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Synthesis of Flower-Like MoS2@CNT Composites with Expanded Interlayer Spacing and Their Electrochemical Properties
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Li SI, Zhonglin LI, Fengqi LU
Hydrometallurgy of China | 2026, 45(5) : 723 - 733
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Hydrometallurgy of China | 2026, 45(5): 723-733
• Experiment Research •
Synthesis of Flower-Like MoS2@CNT Composites with Expanded Interlayer Spacing and Their Electrochemical Properties
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Li SI, Zhonglin LI, Fengqi LU
Affiliations
  • Department of Materials Science and Engineering, Guilin University of Technology, Guilin　541004, China
Published: 2026-10-20 doi: 10.13355/j.cnki.sfyj.2026.05.012
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A one-step hydrothermal method was employed, using urea (H2NCONH2) as an interlayer modulation agent, to realize the in situ growth of molybdenum disulfide (MoS2) within a three-dimensional conductive network constructed by carbon nanotubes (CNTs). MoS2@CNT composite was prpared and used as anode materials for sodium ion batteries, and theri electrochemical properties investigated. The results indicate that the MoS2@CNT composite materials can effectively alleviate volume expansion during sodium-ion insertion and extraction, thereby improving the sodium storage reaction kinetics and structural stability. Structural characterization results reveal that the incorporation of H2NCONH2 increases the interlayer spacing of MoS2 from 0.62 nm to 0.71 nm, thereby providing additional active sites and shortening ion diffusion pathways. Electrochemical properties test results demonstrate that, after 100 cycles at a current density of 0.1 A/g, the composite maintains a reversible capacity of 387.2 mAh/g, corresponding to a capacity retention rate of 97.5%. Furthermore, after cycling at various current densities, the specific capacity recovers to 402.3 mAh/g, indicating excellent rate capability and superior cycling stability.

sodium ion batteries  /  molybdenum disulfide  /  carbon nanotubes  /  composite materials  /  electrochemical properties  /  preparation
司立, 李中林, 卢锋奇. 具有扩展层间距的花球状MoS2@CNT复合材料的制备及其电化学性能研究. 湿法冶金, 2026 , 45 (5) : 723 -733 . DOI: 10.13355/j.cnki.sfyj.2026.05.012
Li SI, Zhonglin LI, Fengqi LU. Synthesis of Flower-Like MoS2@CNT Composites with Expanded Interlayer Spacing and Their Electrochemical Properties[J]. Hydrometallurgy of China, 2026 , 45 (5) : 723 -733 . DOI: 10.13355/j.cnki.sfyj.2026.05.012
Appendix
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Year 2026 volume 45 Issue 5
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doi: 10.13355/j.cnki.sfyj.2026.05.012
  • Receive Date：2026-04-28
  • Online Date：2026-10-14
  • Published：2026-10-20
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  • Received：2026-04-28
  • Revised：2026-05-25
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    Department of Materials Science and Engineering, Guilin University of Technology, Guilin　541004, China
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https://castjournals.cast.org.cn/joweb/sfyj/EN/10.13355/j.cnki.sfyj.2026.05.012
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表12种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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