他, 2批次糖果中检出双丙酚丁。结论 该方法采用磁性分散固相微萃取净化, 超高效液相色谱-串联质谱法检测, 准确性好, 灵敏度高, 能够满足糖果中25种非法添加物的检测需求。

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陈扬(1995—), 男, 硕士, 工程师, 主要研究方向为食品及食品相关产品分析技术。E-mail: 18826077109@163.com

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陈扬(1995—), 男, 硕士, 工程师, 主要研究方向为食品及食品相关产品分析技术。E-mail: 18826077109@163.com

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Journal of Organic Chemistry, 2022(3): 87., articleTitle=Solvation effects in organic chemistry: A short historical overview, refAbstract=null), Reference(id=1177619497226744224, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, doi=null, pmid=null, pmcid=null, year=2019, volume=285, issue=null, pageStart=77, pageEnd=85, url=null, language=null, rfNumber=[34], rfOrder=46, authorNames=XIAN Y, WU Y, DONG H, journalName=Food Chemistry, refType=null, unstructuredReference=XIAN Y, WU Y, DONG H, et al. Modified QuEChERS purification and Fe₃O₄ nanoparticle decoloration for robust analysis of 14 heterocyclic aromatic amines and acrylamide in coffee products using UHPLC-MS/MS[J]. Food Chemistry, 2019, 285: 77-85., articleTitle=Modified QuEChERS purification and Fe₃O₄ nanoparticle decoloration for robust analysis of 14 heterocyclic aromatic amines and acrylamide in coffee products using UHPLC-MS/MS, refAbstract=null)], funds=[Fund(id=1177619493565116785, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, awardId=2023CS03, language=CN, fundingSource=广东省市场监督管理局科技项目(2023CS03), fundOrder=null, country=null)], companyList=[AuthorCompany(id=1177619489748300078, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, xref=null, ext=[AuthorCompanyExt(id=1177619489752494383, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, companyId=1177619489748300078, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1. Guangzhou Inspection Testing and Certification Group Co., Ltd., Guangzhou 511447, China), AuthorCompanyExt(id=1177619489760882992, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, companyId=1177619489748300078, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1.广州检验检测认证集团有限公司, 广州 511447)]), AuthorCompany(id=1177619489819603249, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, xref=null, ext=[AuthorCompanyExt(id=1177619489823797554, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, companyId=1177619489819603249, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2. National Quality Testing Center for Processed Food (Guangdong), Guangzhou 511447, China), AuthorCompanyExt(id=1177619489832186163, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, companyId=1177619489819603249, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.国家加工食品质量检验中心(广东), 广州 511447 )])], figs=[ArticleFig(id=1177619492298436961, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Fig.1, caption=Comparison of extraction effect of extraction solvents, figureFileSmall=NCKQvt095Z3xX9dqG3EvzA==, figureFileBig=o4V42zy2AUOcPZTBAgKc5g==, tableContent=null), ArticleFig(id=1177619492348768610, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=图1, caption=提取溶剂的提取效果比较, figureFileSmall=NCKQvt095Z3xX9dqG3EvzA==, figureFileBig=o4V42zy2AUOcPZTBAgKc5g==, tableContent=null), ArticleFig(id=1177619492411683171, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Fig.2, caption=Effects of ultrasonic time on the recoveries of 25 kinds of illegal additives, figureFileSmall=C2y1+UAjvbXEPL43glb3qg==, figureFileBig=0K7nXCeBiWdtMk0qzpl8cw==, tableContent=null), ArticleFig(id=1177619492470403428, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=图2, caption=超声时间对25种非法添加物回收率的影响, figureFileSmall=C2y1+UAjvbXEPL43glb3qg==, figureFileBig=0K7nXCeBiWdtMk0qzpl8cw==, tableContent=null), ArticleFig(id=1177619492524929381, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Fig.3, caption=Scanning electron microscopy images of the Fe₃O₄/graphene oxide (A) and graphene oxide (B) nanocomposites, figureFileSmall=ipXB98FDOyA0P1QoKKOkXw==, figureFileBig=e+4lrsy+to8EG7rQul/V9w==, tableContent=null), ArticleFig(id=1177619492587843942, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=图3, caption=Fe₃O₄/氧化石墨烯纳米复合材料(A)和氧化石墨烯(B)的扫描电镜图, figureFileSmall=ipXB98FDOyA0P1QoKKOkXw==, figureFileBig=e+4lrsy+to8EG7rQul/V9w==, tableContent=null), ArticleFig(id=1177619492671730023, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Fig.4, caption=Total ion chromatogram of 25 kinds of illegal additives, figureFileSmall=W0JHW7b1ndHx/PJcqHy22w==, figureFileBig=i29RwB3+UeCJe59jVTbm3A==, tableContent=null), ArticleFig(id=1177619492759810408, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=图4, caption=25种非法添加物谱图的总离子流图, figureFileSmall=W0JHW7b1ndHx/PJcqHy22w==, figureFileBig=i29RwB3+UeCJe59jVTbm3A==, tableContent=null), ArticleFig(id=1177619492843696489, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Table 1, caption=

Gradient procedure

, figureFileSmall=null, figureFileBig=null, tableContent=

时间/min	A/%	B/%
0.00	95	5
4.00	95	5
14.00	5	95
18.00	5	95
22.00	95	5
25.00	95	5

), ArticleFig(id=1177619492894028138, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=表1, caption=

洗脱程序

, figureFileSmall=null, figureFileBig=null, tableContent=

时间/min	A/%	B/%
0.00	95	5
4.00	95	5
14.00	5	95
18.00	5	95
22.00	95	5
25.00	95	5

), ArticleFig(id=1177619492944359787, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Table 2, caption=

Mass parameters of 25 kinds of illegal additives compounds

, figureFileSmall=null, figureFileBig=null, tableContent=

目标物	CAS号	化学式	母离子(m/z)	子离子(m/z)	去簇电压/V	碰撞能量/eV
马兜铃酸A	486-84-0	C17H19NO5	359.1	296.0*, 298.1	65	65, 23
马兜铃酸B	467-66-7	C17H19NO5	329.0	268.0*, 294.1	85	85, 18
马兜铃酸C	2447-55-2	C17H19NO5	345.2	282.0*, 310.0	60	60, 23
马兜铃酸D	20325-40-0	C17H19NO5	375.0	297.0*, 312.0	65	65, 43
喜树碱	392973	C20H24N2O4	349.1	305.1*, 220.1	60	60, 32
紫杉醇	33967-61-8	C47H51NO14	852.3	525.2*, 121.1	-60	-60, -19
硫唑嘌呤	69-55-8	C9H7N7S	276.1	158.0*, 117.0	-60	-60, -38
恩曲他滨	132944-85-1	C9H11N3O4	216.2	160.1*, 142.5	60	60, 16
依沙吖啶	54-85-3	C18H19N3O	254.1	226.1*, 197.1	60	60, 35
更昔洛韦	93479-97-1	C9H12N4O4	254.1	150.1*, 133.0	-60	-60, -26
来曲唑	123441-03-0	C17H15Cl2NO2	284.1	242.1*, 127.0	-60	-60, -30
吡喹酮	21399	C22H19N3O	313.2	203.1*, 174.2	60	60, 24
雷莫司琼	98489-61-1	C22H26N2O3	280.2	120.3*, 143.7	60	60, 50
新利司他	28376	C20H14O4S	402.3	180.1*, 178.1	60	60, 40
酚酞	61-68-7	C22H23NO4	319.0	105.0*, 225.0	100	100, 54
比沙可啶	105650-23-5	C35H49NO13	362.1	184.1*, 226.1	60	60, 38
双醋酚丁	59986-10-6	C26H37N3O4	402.1	224.1*, 266.1	120	120, 25
双丙酚丁	63-92-3	C20H22O4	430.1	224.1*, 196.1	100	100, 30
西沙比利	518-28-5	C15H10O5	466.2	234.2*, 434.3	60	60, 33
大黄素	481-74-1	C15H10O5	269.0	225.0*, 240.9	-60	-60, -38
芦荟大黄素	518-82-1	C15H8O6	269.0	239.0*, 182.9	-60	-60, -35
大黄酸	471-53-4	C15H10O6	2850	240.9*, 212.9	-60	-60, -19
大黄酚	517-38-4	C16H12O6	253.0	225.0*, 182.0	-60	-60, -40
大黄素甲醚	76-49-3	C6H14O6	283.3	240.1*, 183.2	-60	-60, -35
拉克替醇	50-84-0	C22H30O4	311.1	182.9*, 196.8	-60	-60, -60

), ArticleFig(id=1177619493049217388, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=表2, caption=

25种非法添加物的质谱参数

, figureFileSmall=null, figureFileBig=null, tableContent=

目标物	CAS号	化学式	母离子(m/z)	子离子(m/z)	去簇电压/V	碰撞能量/eV
马兜铃酸A	486-84-0	C17H19NO5	359.1	296.0*, 298.1	65	65, 23
马兜铃酸B	467-66-7	C17H19NO5	329.0	268.0*, 294.1	85	85, 18
马兜铃酸C	2447-55-2	C17H19NO5	345.2	282.0*, 310.0	60	60, 23
马兜铃酸D	20325-40-0	C17H19NO5	375.0	297.0*, 312.0	65	65, 43
喜树碱	392973	C20H24N2O4	349.1	305.1*, 220.1	60	60, 32
紫杉醇	33967-61-8	C47H51NO14	852.3	525.2*, 121.1	-60	-60, -19
硫唑嘌呤	69-55-8	C9H7N7S	276.1	158.0*, 117.0	-60	-60, -38
恩曲他滨	132944-85-1	C9H11N3O4	216.2	160.1*, 142.5	60	60, 16
依沙吖啶	54-85-3	C18H19N3O	254.1	226.1*, 197.1	60	60, 35
更昔洛韦	93479-97-1	C9H12N4O4	254.1	150.1*, 133.0	-60	-60, -26
来曲唑	123441-03-0	C17H15Cl2NO2	284.1	242.1*, 127.0	-60	-60, -30
吡喹酮	21399	C22H19N3O	313.2	203.1*, 174.2	60	60, 24
雷莫司琼	98489-61-1	C22H26N2O3	280.2	120.3*, 143.7	60	60, 50
新利司他	28376	C20H14O4S	402.3	180.1*, 178.1	60	60, 40
酚酞	61-68-7	C22H23NO4	319.0	105.0*, 225.0	100	100, 54
比沙可啶	105650-23-5	C35H49NO13	362.1	184.1*, 226.1	60	60, 38
双醋酚丁	59986-10-6	C26H37N3O4	402.1	224.1*, 266.1	120	120, 25
双丙酚丁	63-92-3	C20H22O4	430.1	224.1*, 196.1	100	100, 30
西沙比利	518-28-5	C15H10O5	466.2	234.2*, 434.3	60	60, 33
大黄素	481-74-1	C15H10O5	269.0	225.0*, 240.9	-60	-60, -38
芦荟大黄素	518-82-1	C15H8O6	269.0	239.0*, 182.9	-60	-60, -35
大黄酸	471-53-4	C15H10O6	2850	240.9*, 212.9	-60	-60, -19
大黄酚	517-38-4	C16H12O6	253.0	225.0*, 182.0	-60	-60, -40
大黄素甲醚	76-49-3	C6H14O6	283.3	240.1*, 183.2	-60	-60, -35
拉克替醇	50-84-0	C22H30O4	311.1	182.9*, 196.8	-60	-60, -60

), ArticleFig(id=1177619493145686381, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Table 3, caption=

Linear equations, correlation cofficients, limits of detection and limits of quantitation of 25 kinds of illegal additives

, figureFileSmall=null, figureFileBig=null, tableContent=

组分	线性范围/(μg/L)	线性方程	相关系数(r)	检出限/(mg/kg)	定量限/(mg/kg)
马兜铃酸A	2.00~50.00	Y=1162.48X+37957.28	0.9989	0.05	0.10
马兜铃酸B	2.00~50.00	Y=1407.49X-6925.69	0.9918	0.05	0.10
马兜铃酸C	2.00~50.00	Y=1349.15X-11051.90	0.9980	0.05	0.10
马兜铃酸D	2.00~50.00	Y=1254.96X-11349.54	0.9981	0.05	0.10
喜树碱	2.00~50.00	Y=5729.91X-1241.43	0.9990	0.05	0.10
紫杉醇	2.00~50.00	Y=494.86X-3941.95	0.9914	0.05	0.10
硫唑嘌呤	2.00~50.00	Y=576.4X-7451.81	0.9836	0.05	0.10
恩曲他滨	2.00~50.00	Y=761.09X-4810.69	0.9979	0.05	0.10
依沙吖啶	2.00~50.00	Y=1040.3X+37784.76	0.9950	0.05	0.10
更昔洛韦	2.00~50.00	Y=1407.63X-6888.80	0.9976	0.05	0.10
来曲唑	2.00~50.00	Y=1450.2X-10875.66	0.9937	0.05	0.10
吡喹酮	2.00~50.00	Y=1317.61X-11480.07	0.9938	0.05	0.10
雷莫司琼	2.00~50.00	Y=5707.67X-1635.59	0.9976	0.05	0.10
新利司他	2.00~50.00	Y=985.5X-4062.42	0.9987	0.05	0.10
酚酞	2.00~50.00	Y=694.45X-6991.94	0.9912	0.05	0.10
比沙可啶	2.00~50.00	Y=1026.59X-4449.1	0.9938	0.05	0.10
双醋酚丁	2.00~50.00	Y=711.83X-7459.26	0.9945	0.05	0.10
双丙酚丁	2.00~50.00	Y=891.27X-4801.84	0.9970	0.05	0.10
西沙比利	2.00~50.00	Y=998.94X+37791.08	0.9904	0.05	0.10
大黄素	2.00~50.00	Y=1394.42X-6640.81	0.9979	0.05	0.10
芦荟大黄素	2.00~50.00	Y=1444.58X-11099.2	0.9970	0.05	0.10
大黄酸	2.00~50.00	Y=5715.91X-1412.3	0.9933	0.05	0.10
大黄酚	2.00~50.00	Y=909.54X-7427.85	0.9909	0.05	0.10
大黄素甲醚	2.00~50.00	Y=629.52X-4668.76	0.9915	0.05	0.10
拉克替醇	2.00~50.00	Y=948.49X-6932.69	0.9941	0.05	0.10

), ArticleFig(id=1177619493254738286, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=表3, caption=

25种非法添加物的线性方程、相关系数、检出限和定量限

, figureFileSmall=null, figureFileBig=null, tableContent=

组分	线性范围/(μg/L)	线性方程	相关系数(r)	检出限/(mg/kg)	定量限/(mg/kg)
马兜铃酸A	2.00~50.00	Y=1162.48X+37957.28	0.9989	0.05	0.10
马兜铃酸B	2.00~50.00	Y=1407.49X-6925.69	0.9918	0.05	0.10
马兜铃酸C	2.00~50.00	Y=1349.15X-11051.90	0.9980	0.05	0.10
马兜铃酸D	2.00~50.00	Y=1254.96X-11349.54	0.9981	0.05	0.10
喜树碱	2.00~50.00	Y=5729.91X-1241.43	0.9990	0.05	0.10
紫杉醇	2.00~50.00	Y=494.86X-3941.95	0.9914	0.05	0.10
硫唑嘌呤	2.00~50.00	Y=576.4X-7451.81	0.9836	0.05	0.10
恩曲他滨	2.00~50.00	Y=761.09X-4810.69	0.9979	0.05	0.10
依沙吖啶	2.00~50.00	Y=1040.3X+37784.76	0.9950	0.05	0.10
更昔洛韦	2.00~50.00	Y=1407.63X-6888.80	0.9976	0.05	0.10
来曲唑	2.00~50.00	Y=1450.2X-10875.66	0.9937	0.05	0.10
吡喹酮	2.00~50.00	Y=1317.61X-11480.07	0.9938	0.05	0.10
雷莫司琼	2.00~50.00	Y=5707.67X-1635.59	0.9976	0.05	0.10
新利司他	2.00~50.00	Y=985.5X-4062.42	0.9987	0.05	0.10
酚酞	2.00~50.00	Y=694.45X-6991.94	0.9912	0.05	0.10
比沙可啶	2.00~50.00	Y=1026.59X-4449.1	0.9938	0.05	0.10
双醋酚丁	2.00~50.00	Y=711.83X-7459.26	0.9945	0.05	0.10
双丙酚丁	2.00~50.00	Y=891.27X-4801.84	0.9970	0.05	0.10
西沙比利	2.00~50.00	Y=998.94X+37791.08	0.9904	0.05	0.10
大黄素	2.00~50.00	Y=1394.42X-6640.81	0.9979	0.05	0.10
芦荟大黄素	2.00~50.00	Y=1444.58X-11099.2	0.9970	0.05	0.10
大黄酸	2.00~50.00	Y=5715.91X-1412.3	0.9933	0.05	0.10
大黄酚	2.00~50.00	Y=909.54X-7427.85	0.9909	0.05	0.10
大黄素甲醚	2.00~50.00	Y=629.52X-4668.76	0.9915	0.05	0.10
拉克替醇	2.00~50.00	Y=948.49X-6932.69	0.9941	0.05	0.10

), ArticleFig(id=1177619493334430063, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=EN, label=Table 4, caption=

Recoveries and precisions for 25 kinds of illegal additives

, figureFileSmall=null, figureFileBig=null, tableContent=

化合物	0.1 mg/kg		0.2 mg/kg		1.0 mg/kg
	回收率/%	相对标准偏差/%	回收率/%	相对标准偏差/%	回收率/%	相对标准偏差/%
马兜铃酸A	84.1	2.0	82.8	1.9	85.8	4.1
马兜铃酸B	84.0	3.5	84.5	2.3	82.9	2.5
马兜铃酸C	84.3	2.9	88.1	1.3	83.1	3.4
马兜铃酸D	77.4	5.0	75.4	4.7	79.4	4.5
喜树碱	73.3	3.0	69.8	2.8	68.7	2.5
紫杉醇	96.8	4.4	95.2	3.1	99.3	2.6
硫唑嘌呤	86.4	4.7	87.6	1.6	87.1	2.8
恩曲他滨	76.7	4.0	73.7	3.9	77.8	3.8
依沙吖啶	69.4	1.2	65.5	2.3	65.1	3.4
更昔洛韦	69.7	1.8	67.2	3.0	72.3	1.8
来曲唑	83.0	4.0	79.1	3.9	82.6	4.3
吡喹酮	94.1	1.7	94.2	1.7	91.9	2.8
雷莫司琼	76.5	5.0	72.4	2.8	72.0	2.3
新利司他	83.0	4.7	78.2	2.3	79.2	3.9
酚酞	82.7	2.3	85.7	3.1	86.3	3.1
比沙可啶	76.9	3.1	74.5	2.1	74.4	2.1
双醋酚丁	83.5	3.5	81.7	4.9	80.6	3.5
双丙酚丁	81.3	3.4	85.2	2.3	82.3	4.5
西沙比利	89.8	3.8	91.4	2.2	85.3	2.4
大黄素	83.4	4.6	84.6	4.9	80.1	4.5
芦荟大黄素	84.8	3.1	86.4	2.1	81.4	2.0
大黄酸	77.9	2.1	80.1	1.3	79.8	2.3
大黄酚	88.9	3.1	90.2	1.4	85.1	4.9
大黄素甲醚	86.1	4.4	83.2	3.7	84.3	4.3
拉克替醇	89.3	2.1	91.3	1.8	90.8	1.1

), ArticleFig(id=1177619493422510448, tenantId=1146029695717560320, journalId=1149652044408987649, articleId=1153429499095015961, language=CN, label=表4, caption=

25种非法添加物的加标回收率及精密度

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化合物	0.1 mg/kg		0.2 mg/kg		1.0 mg/kg
	回收率/%	相对标准偏差/%	回收率/%	相对标准偏差/%	回收率/%	相对标准偏差/%
马兜铃酸A	84.1	2.0	82.8	1.9	85.8	4.1
马兜铃酸B	84.0	3.5	84.5	2.3	82.9	2.5
马兜铃酸C	84.3	2.9	88.1	1.3	83.1	3.4
马兜铃酸D	77.4	5.0	75.4	4.7	79.4	4.5
喜树碱	73.3	3.0	69.8	2.8	68.7	2.5
紫杉醇	96.8	4.4	95.2	3.1	99.3	2.6
硫唑嘌呤	86.4	4.7	87.6	1.6	87.1	2.8
恩曲他滨	76.7	4.0	73.7	3.9	77.8	3.8
依沙吖啶	69.4	1.2	65.5	2.3	65.1	3.4
更昔洛韦	69.7	1.8	67.2	3.0	72.3	1.8
来曲唑	83.0	4.0	79.1	3.9	82.6	4.3
吡喹酮	94.1	1.7	94.2	1.7	91.9	2.8
雷莫司琼	76.5	5.0	72.4	2.8	72.0	2.3
新利司他	83.0	4.7	78.2	2.3	79.2	3.9
酚酞	82.7	2.3	85.7	3.1	86.3	3.1
比沙可啶	76.9	3.1	74.5	2.1	74.4	2.1
双醋酚丁	83.5	3.5	81.7	4.9	80.6	3.5
双丙酚丁	81.3	3.4	85.2	2.3	82.3	4.5
西沙比利	89.8	3.8	91.4	2.2	85.3	2.4
大黄素	83.4	4.6	84.6	4.9	80.1	4.5
芦荟大黄素	84.8	3.1	86.4	2.1	81.4	2.0
大黄酸	77.9	2.1	80.1	1.3	79.8	2.3
大黄酚	88.9	3.1	90.2	1.4	85.1	4.9
大黄素甲醚	86.1	4.4	83.2	3.7	84.3	4.3
拉克替醇	89.3	2.1	91.3	1.8	90.8	1.1

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