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Hydrogen Reduction Process for Bayan Obo Niobium Concentrate
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Yanlu ZHAO1, 2, Bo ZHANG1, 2, 3, Chengjun LIU1, 2, Maofa JIANG1, 2
Mining and Metallurgical Engineering | 2024, 44(6) : 112 - 116
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Mining and Metallurgical Engineering | 2024, 44(6): 112-116
METALLURGY
Hydrogen Reduction Process for Bayan Obo Niobium Concentrate
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Yanlu ZHAO1, 2, Bo ZHANG1, 2, 3, Chengjun LIU1, 2, Maofa JIANG1, 2
Affiliations
  • 1.Key Laboratory of Ecological Metallurgy of Multimetallic Minerals, Ministry of Education, Northeastern University, Shenyang 110819, Liaoning, China
  • 2.School of Metallurgy, Northeastern University, Shenyang 110819, Liaoning, China
  • 3.State Key Laboratory of Research and Comprehensive Utilization of Bayan Obo Rare Earth Resource, Baotou Research Institute of Rare Earths, Baotou 014030, Inner Mongolia, China
Published: 2024-12-01 doi: 10.3969/j.issn.0253-6099.2024.06.024
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The occurrence state of key elements of niobium, rare earths, and titanium in Bayan Obo niobium concentrate samples was characterized before and after hydrogen reduction, and effect of hydrogen reduction condition on iron metallization rate was also explored. After 90 min reduction with flow rate of hydrogen at 300 mL/min, and reduction temperatures of 800 ℃, 850 ℃, 900 ℃, 950 ℃, 1 000 ℃, and 1 050 ℃ respectively, the corresponding metallization rates are 89.22%, 85.79%, 82.50%, 80.52%, 72.15%, and 70.64%. It is found that during hydrogen reduction process, most of iron minerals can be reduced to metallic iron, but with temperature rise, the reduction rate of iron minerals decreases due to effect of mineral powder bonding. Niobite, as the main niobium-containing phase, is easily reduced, while aeschynite and niobium-iron rutile are difficult to be reduced; bastnasite, the main rare earth-containing phase, doesn't change, while monazite can undergo thermal decomposition at 1 050 ℃; ilmenite, niobium-iron rutile and aeschynite, as the main titanium-containing phases, are difficult to be reduced.

Bayan Obo deposit  /  niobium  /  hydrogen reduction  /  phase transition  /  rare earth  /  niobite  /  ilmenite
Yanlu ZHAO, Bo ZHANG, Chengjun LIU, Maofa JIANG. Hydrogen Reduction Process for Bayan Obo Niobium Concentrate[J]. Mining and Metallurgical Engineering, 2024 , 44 (6) : 112 -116 . DOI: 10.3969/j.issn.0253-6099.2024.06.024
Year 2024 volume 44 Issue 6
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doi: 10.3969/j.issn.0253-6099.2024.06.024
  • Receive Date:2024-06-07
  • Online Date:2026-03-19
  • Published:2024-12-01
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  • Received:2024-06-07
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Affiliations
    1.Key Laboratory of Ecological Metallurgy of Multimetallic Minerals, Ministry of Education, Northeastern University, Shenyang 110819, Liaoning, China
    2.School of Metallurgy, Northeastern University, Shenyang 110819, Liaoning, China
    3.State Key Laboratory of Research and Comprehensive Utilization of Bayan Obo Rare Earth Resource, Baotou Research Institute of Rare Earths, Baotou 014030, Inner Mongolia, China
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https://castjournals.cast.org.cn/joweb/kygczz/EN/10.3969/j.issn.0253-6099.2024.06.024
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表12种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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