The sample is dissolved by acid, residue is precipitated and filtered, the mixed flux of anhydrous sodium carbonate and boric acid is melted as well as it is mixed with acid dissolving test solution and the constant volume process is carried out. The contents of Si, Mn, P, Al and Cu in ferrotitanium are determined with the ICP-AES, the analytical spectral lines of elements to be determined and working parameters of instrument are optimized with this method as well as the disturbing effects of matrix elements Ti and Fe are investigated. The disturbing effects are eliminated with the mode of matrix matching and detection limit of the method is 0.000 3%~0.002 7%. The standard samples are determined with this method as well as measured values are consistent with certified values of all compositions, relative standard deviation (RSD, n=11) is 0.85%~9.03%, which could meet the analysis requirements of ferrotitanium.
| 科 Family | 属数 Number of genus | 种数 Number of species | 占总种数比例 Percentage of total species (%) | 属 Genus | 种数 Number of species | 占总种数比例 Percentage of total species (%) |
|---|---|---|---|---|---|---|
| 鹅膏菌科Amanitaceae | 2 | 11 | 5.26 | 鹅膏菌属 Amanita | 10 | 4.78 |
| 小菇科 Mycenaceae | 2 | 12 | 5.74 | 丝盖伞属 Inocybe | 5 | 2.39 |
| 多孔菌科 Polyporaceae | 8 | 14 | 6.70 | 蜡蘑属 Laccaria | 5 | 2.39 |
| 红菇科 Russulaceae | 3 | 23 | 11.00 | 小皮伞属 Marasmius | 6 | 2.87 |
| 小菇属 Mycena | 11 | 5.26 | ||||
| 光柄菇属 Pluteus | 5 | 2.39 | ||||
| 红菇属 Russula | 17 | 8.13 | ||||
| 栓菌属 Trametes | 5 | 2.39 |