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Methods The compounds were isolated and purified by silica gel column chromatography, Sephadex LH-20, ODS reversed-phase column chromatography and semi-preparative HPLC, and the structures were identified by spectral data (NMR and MS). Results A total of 19 compounds were isolated and identified as follows 1-[(1S,3aR,4R,7S,7aS)-4-hydroxy-4-hydroxymethyl-7-propan-2-yl-1,2,3,3a,5,6,7,7a-octahydroinden-1-yl]ethanone (1), 10α-hydroxy-1-oxoeremophila-7(11),8(9)-dien-12,8-olide (2), 6α,10α-dihydroxy-1-oxoeremophila-7(11),8(9)-dien-12,8-olide (3), 3-hydroxycacalolide (4), 6β-acetoxy-9-oxo-10αH-furanoeremophilane (5), pinoresinol (6), medioresinol (7), syringaresinol (8), p-hydroxybenzoic acid (9), methyl 3,4-dihydroxybenzoate (10), syringic acid (11), 3,4,5-trimethoxybenzoic acid (12), dimethy phthalate (13), syringin (14)、lupeol (15), obtusifoliol (16), ethyl linoleate (17), 15-vaccenic acid (18), 10-eicosenoic acid (19). Conclusion Compound 1 is a new compound, designated 14-hydroxy-oplopanone. Compounds 5—14, 16—19 are isolated from L. virgaurea for the first time., authors=WANG Yao, ZHANG Xinyu, LIAO Jiahui, WANG Hongling, authorsList=WANG Yao, ZHANG Xinyu, LIAO Jiahui, WANG Hongling, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1304415536125862439, articleId=1304415534515249702, tenantId=1146029695717560320, journalId=1302319053441957962, language=CN, title=藏药黄帚橐吾化学成分研究, columnId=1304140187169214944, journalTitle=中草药, columnName=化学成分, runingTitle=null, highlight=null, articleAbstract=目的 研究藏药黄帚橐吾Ligularia virgaurea的化学成分。方法 采用硅胶柱色谱、Sephadex LH-20、ODS反相柱色谱与半制备HPLC对黄帚橐吾进行分离纯化，结合NMR、MS等波谱学方法鉴定化合物结构。结果 从黄帚橐吾石油醚和醋酸乙酯部位中分离得到19个化合物，分别鉴定为1-[(1S,3aR,4R,7S,7aS)-4-羟基-4-羟甲基-7-异丙基-1,2,3,3a,5,6,7,7a-八氢茚-1-基]乙酮（1）、10α-hydroxy-1-oxoeremophila-7(11),8(9)-dien-12,8-olide（2）、6α,10α-dihydroxy-1-oxoeremophila-7(11),8(9)-dien-12,8-olide（3）、3-hydroxycacalolide（4）、6β-acetoxy-9-oxo-10αH-furanoeremophilane（5）、松脂醇（6）、皮树脂醇（7）、丁香脂素（8）、对羟基苯甲酸（9）、3,4-二羟基苯甲酸甲酯（10）、丁香酸（syringic acid，11）、3,4,5-三甲氧基苯甲酸（3,4,5-trimethoxybenzoic acid，12）、邻苯二甲酸二甲酯（13）、紫丁香苷（14）、羽扇豆醇（15）、钝叶醇（16）、亚油酸乙酯（17）、15-十八碳烯酸（18）、10-二十碳烯酸（19）。结论 其中，化合物1为新化合物，命名为黄帚橐吾酮A（14-hydroxy-oplopanone）；化合物5～14、16～19均为首次从黄帚橐吾中分离得到。, authors=王瑶¹, 张馨予¹, 廖佳慧¹, 王洪玲¹, authorsList=王瑶, 张馨予, 廖佳慧, 王洪玲, authorCompany=1 江西中医药大学, 中药资源与民族药研究中心, 江西 南昌 330004, correspAuthors=王洪玲, authorNote=王瑶: 王瑶(2002-),女,汉族,硕士研究生,主要从事中药尤其是民族药药效物质基础研究。E-mail:wangyao1@jxutcm.edu.cn, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=Qbw8Wy+TayOz9ttvU8tGuQ==, pdfFileSize=1023090, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=国家自然科学基金资助项目(U2202213);国家自然科学基金资助项目(32470428))}, authors=null, keywords=[Keyword(id=1304415536394297897, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=CN, orderNo=1, keyword=藏药), Keyword(id=1304415536482378282, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=CN, orderNo=2, keyword=黄帚橐吾), Keyword(id=1304415536562070059, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=CN, orderNo=3, keyword=黄帚橐吾酮A), Keyword(id=1304415536616596012, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=CN, orderNo=4, keyword=松脂醇), Keyword(id=1304415536687899181, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=CN, orderNo=5, keyword=皮树脂醇), Keyword(id=1304415536792756782, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=CN, orderNo=6, keyword=紫丁香苷), Keyword(id=1304415536868254255, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=CN, orderNo=7, keyword=15-十八碳烯酸), Keyword(id=1304415536960528944, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=EN, orderNo=1, keyword=Tibetan medicine), Keyword(id=1304415537027637809, tenantId=1146029695717560320, journalId=1302319053441957962, articleId=1304415534515249702, language=EN, orderNo=2, keyword=Ligularia virgaurea (Maxim.) 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