Article(id=1236369020874707942, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236369012058288373, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=null, receivedDateStr=null, revisedDate=null, revisedDateStr=null, acceptedDate=1676304000000, acceptedDateStr=2023-02-14, onlineDate=1772702945202, onlineDateStr=2026-03-05, pubDate=1693324800000, pubDateStr=2023-08-30, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772702945202, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772702945202, creator=13701087609, updateTime=1772702945202, updator=13701087609, issue=Issue{id=1236369012058288373, tenantId=1146029695717560320, journalId=1235980733773295621, year='2023', volume='32', issue='16', pageStart='1593', pageEnd='1696', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772702943100, creator=13701087609, updateTime=1772703272680, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236370394492490265, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236369012058288373, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236370394496684570, tenantId=1146029695717560320, journalId=1235980733773295621, issueId=1236369012058288373, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=1690, endPage=1696, ext={EN=ArticleExt(id=1236369021206056965, articleId=1236369020874707942, tenantId=1146029695717560320, journalId=1235980733773295621, language=EN, title=Preparation of β-cyclodextrin inclusion complexes of volatile oil in Qizhu granules and its characterization, columnId=null, journalTitle=Chinese Journal of New Drugs, columnName=null, runingTitle=null, highlight=null, articleAbstract=
Objective: To prepare the β-cyclodextrin inclusion complexes of volatile oil in Qizhu granules.
Methods: The technology parameters like inclusion time, inclusion temperature, and the ratio of volatile oil to β-cyclodextrin in the preparation process of inclusion complexes were investigated by single factor experiment with inclusion rate as the index. With inclusion rate and inclusion yield as indexes, Box-Behnken response surface method was used to optimize the preparation process of inclusion complexes. Thin-layer chromatography, infrared spectroscopy and differential scanning calorimetry were utilized to characterize the inclusion complexes.
Results: The optimal conditions were as follows: 9∶1 for volatile oils-(β-cyclodextrin) ratio, 64 ℃ for inclusion temperature, and 1 h for inclusion time. The inclusion rate and yield of the obtained inclusion complexes were 90.68% and 80.40%, respectively. All characterization results revealed the formation of inclusion complexes.
Conclusion: The established method is stable and feasible, which can be used for preparing the β-cyclodextrin inclusion complexes of volatile oil in Qizhu granules．
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方法： 以包合率为指标进行单因素实验，进行包合时间、包合温度和挥发油与β-环糊精比例的工艺参数优选；以包合率、包合物得率作为指标，采用Box-Behnken响应面法对包合物制备工艺进行优化。采用薄层色谱、红外光谱、差示扫描量热法对所得包合物进行表征。
结果： 最佳工艺为：挥发油与β-环糊精比例1∶9，包合温度64 ℃，包合时间1 h，所得包合物的包合率为90.68%，包合物得率为80.40%。表征结果均证明包合物形成。
结论： 该工艺稳定可靠，可用于制备芪术颗粒中挥发油β-环糊精包合物。
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王炳琪，男，硕士在读，主要从事中药制剂新技术研究与应用。E-mail: wang-bingqi@163.com。
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