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Experimental Study on Deep Reduction and Iron-Titanium Separation of Titanium-Bearing Hematite Rough Concentrate Based on Thermodynamic Analysis
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Kaixi Zhang1, 2, Gang Wei1, 2, Jiangtao Tian1, 2, Yangyang Ge1, 2, Su Wang1, 2, Yueming Cao1, 2, Mengle Li1
Mining Research and Development | 2026, 46(8) : 316 - 324
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Mining Research and Development | 2026, 46(8): 316-324
Experimental Study on Deep Reduction and Iron-Titanium Separation of Titanium-Bearing Hematite Rough Concentrate Based on Thermodynamic Analysis
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Kaixi Zhang1, 2, Gang Wei1, 2, Jiangtao Tian1, 2, Yangyang Ge1, 2, Su Wang1, 2, Yueming Cao1, 2, Mengle Li1
Affiliations
  • 1.Hebei Geological Experiment and Testing Center, Baoding, Hebei 071052, China
  • 2.Hebei Key Laboratory of Mineral Resources and Ecological Environment Monitoring, Baoding, Hebei 071052, China
Published: 2026-08-25
Outline
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Hematite is the main associated mineral in a rutile ore deposit in Hebei Province. The rutile particles are fine and intergrown with or enclosed by hematite. Conventional magnetic separation has poor separation effect, making it difficult to achieve effective separation of iron and titanium. Reduction roasting has been proven as an effective technological approach for achieving efficient liberation of fine-grained iron ores from associated gangue minerals. A mineral quantitative automatic analysis system and scanning electron microscope (SEM) were adopted to clarify the mineral composition, element distribution and other information of the samples. The combined process of deep reduction and magnetic separation was adopted to treat the titanium-bearing hematite rough concentrate. Thermodynamic calculation was used to simulate the reaction behaviors of iron minerals and gangue minerals during the reduction process. The optimal experimental conditions were determined as follows: reduction temperature of 1 623 K, reduction time of 120 min, C/O molar ratio of 2.0, and magnetic field intensity of 85 mT. Under the optimal conditions, the metallization rate of reduced products reaches 78.94%. The total iron grade and total iron recovery of iron concentrate are 89.08% and 88.39%, respectively. The TiO2 grade and TiO2 recovery of titanium concentrate are 36.67% and 71.88%, respectively, showing favorable mineral processing and smelting indexes.

Rutile ore  /  Titanium-bearing hematite  /  Thermodynamic analysis  /  Deep reduction  /  Magnetic separation  /  Iron-titanium separation
张凯熙, 危刚, 田江涛, 葛阳阳, 王素, 曹月明, 李孟乐. 基于热力学分析的含钛赤铁粗精矿深度还原-铁钛分离试验研究. 矿业研究与开发, 2026 , 46 (8) : 316 -324 .
Kaixi Zhang, Gang Wei, Jiangtao Tian, Yangyang Ge, Su Wang, Yueming Cao, Mengle Li. Experimental Study on Deep Reduction and Iron-Titanium Separation of Titanium-Bearing Hematite Rough Concentrate Based on Thermodynamic Analysis[J]. Mining Research and Development, 2026 , 46 (8) : 316 -324 .
Year 2026 volume 46 Issue 8
48
8
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  • Receive Date:2025-07-25
  • Online Date:2026-10-27
  • Published:2026-08-25
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  • Received:2025-07-25
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Affiliations
    1.Hebei Geological Experiment and Testing Center, Baoding, Hebei 071052, China
    2.Hebei Key Laboratory of Mineral Resources and Ecological Environment Monitoring, Baoding, Hebei 071052, China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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