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Preparation of Battery-grade Lithium Carbonate by Shear-assisted Carbonization Method
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Yan ZHANG, Jianguang YANG, Xiaobin FAN, Jiang LIU, Anbang SU, Qiang ZHU, Shiyang TANG
Hydrometallurgy of China | 2024, 43(2) : 189 - 194
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Hydrometallurgy of China | 2024, 43(2): 189-194
Experiment Research
Preparation of Battery-grade Lithium Carbonate by Shear-assisted Carbonization Method
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Yan ZHANG, Jianguang YANG, Xiaobin FAN, Jiang LIU, Anbang SU, Qiang ZHU, Shiyang TANG
Affiliations
  • School of Metallurgy and Environment, Central South University, Changsha 410083, China
Published: 2024-04-20 doi: 10.13355/j.cnki.sfyj.2024.02.013
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Aiming at the problems such as long production cycle, low utilization rate of carbon dioxide and difficult to meet the standard requirements of battery grade lithium carbonate produced by traditional carbonization decomposition method, the preparation of battery grade lithium carbonate by sodium carbonate—shear carbonization—ion exchange—heating decomposition process was studied using low-grade leachite ore as raw material. The results show that the removal rates of calcium, magnesium and manganese are 97.26%, 81.82% and 95.73%, respectively, under the conditions of 30 ℃, liquid volume/solid mass ratio of 25/1, carbon dioxide input rate of 0.5 L/min and shear speed of 6 000 r/min. The shear assisted carbonization method can significantly improve the carbonization reaction rate, shorten the reaction time, save more than 70% of CO2, and is more conducive to the production of battery grade lithium carbonate. The prepared lithium carbonate can meet the standard of battery grade lithium carbonate.

lithium extraction from brine  /  shear enhancement  /  carbide decomposition method  /  preparation  /  battery-grade lithium carbonate  /  calcium  /  manganese  /  magnesium
Yan ZHANG, Jianguang YANG, Xiaobin FAN, Jiang LIU, Anbang SU, Qiang ZHU, Shiyang TANG. Preparation of Battery-grade Lithium Carbonate by Shear-assisted Carbonization Method[J]. Hydrometallurgy of China, 2024 , 43 (2) : 189 -194 . DOI: 10.13355/j.cnki.sfyj.2024.02.013
Year 2024 volume 43 Issue 2
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doi: 10.13355/j.cnki.sfyj.2024.02.013
  • Receive Date:2023-12-21
  • Online Date:2025-09-10
  • Published:2024-04-20
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  • Received:2023-12-21
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    School of Metallurgy and Environment, Central South University, Changsha 410083, China
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表12种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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