The contents of calcium oxide, silicon dioxide, magnesium oxide, phosphorus and sulfur in metallurgical lime are determined by means of fusion sample preparation-X-ray fluorescent spectrometry. The optimum experimental conditions are determined by analyzing the influences of such factors as fusing agent, release agent, dilution ratio, melting time and temperature on the determination results. Meanwhile, the calibration curves of each element are drawn with standard samples and self-made standard samples with appropriate contents as well as the correlation coefficients are all over 0.999. The experimental samples are determined with test methods. The results showed that the measured and theoretical values of each element could meet the requirements of tolerances as well as relative standard deviations of each element in precision experiment were all less than 5%, which was with higher accuracy and precision. The operation of loss on ignition is not needed for preparing fusion samples in this method so that the experimental processes are greatly simplified and work efficiency is effectively improved, which is with certain promotional and application values.
| 科 Family | 属数 Number of genus | 种数 Number of species | 占总种数比例 Percentage of total species (%) | 属 Genus | 种数 Number of species | 占总种数比例 Percentage of total species (%) |
|---|---|---|---|---|---|---|
| 鹅膏菌科Amanitaceae | 2 | 11 | 5.26 | 鹅膏菌属 Amanita | 10 | 4.78 |
| 小菇科 Mycenaceae | 2 | 12 | 5.74 | 丝盖伞属 Inocybe | 5 | 2.39 |
| 多孔菌科 Polyporaceae | 8 | 14 | 6.70 | 蜡蘑属 Laccaria | 5 | 2.39 |
| 红菇科 Russulaceae | 3 | 23 | 11.00 | 小皮伞属 Marasmius | 6 | 2.87 |
| 小菇属 Mycena | 11 | 5.26 | ||||
| 光柄菇属 Pluteus | 5 | 2.39 | ||||
| 红菇属 Russula | 17 | 8.13 | ||||
| 栓菌属 Trametes | 5 | 2.39 |