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Development of a Doubly Curved Crystal Wavelength Dispersive X-ray Fluorescence Spectrometer and Its Application in Actinide Element Analysis
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Lianwei LIU, Zhiyuan Chang, Chaojie XIONG, Hui WANG, Cheng ZUO
Hydrometallurgy of China | 2025, 44(6) : 833 - 838
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Hydrometallurgy of China | 2025, 44(6): 833-838
• Analysis •
Development of a Doubly Curved Crystal Wavelength Dispersive X-ray Fluorescence Spectrometer and Its Application in Actinide Element Analysis
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Lianwei LIU, Zhiyuan Chang, Chaojie XIONG, Hui WANG, Cheng ZUO
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  • Department of Radiochemistry, China Institute of Atomic Energy, Beijing 102413, China
Published: 2025-12-20 doi: 10.13355/j.cnki.sfyj.2025.06.016
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The precise determination of critical elements such as uranium and plutonium in spent nuclear fuel reprocessing workflows holds paramount significance for process optimization and safety assurance. Building upon international technological precedents, the LiF(200) doubly curved crystal optical element was optimized and selected, and the MWDXRF prototype for quantitative analysis of actinide elements was successfully developed. The results of the diffraction intensity and fluorescence characteristic experiments show that the instrument is feasible for the micro-trace-level analysis of actinide elements, and its detection limit for uranium determination is 18.97 μg/mL. The development of the device provides a new way for novel approaches to the simultaneous determination of trace/ultra-trace actinides in complex matrices.

wavelength dispersive X-ray fluorescence  /  doubly curved crystal  /  actinide elements  /  uranium
刘联伟, 常志远, 熊超杰, 王辉, 左臣. 双曲面弯晶波长色散X射线荧光光谱仪的研制及其测定锕系元素研究. 湿法冶金, 2025 , 44 (6) : 833 -838 . DOI: 10.13355/j.cnki.sfyj.2025.06.016
Lianwei LIU, Zhiyuan Chang, Chaojie XIONG, Hui WANG, Cheng ZUO. Development of a Doubly Curved Crystal Wavelength Dispersive X-ray Fluorescence Spectrometer and Its Application in Actinide Element Analysis[J]. Hydrometallurgy of China, 2025 , 44 (6) : 833 -838 . DOI: 10.13355/j.cnki.sfyj.2025.06.016
Year 2025 volume 44 Issue 6
131
27
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doi: 10.13355/j.cnki.sfyj.2025.06.016
  • Receive Date:2025-04-24
  • Online Date:2026-09-28
  • Published:2025-12-20
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  • Received:2025-04-24
Affiliations
    Department of Radiochemistry, China Institute of Atomic Energy, Beijing 102413, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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