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Study on Preparation Optimization and Flotation Desilication Performance of Causticized Starch Based on Response Surface Methodology
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Shuai WANG1, 2, Tingting MA1, 2, Lan ZHOU1, 2, Baoxu SONG1, 2, Peng LI3
Mining Research and Development | 2026, 46(1) : 281 - 289
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Mining Research and Development | 2026, 46(1): 281-289
Study on Preparation Optimization and Flotation Desilication Performance of Causticized Starch Based on Response Surface Methodology
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Shuai WANG1, 2, Tingting MA1, 2, Lan ZHOU1, 2, Baoxu SONG1, 2, Peng LI3
Affiliations
  • 1.School of Mining Engineering, University of Science and Technology Liaoning, Anshan, Liaoning 114051, China
  • 2.Institute of Smart Mining, University of Science and Technology Liaoning, Anshan, Liaoning 114051, China
  • 3.Power Generation Branch of the Energy and Power Plant, Ansteel Group Corporation, Anshan, Liaoning 114021, China
Published: 2026-01-25
Outline
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To improve the inhibition performance of causticized starch and the recovery rate of iron concentrate in the process of reverse flotation desilication of iron ore, the Box-Behnken design of response surface methodology was adopted to systematically investigate the effects of three factors of causticizing time, causticizing temperature and causticizing ratio, as well as their interaction on the recovery rate of iron concentrate. The results show that causticizing temperature exerts the most significant impact on the recovery rate, with the order of significance of influence being: causticizing temperature >causticizing time >causticizing ratio. Among them, the interaction between causticizing temperature and causticizing ratio also has a significant effect. The optimal preparation conditions obtained through optimization are as follows: causticizing temperature of 95 ℃, causticizing time of 80 min, and causticizing ratio of 0.07. Under these conditions, the recovery rate of iron concentrate reaches 63.65%, which is 1.3% higher than that under the initial conditions. Infrared spectroscopy analysis results show that after optimization of preparation conditions, the intensity of O—H, C=O, C—OH and C—O—C characteristic peaks of causticized starch is significantly enhanced, indicating that the intramolecular hydrogen bond network is more stable, the structure is more orderly, and the inhibition performance is significantly improved. The research results verify the effectiveness and reliability of the response surface methodology in the optimization of flotation reagents, and provide a theoretical basis and technical support for the industrial application of causticized starch.

Causticized starch  /  Response surface methodology  /  Reverse flotation of iron ore  /  Process optimization
王帅, 马婷婷, 周兰, 宋宝旭, 李鹏. 基于响应曲面法的苛化淀粉制备优化与浮选脱硅性能研究. 矿业研究与开发, 2026 , 46 (1) : 281 -289 .
Shuai WANG, Tingting MA, Lan ZHOU, Baoxu SONG, Peng LI. Study on Preparation Optimization and Flotation Desilication Performance of Causticized Starch Based on Response Surface Methodology[J]. Mining Research and Development, 2026 , 46 (1) : 281 -289 .
Year 2026 volume 46 Issue 1
28
9
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  • Receive Date:2025-01-26
  • Online Date:2026-10-29
  • Published:2026-01-25
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  • Received:2025-01-26
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Affiliations
    1.School of Mining Engineering, University of Science and Technology Liaoning, Anshan, Liaoning 114051, China
    2.Institute of Smart Mining, University of Science and Technology Liaoning, Anshan, Liaoning 114051, China
    3.Power Generation Branch of the Energy and Power Plant, Ansteel Group Corporation, Anshan, Liaoning 114021, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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