Article(id=1236687124519506751, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236687122619495346, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=1652630400000, acceptedDateStr=2022-05-16, onlineDate=1772778787021, onlineDateStr=2026-03-06, pubDate=1682784000000, pubDateStr=2023-04-30, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772778787021, onlineIssueDateStr=2026-03-06, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772778787021, creator=13701087609, updateTime=1772778787021, updator=13701087609, issue=Issue{id=1236687122619495346, tenantId=1146029695717560320, journalId=1235980733773295621, year='2023', volume='32', issue='8', pageStart='761', pageEnd='864', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772778786568, creator=13701087609, updateTime=1772779118928, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236688516713861515, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236687122619495346, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236688516713861516, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236687122619495346, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=826, endPage=834, ext={EN=ArticleExt(id=1236687126088176452, articleId=1236687124519506751, tenantId=1146029695717560320, journalId=1235980733773295621, language=EN, title=Recent advances in sample preparation and analysis methods for vitamin D in different matrices, columnId=null, journalTitle=Chinese Journal of New Drugs, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Vitamin D is an essential fat-soluble vitamin, which plays a very important role in maintaining the dynamic balance of calcium in human body and can prevent calcium deficiency diseases such as osteoporosis and rickets. Both excess and deficiency of vitamin D pose a threat to human health, so it is necessary to establish methods for monitoring vitamin D concentrations in different matrices (e.g., pharmaceuticals, foods, biological samples, etc.). However, due to the unstable chemical properties of vitamin D and the complex matrix of vitamin D-containing samples, the pre-treatment and determination of vitamin D-containing samples have a great challenge. This paper reviews the research progress of pretreatment and determination of vitamin D in different matrices in recent years. It is reported that the most commonly used pretreatment methods are liquid-liquid extraction, solid-phase extraction and liquid-liquid microextraction, and the determination methods mainly include high performance liquid chromatography, mass spectrometry, supercritical fluid chromatography and other methods. This review is expected to provide technical support for the determination of vitamin D series preparations.

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维生素D是一种人体必需的脂溶性维生素，在维持人体内钙的动态平衡方面起着非常重要的作用，可预防骨质疏松、佝偻病等钙缺乏疾病。维生素D过量或缺乏都会对人体健康产生严重威胁，因此有必要建立监测不同基质（如药品、食品、生物样品等）中维生素D浓度的方法。但维生素D化学性质不稳定且含维生素D的样品基质大多较为复杂，因此含维生素D样品的前处理以及测定具有较大挑战。本文综述了近年来不同基质中维生素D含量测定前处理方法和测定方法的研究进展，据报道目前最常用的前处理方法为液-液萃取、固相萃取和液-液微萃取，而测定方法主要包括高效液相色谱、质谱、超临界流体色谱等方法，通过该综述以期为维生素D系列制剂的含量测定提供技术支持。

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张庆，女，硕士研究生，主要从事药品质量研究。E-mail: zhang_qing0918@163.com。

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张庆，女，硕士研究生，主要从事药品质量研究。E-mail: zhang_qing0918@163.com。

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