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Determination of Major and Minor Components in Metallurgical Lime with Fusion Sample Preparation-X-ray Fluorescent Spectrometry
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Li-rong Hao, Jing-tao Zhou, Zhi-feng Sun, Fang Tian, Rui-xia Yang
Science & Technology of Baotou Steel | 2023, 49(5) : 94 - 98
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Science & Technology of Baotou Steel | 2023, 49(5): 94-98
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Determination of Major and Minor Components in Metallurgical Lime with Fusion Sample Preparation-X-ray Fluorescent Spectrometry
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Li-rong Hao, Jing-tao Zhou, Zhi-feng Sun, Fang Tian, Rui-xia Yang
Affiliations
  • Chemical Inspection Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
Published: 2023-10-25
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The contents of calcium oxide, silicon dioxide, magnesium oxide, phosphorus and sulfur in metallurgical lime are determined by means of fusion sample preparation-X-ray fluorescent spectrometry. The optimum experimental conditions are determined by analyzing the influences of such factors as fusing agent, release agent, dilution ratio, melting time and temperature on the determination results. Meanwhile, the calibration curves of each element are drawn with standard samples and self-made standard samples with appropriate contents as well as the correlation coefficients are all over 0.999. The experimental samples are determined with test methods. The results showed that the measured and theoretical values of each element could meet the requirements of tolerances as well as relative standard deviations of each element in precision experiment were all less than 5%, which was with higher accuracy and precision. The operation of loss on ignition is not needed for preparing fusion samples in this method so that the experimental processes are greatly simplified and work efficiency is effectively improved, which is with certain promotional and application values.

X-ray fluorescence spectrum analysis  /  metallurgical lime  /  glass melting method
Li-rong Hao, Jing-tao Zhou, Zhi-feng Sun, Fang Tian, Rui-xia Yang. Determination of Major and Minor Components in Metallurgical Lime with Fusion Sample Preparation-X-ray Fluorescent Spectrometry[J]. Science & Technology of Baotou Steel, 2023 , 49 (5) : 94 -98 .
Year 2023 volume 49 Issue 5
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  • Receive Date:2023-03-01
  • Online Date:2025-11-21
  • Published:2023-10-25
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  • Received:2023-03-01
Affiliations
    Chemical Inspection Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
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表12种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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