首页 期刊 论文 学科刊群 资讯 加盟 关于
EN
image
Article(id=1236689045900808590, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236689043514257626, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=1656000000000, acceptedDateStr=2022-06-24, onlineDate=1772779245114, onlineDateStr=2026-03-06, pubDate=1680105600000, pubDateStr=2023-03-30, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772779245114, onlineIssueDateStr=2026-03-06, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772779245114, creator=13701087609, updateTime=1772779245114, updator=13701087609, issue=Issue{id=1236689043514257626, tenantId=1146029695717560320, journalId=1235980733773295621, year='2023', volume='32', issue='6', pageStart='553', pageEnd='656', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772779244545, creator=13701087609, updateTime=1772779562627, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236690377705575144, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236689043514257626, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236690377705575145, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236689043514257626, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=638, endPage=642, ext={EN=ArticleExt(id=1236689046169244048, articleId=1236689045900808590, tenantId=1146029695717560320, journalId=1235980733773295621, language=EN, title=Study on the quality standard of Shashen Zhike Decoction Powder, columnId=null, journalTitle=Chinese Journal of New Drugs, columnName=null, runingTitle=null, highlight=null, articleAbstract=
Objective:

To improve the quality standards of Mongolian medicine Shashen Zhike Decoction Powder.

Methods:

TLC method was used to establish the identification of Bistortae Rhizoma and Shikonin, and the identification of Glycyrrhizae Radix et Rhizoma was revised. The content determination of glycyrrhizic acid was established by reversed phase HPLC.

Results:

The TLC identification methods resulted in clear spots of Bistortae Rhizoma, Shikonin and Glycyrrhizae Radix Et Rhizoma, without interference for the negative control. Glycyrrhizic acid had good linear relationship in the range from 92.90 to 1 161.25 ng (r=0.999 9). The average recovery was 102.57%, and the RSD was 1.85% (n=9).

Conclusion:

The method is simple, specific, stable and repeatable, and can be used for the quality evaluation and control of Shashen Zhike Decoction Powder.

, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Dong WANG, Fei-fan YANG, Bao-feng GUO), CN=ArticleExt(id=1236689046467039636, articleId=1236689045900808590, tenantId=1146029695717560320, journalId=1235980733773295621, language=CN, title=蒙药沙参止咳汤散质量标准提高研究, columnId=1236330556003242277, journalTitle=中国新药杂志, columnName=实验研究, runingTitle=null, highlight=null, articleAbstract=
目的：

对蒙药沙参止咳汤散的质量标准进行完善和提高。

方法：

采用TLC法建立拳参、紫草茸的鉴别项，修订甘草鉴别项；采用反相高效液相色谱法建立甘草酸的含量测定项。

结果：

甘草、拳参、紫草茸薄层鉴别方法斑点清晰，阴性对照无干扰：甘草酸在92.90~1 161.25 ng（r=1.000 0）范围内呈良好的线性关系，平均回收率为102.5%，RSD为1.85%（n=9）。

结论：

新建立的方法简单易行、专属性强、稳定性好、重复性好，可用于沙参止咳汤散的质量评价和控制。

, correspAuthors=null, authorNote=null, correspAuthorsNote=
郭宝凤，女，副主任药师，硕士研究生，主要从事中蒙药标准及质量的研究。E-mail: 。
, copyrightStatement=null, copyrightOwner=《中国新药杂志》有限公司, extLink=null, articleAbsUrl=null, sourceXml=Mw1tXLppFTpyCkB6nmkR5Q==, magXml=jSmfWNdFSN8IBVEfX3ihpQ==, pdfUrl=null, pdf=9Jxoh0BFgxQ3bTOq/XewFw==, pdfFileSize=12645019, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=YhoyIsGamXDLKYQgCnF/kQ==, mapNumber=null, authorCompany=null, fund=null, authors=

王栋，男，副主任中药师，大学本科，主要从事药品标准及质量的研究。E-mail: 。

, authorsList=王栋, 杨非凡, 郭宝凤)}, authors=[Author(id=1236689048576774575, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=233419826@qq.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1236689048685826486, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, authorId=1236689048576774575, language=EN, stringName=Dong WANG, firstName=Dong, middleName=null, lastName=WANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, 2, address=1Inner Mongolia Autonomous Region Drug Inspection and Research Institute, Hohhot 010010, China
2Inner Mongolia Autonomous Region, China-Mongolia Medicine Standard Research Key Laboratory, Hohhot 010010, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1236689048794878399, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, authorId=1236689048576774575, language=CN, stringName=王栋, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, 2, address=1内蒙古自治区药品检验研究院，呼和浩特 010010
2内蒙古自治区中蒙药标准研究重点实验室，呼和浩特 010010, bio={"content":"

王栋，男，副主任中药师，大学本科，主要从事药品标准及质量的研究。E-mail: 。

"}, bioImg=null, bioContent=

王栋，男，副主任中药师，大学本科，主要从事药品标准及质量的研究。E-mail: 。

, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1236689048211870110, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=1, ext=[AuthorCompanyExt(id=1236689048220258719, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048211870110, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1Inner Mongolia Autonomous Region Drug Inspection and Research Institute, Hohhot 010010, China), AuthorCompanyExt(id=1236689048232841632, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048211870110, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1内蒙古自治区药品检验研究院，呼和浩特 010010)]), AuthorCompany(id=1236689048316727715, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=2, ext=[AuthorCompanyExt(id=1236689048383836580, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048316727715, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2Inner Mongolia Autonomous Region, China-Mongolia Medicine Standard Research Key Laboratory, Hohhot 010010, China), AuthorCompanyExt(id=1236689048392225189, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048316727715, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2内蒙古自治区中蒙药标准研究重点实验室，呼和浩特 010010)])]), Author(id=1236689048916513223, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, orderNo=1, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1236689049029759438, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, authorId=1236689048916513223, language=EN, stringName=Fei-fan YANG, firstName=Fei-fan, middleName=null, lastName=YANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=3, address=3Hohhot Inspection and Testing Center, Hohhot 010010, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1236689049130422739, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, authorId=1236689048916513223, language=CN, stringName=杨非凡, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=3, address=3呼和浩特市检验检测中心，呼和浩特 010010, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1236689048471916966, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=3, ext=[AuthorCompanyExt(id=1236689048480305575, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048471916966, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3Hohhot Inspection and Testing Center, Hohhot 010010, China), AuthorCompanyExt(id=1236689048488694184, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048471916966, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3呼和浩特市检验检测中心，呼和浩特 010010)])]), Author(id=1236689049231086047, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, orderNo=2, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=guobaofengzf@163.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1236689049327555049, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, authorId=1236689049231086047, language=EN, stringName=Bao-feng GUO, firstName=Bao-feng, middleName=null, lastName=GUO, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, 2, address=1Inner Mongolia Autonomous Region Drug Inspection and Research Institute, Hohhot 010010, China
2Inner Mongolia Autonomous Region, China-Mongolia Medicine Standard Research Key Laboratory, Hohhot 010010, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1236689049453384179, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, authorId=1236689049231086047, language=CN, stringName=郭宝凤, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, 2, address=1内蒙古自治区药品检验研究院，呼和浩特 010010
2内蒙古自治区中蒙药标准研究重点实验室，呼和浩特 010010, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1236689048211870110, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=1, ext=[AuthorCompanyExt(id=1236689048220258719, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048211870110, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1Inner Mongolia Autonomous Region Drug Inspection and Research Institute, Hohhot 010010, China), AuthorCompanyExt(id=1236689048232841632, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048211870110, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1内蒙古自治区药品检验研究院，呼和浩特 010010)]), AuthorCompany(id=1236689048316727715, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=2, ext=[AuthorCompanyExt(id=1236689048383836580, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048316727715, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2Inner Mongolia Autonomous Region, China-Mongolia Medicine Standard Research Key Laboratory, Hohhot 010010, China), AuthorCompanyExt(id=1236689048392225189, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048316727715, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2内蒙古自治区中蒙药标准研究重点实验室，呼和浩特 010010)])])], keywords=[Keyword(id=1236689049579213310, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=EN, orderNo=1, keyword=Shashen Zhike Decoction Powder), Keyword(id=1236689049658905096, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=EN, orderNo=2, keyword=TLC), Keyword(id=1236689049759568396, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=EN, orderNo=3, keyword=HPLC), Keyword(id=1236689049868620313, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=EN, orderNo=4, keyword=quality standards), Keyword(id=1236689049969283616, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=CN, orderNo=1, keyword=沙参止咳汤散), Keyword(id=1236689050028003878, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=CN, orderNo=2, keyword=TLC法), Keyword(id=1236689050107695661, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=CN, orderNo=3, keyword=HPLC法), Keyword(id=1236689050178998837, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, language=CN, orderNo=4, keyword=质量标准)], refs=null, funds=[Fund(id=1236689050296439361, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, awardId=49, language=CN, fundingSource=《中华人民共和国药典》药品标准提高：沙参止咳汤散项目(49), fundOrder=null, country=null)], companyList=[AuthorCompany(id=1236689048211870110, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=1, ext=[AuthorCompanyExt(id=1236689048220258719, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048211870110, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1Inner Mongolia Autonomous Region Drug Inspection and Research Institute, Hohhot 010010, China), AuthorCompanyExt(id=1236689048232841632, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048211870110, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1内蒙古自治区药品检验研究院，呼和浩特 010010)]), AuthorCompany(id=1236689048316727715, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=2, ext=[AuthorCompanyExt(id=1236689048383836580, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048316727715, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2Inner Mongolia Autonomous Region, China-Mongolia Medicine Standard Research Key Laboratory, Hohhot 010010, China), AuthorCompanyExt(id=1236689048392225189, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048316727715, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2内蒙古自治区中蒙药标准研究重点实验室，呼和浩特 010010)]), AuthorCompany(id=1236689048471916966, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, xref=3, ext=[AuthorCompanyExt(id=1236689048480305575, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048471916966, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3Hohhot Inspection and Testing Center, Hohhot 010010, China), AuthorCompanyExt(id=1236689048488694184, tenantId=1146029695717560320, journalId=1235980733773295621, articleId=1236689045900808590, companyId=1236689048471916966, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=3呼和浩特市检验检测中心，呼和浩特 010010)])], figs=null, attaches=null, journal=Journal(id=1235980159023624194, delFlag=0, nameCn=中国新药杂志, nameEn=Chinese Journal of New Drugs, nameHistory1=null, nameHistory2=null, issn=1003-3734, eissn=null, cn=11-2850/R, coden=ZXZHA6, periodic=3, language=CN, oaType=null, ccby=null, superviseOffice=null, ownerOffice=null, pubOffice=null, editorOffice=null, officeType=null, aims=null, clcCode=null, officeProv=null, officeCity=null, officeAddr=null, officeZip=null, officeEmail=null, officePhone=null, editDirector=null, officeDirector=null, officeDirectorPhone=null, officeStaffNum=null, officeEmpNum=null, coverPicUrl=ohPEEN//Vz1tDT3ZBNTp4Q==, journalPrice=null, startedYear=null, abbrevIsoEn=Chinese Journal of New Drugs, journalRemark=null, publicationField=null, createdTime=1772610233314, updatedTime=1772610649152, createdBy=18614031015, updatedBy=13701087609, firstLetterCn=C, firstLetterEn=C, subjectCode=Life Sciences, subjectName=null, subjectCodeEn=Life Sciences, subjectNameEn=null, picCn=ohPEEN//Vz1tDT3ZBNTp4Q==, picEn=f9WK9bvTM4guTmS/iGhOMg==, jcr=null, cjcr=null, exts=[JournalExt(id=1235981903275290962, language=CN, name=中国新药杂志, nameHistory1=null, nameHistory2=null, managedBy=, sponsoredBy=, publishedBy=, editorOffice=, officeProv=null, officeCity=null, officeAddr=, officeZip=, editDirector=, officeDirector=null, officePhone=null, coverPicUrl=null, journalRemark=, submitArticleUrl=null, websiteUrl=, createdTime=1772610649174, updatedTime=1772610649174, createdBy=13701087609, updatedBy=13701087609, submissionGuidelinesUrl=, submissionAuthorUrl=http://draft.newdrug.cn/journalx_zgxy/authorLogOn.action, submissionEditorUrl=http://draft.newdrug.cn/journalx_zgxy/editorLogOn.action, submissionReviewUrl=http://draft.newdrug.cn/journalx_zgxy/expertLogOn.action, submissionCeEditorUrl=, submissionAeEditorUrl=, option={"copyright":""}), JournalExt(id=1235981903338205523, language=EN, name=Chinese Journal of New Drugs, nameHistory1=null, nameHistory2=null, managedBy=, sponsoredBy=, publishedBy=, editorOffice=, officeProv=null, officeCity=null, officeAddr=, officeZip=, editDirector=, officeDirector=null, officePhone=null, coverPicUrl=null, journalRemark=, submitArticleUrl=null, websiteUrl=, createdTime=1772610649189, updatedTime=1772610649189, createdBy=13701087609, updatedBy=13701087609, submissionGuidelinesUrl=, submissionAuthorUrl=http://draft.newdrug.cn/journalx_zgxy/authorLogOn.action, submissionEditorUrl=http://draft.newdrug.cn/journalx_zgxy/editorLogOn.action, submissionReviewUrl=http://draft.newdrug.cn/journalx_zgxy/expertLogOn.action, submissionCeEditorUrl=, submissionAeEditorUrl=, option={"copyright":""})], databaseList=null, tenantJournalId=1235980733773295621, websiteList=[Website(id=1235982099191222761, webName=null, webTitle=null, webDomain=null, webCopyrigh=null, webIpcNo=null, seoTitle=null, seoKeywords=null, seoDescription=null, tenantJournalId=null, journalId=1235980733773295621, journalNameCn=null, journalNameEn=null, grayFlag=null, tenantId=1146029695717560320, platformId=null, journalGroupId=null, journalGroupNameCn=null, journalGroupNameEn=null, type=1, domain=https://castjournals.cast.org.cn/joweb/zgxyzz/CN, language=CN, createTime=1772610695884, createBy=18614031015, updateTime=1772610860397, updateBy=18614031015, name=中国新药杂志-中文, tplId=1146099689490845704, title=中国新药杂志, delFlag=0, indexPage=/home, props=[WebsiteProps(id=1235983918629966444, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=articleTextType, value=kx, createTime=1772611129672, updateTime=1772611129672, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918604800617, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=banner, value=null, createTime=1772611129666, updateTime=1772611129666, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918655132271, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=grayFlag, value=0, createTime=1772611129678, updateTime=1772611129678, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918596412008, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=logo, value=https://castjournals.cast.org.cn/joweb/zgxyzz/CN/file/pic?fileId=W567vm71kFC7UhK9TSU6xw==, createTime=1772611129664, updateTime=1772611129664, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918667715185, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=minRunFlag, value=0, createTime=1772611129681, updateTime=1772611129681, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918617383531, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=picServerUrl, value=https://castjournals.cast.org.cn/joweb/zgxyzz/CN/file/pic, createTime=1772611129669, updateTime=1772611129669, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918659326576, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=silenceFlag, value=0, createTime=1772611129679, updateTime=1772611129679, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918613189226, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=staticResourcePath, value=https://castjournals.cast.org.cn/joweb/cast_kjdb_cn_619/, createTime=1772611129668, updateTime=1772611129668, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918634160749, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=themeColor, value=null, createTime=1772611129673, updateTime=1772611129673, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983918646743662, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099191222761, code=themeStyle, value=null, createTime=1772611129676, updateTime=1772611129676, creator=18614031015, updator=18614031015)]), Website(id=1235982099270914542, webName=null, webTitle=null, webDomain=null, webCopyrigh=null, webIpcNo=null, seoTitle=null, seoKeywords=null, seoDescription=null, tenantJournalId=null, journalId=1235980733773295621, journalNameCn=null, journalNameEn=null, grayFlag=null, tenantId=1146029695717560320, platformId=null, journalGroupId=null, journalGroupNameCn=null, journalGroupNameEn=null, type=1, domain=https://castjournals.cast.org.cn/joweb/zgxyzz/EN, language=EN, createTime=1772610695903, createBy=18614031015, updateTime=1772610875891, updateBy=18614031015, name=中国新药杂志-英文, tplId=1146101810881728533, title=Chinese Journal of New Drugs, delFlag=0, indexPage=/home, props=[WebsiteProps(id=1235983955829248630, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=articleTextType, value=kx, createTime=1772611138541, updateTime=1772611138541, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955804082803, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=banner, value=null, createTime=1772611138535, updateTime=1772611138535, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955854414457, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=grayFlag, value=0, createTime=1772611138547, updateTime=1772611138547, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955795694194, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=logo, value=https://castjournals.cast.org.cn/joweb/zgxyzz/EN/file/pic?fileId=W567vm71kFC7UhK9TSU6xw==, createTime=1772611138533, updateTime=1772611138533, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955866997371, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=minRunFlag, value=0, createTime=1772611138550, updateTime=1772611138550, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955820860021, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=picServerUrl, value=https://castjournals.cast.org.cn/joweb/zgxyzz/EN/file/pic, createTime=1772611138539, updateTime=1772611138539, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955862803066, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=silenceFlag, value=0, createTime=1772611138549, updateTime=1772611138549, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955812471412, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=staticResourcePath, value=https://castjournals.cast.org.cn/joweb/cast_kjdb_en_623/, createTime=1772611138537, updateTime=1772611138537, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955837637239, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=themeColor, value=null, createTime=1772611138543, updateTime=1772611138543, creator=18614031015, updator=18614031015), WebsiteProps(id=1235983955846025848, tenantId=1146029695717560320, journalId=null, journalGroupId=null, siteId=1235982099270914542, code=themeStyle, value=null, createTime=1772611138545, updateTime=1772611138545, creator=18614031015, updator=18614031015)])], journalTitle=中国新药杂志, weixinUrl=null, journalUrl=http://www.newdrug.cn/, iacademicId=null, status=1, seqNo=null, journalTitleEn=Chinese Journal of New Drugs, journalPhotoCn=ohPEEN//Vz1tDT3ZBNTp4Q==, journalPhotoEn=f9WK9bvTM4guTmS/iGhOMg==, journalFirstLetter=C, journalRecommend=null, journalNew=null, journalCollection=null, jcrJf=null, cjcrJf=null, jcrJfStr=null, cjcrJfStr=null, submissionFirstDecision=null, sciSubjectClassification=null, casSubjectClassification=null, citeScore=null, totalCitationFrequency=null, icpCode=null, psCode=null, advertisingLicenseCode=null, copyrightInformation=null, country=null, option=, provinceCode=null, provinceName=null, collectFlag=false), detailUrlCn=https://castjournals.cast.org.cn/joweb/zgxyzz/CN/Y2023/V32/I6/638, detailUrlEn=https://castjournals.cast.org.cn/joweb/zgxyzz/EN/Y2023/V32/I6/638, pdfUrlCn=https://castjournals.cast.org.cn/joweb/zgxyzz/CN/PDF/Y2023/V32/I6/638, pdfUrlEn=https://castjournals.cast.org.cn/joweb/zgxyzz/EN/PDF/Y2023/V32/I6/638, aliStartDate=null, aliEndDate=null, collectionFlag=false, citedCount=null, citedUrl=null, reference=null)
收藏切换
蒙药沙参止咳汤散质量标准提高研究
收藏切换
PDF下载
王栋 1, 2 , 杨非凡 3 , 郭宝凤 1, 2
中国新药杂志 | 实验研究 2023,32(6): 638-642
收起
收藏切换
中国新药杂志 | 实验研究 2023, 32(6): 638-642
蒙药沙参止咳汤散质量标准提高研究
全屏
王栋1, 2 , 杨非凡3, 郭宝凤1, 2
作者信息
  • 1内蒙古自治区药品检验研究院，呼和浩特 010010
  • 2内蒙古自治区中蒙药标准研究重点实验室，呼和浩特 010010
  • 3呼和浩特市检验检测中心，呼和浩特 010010

    • 王栋，男，副主任中药师，大学本科，主要从事药品标准及质量的研究。E-mail: 。

通讯作者:

郭宝凤，女，副主任药师，硕士研究生，主要从事中蒙药标准及质量的研究。E-mail: 。
Study on the quality standard of Shashen Zhike Decoction Powder
Dong WANG1, 2 , Fei-fan YANG3, Bao-feng GUO1, 2
Affiliations
  • 1Inner Mongolia Autonomous Region Drug Inspection and Research Institute, Hohhot 010010, China
  • 2Inner Mongolia Autonomous Region, China-Mongolia Medicine Standard Research Key Laboratory, Hohhot 010010, China
  • 3Hohhot Inspection and Testing Center, Hohhot 010010, China
出版时间: 2023-03-30
文章导航
收藏切换
摘要
收起
目的：

对蒙药沙参止咳汤散的质量标准进行完善和提高。

方法：

采用TLC法建立拳参、紫草茸的鉴别项，修订甘草鉴别项；采用反相高效液相色谱法建立甘草酸的含量测定项。

结果：

甘草、拳参、紫草茸薄层鉴别方法斑点清晰，阴性对照无干扰：甘草酸在92.90~1 161.25 ng（r=1.000 0）范围内呈良好的线性关系，平均回收率为102.5%，RSD为1.85%（n=9）。

结论：

新建立的方法简单易行、专属性强、稳定性好、重复性好，可用于沙参止咳汤散的质量评价和控制。

沙参止咳汤散  /  TLC法  /  HPLC法  /  质量标准
Objective:

To improve the quality standards of Mongolian medicine Shashen Zhike Decoction Powder.

Methods:

TLC method was used to establish the identification of Bistortae Rhizoma and Shikonin, and the identification of Glycyrrhizae Radix et Rhizoma was revised. The content determination of glycyrrhizic acid was established by reversed phase HPLC.

Results:

The TLC identification methods resulted in clear spots of Bistortae Rhizoma, Shikonin and Glycyrrhizae Radix Et Rhizoma, without interference for the negative control. Glycyrrhizic acid had good linear relationship in the range from 92.90 to 1 161.25 ng (r=0.999 9). The average recovery was 102.57%, and the RSD was 1.85% (n=9).

Conclusion:

The method is simple, specific, stable and repeatable, and can be used for the quality evaluation and control of Shashen Zhike Decoction Powder.

Shashen Zhike Decoction Powder  /  TLC  /  HPLC  /  quality standards
王栋, 杨非凡, 郭宝凤. 蒙药沙参止咳汤散质量标准提高研究. 中国新药杂志, 2023 , 32 (6) : 638 -642 .
Dong WANG, Fei-fan YANG, Bao-feng GUO. Study on the quality standard of Shashen Zhike Decoction Powder[J]. Chinese Journal of New Drugs, 2023 , 32 (6) : 638 -642 .
基金
收起
  • 《中华人民共和国药典》药品标准提高：沙参止咳汤散项目(49)
2023年第32卷第6期
PDF下载
40
17
引用本文
BibTeX
文章信息
  • 首发时间：2026-03-06
  • 出版时间：2023-03-30
补充材料
相关文章
文章信息
作者
出版历史
  • 录用日期：2022-06-24
基金
《中华人民共和国药典》药品标准提高：沙参止咳汤散项目(49)
作者信息
    1内蒙古自治区药品检验研究院，呼和浩特 010010
    2内蒙古自治区中蒙药标准研究重点实验室，呼和浩特 010010
    3呼和浩特市检验检测中心，呼和浩特 010010

通讯作者:

郭宝凤，女，副主任药师，硕士研究生，主要从事中蒙药标准及质量的研究。E-mail: 。
参考文献
分享链接
https://castjournals.cast.org.cn/joweb/zgxyzz/CN/1236689045900808590
分享至
全文二维码

扫描看全文

引用本文
BibTeX
本文的引用情况
2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
关闭全屏
相关链接
论文
最新文章
热读文章
热点专题
内参
蓝皮书
产业发展报告
传播力报告
期刊分级目录
资讯
学术新闻
行业新闻
学术会议
行业会议
关于
关于我们
联系我们
北京市海淀区学院南路86号
100081
010-62199257
qkjq@cast.org.cn

中国科学技术协会版权所有 京ICP 备10216604号-4 海淀分局备案 1101084647
科技导报社主办 中国科协信息中心技术支持