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Preparation and microstructure evolution of AuSn20 solder ball based on pulsated orifice ejection method
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Wei DONG, Fengyue GE, Fumin XU
Journal of Materials Engineering | 2026, 54(9) : 91 - 98
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Journal of Materials Engineering | 2026, 54(9): 91-98
• RESEARCH ARTICLE •
Preparation and microstructure evolution of AuSn20 solder ball based on pulsated orifice ejection method
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Wei DONG, Fengyue GE, Fumin XU
Affiliations
  • School of Materials Science and Engineering,Dalian University of Technology,Dalian 116024,Liaoning,China
Published: 2026-09-20 doi: 10.11868/j.issn.1001-4381.2024.000864
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In the field of electronic packaging, Au-Sn eutectic alloy (AuSn20) serves as key solder materials, and its preparation process directly affects the packaging performance and reliability. However, due to the brittleness of AuSn20, there is currently no efficient method for the preparation of AuSn20 solder balls. This study uses pulsated orifice ejection method to achieve the high precision and consistency of the on-demand preparation of AuSn20 solder balls. The results show that various specifications of AuSn20 solder balls are prepared under optimal process conditions, with the smallest specification being 50 μm, and the maximum standard deviation of the target particle size being 1.58 μm, significantly improving the preparation accuracy. Microstructural analysis reveals that the solder balls are mainly composed of δ-AuSn and ζ'-Au5Sn eutectic phases, with no abnormal new phases observed. After reflow treatment, the composition distribution inside the solder ball tends to be uniform.Interface reaction studies show that due to the synergistic diffusion of Ni atoms in the diffusion barrier layer, a complex intermetallic compounds (Au,Ni)Sn and (Au,Ni)3Sn2 are formed at the interface joint. The AuSn20 solder balls prepared in this study not only achieve precise control of particle size and consistent thermal history, but also show excellent interface stability and structural integrity under simulated service conditions, opening up new application avenues for Au-Sn alloy brazing materials in advanced electronic packaging.

pulsated orifice ejection method  /  AuSn20 alloy  /  solder ball preparation  /  particle size control
董伟, 葛凤跃, 许富民. 脉冲微孔喷射法制备AuSn20焊球及组织演变行为. 材料工程, 2026 , 54 (9) : 91 -98 . DOI: 10.11868/j.issn.1001-4381.2024.000864
Wei DONG, Fengyue GE, Fumin XU. Preparation and microstructure evolution of AuSn20 solder ball based on pulsated orifice ejection method[J]. Journal of Materials Engineering, 2026 , 54 (9) : 91 -98 . DOI: 10.11868/j.issn.1001-4381.2024.000864
Year 2026 volume 54 Issue 9
83
37
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Article Info
doi: 10.11868/j.issn.1001-4381.2024.000864
  • Receive Date:2024-12-25
  • Online Date:2026-10-28
  • Published:2026-09-20
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History
  • Received:2024-12-25
  • Accepted:2025-01-24
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Affiliations
    School of Materials Science and Engineering,Dalian University of Technology,Dalian 116024,Liaoning,China
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表12种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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