Article(id=1193259087325524515, tenantId=1146029695717560320, journalId=1189982191388893191, issueId=1193259081696772901, articleNumber=null, orderNo=null, doi=10.16438/j.0513-4870.2024-0995, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=research-article, receivedDate=1728921600000, receivedDateStr=2024-10-15, revisedDate=1734192000000, revisedDateStr=2024-12-15, acceptedDate=null, acceptedDateStr=null, onlineDate=1762424736100, onlineDateStr=2025-11-06, pubDate=1741708800000, pubDateStr=2025-03-12, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1762424736100, onlineIssueDateStr=2025-11-06, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1762424736100, creator=13701087609, updateTime=1762424736100, updator=13701087609, issue=Issue{id=1193259081696772901, tenantId=1146029695717560320, journalId=1189982191388893191, year='2025', volume='60', issue='3', pageStart='533', pageEnd='842', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1762424734756, creator=13701087609, updateTime=1764224876724, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1200809424412602670, tenantId=1146029695717560320, journalId=1189982191388893191, issueId=1193259081696772901, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1200809424412602671, tenantId=1146029695717560320, journalId=1189982191388893191, issueId=1193259081696772901, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=791, endPage=800, ext={EN=ArticleExt(id=1193259087728177704, articleId=1193259087325524515, tenantId=1146029695717560320, journalId=1189982191388893191, language=EN, title=Determination of 53 prohibited veterinary drug residues in goat horn by salting-out assisted liquid-liquid extraction combined with UHPLC-MS/MS, columnId=1190335348761793317, journalTitle=Acta Pharmaceutica Sinica, columnName=Original Articles, runingTitle=null, highlight=null, articleAbstract=
A detection method using UHPLC-MS/MS was established for the determination of 53 prohibited veterinary drug residues in goat horns, including 16 tranquilizers, 14 β-agonists, chloramphenicol, 4 fluoroquinolones, 7 nitroimidazoles, 3 quinoxalines, and 8 other compounds. Samples were extracted using salting-out assisted liquid-liquid extraction (SALLE). A Zorbax Eclipse Plus C18 column (1.8 μm, 3.0 mm × 150 mm, Agilent) was used with 0.1% formic acid solution-acetonitrile as the mobile phase for gradient elution. Detection was performed in positive and negative electrospray ionization modes using multiple reaction monitoring (MRM). All 53 analytes showed good linearity within their respective concentration ranges, with correlation coefficients above 0.99. The average recoveries at three spiked levels ranged from 70.4% to 118.7%, with relative standard deviations (RSDs) ranging from 0.69% to 12.07%. The limits of detection (LODs) ranged from 0.1 to 50 μg·kg-1, and the limits of quantitation (LOQs) ranged from 0.2 to 100 μg·kg-1. This method has been applied to the determination of real samples.
, correspAuthors=Jian SUN, Qing HU, authorNote=null, correspAuthorsNote=null, copyrightStatement=Copyright ©2025 Acta Pharmaceutica Sinica. All rights reserved., copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Bai-hao LAO, Jian SUN, Jing-xian ZHANG, Hong YU, Ying-ying RAN, Fan HUANG, Shen JI, Qing HU), CN=ArticleExt(id=1193259246155428744, articleId=1193259087325524515, tenantId=1146029695717560320, journalId=1189982191388893191, language=CN, title=盐析辅助液液萃取-超高效液相色谱串联质谱法测定山羊角中53种禁用兽药残留, columnId=1190335348896011050, journalTitle=药学学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=
建立了UHPLC-MS/MS测定山羊角中53种禁用兽药残留的检测方法, 包括16种镇静剂类、14种β-受体激动剂类、氯霉素、4种氟喹诺酮类、7种硝基咪唑类、3种喹噁啉类化合物、8种其他类化合物。采用盐析辅助液液萃取样品, Zorbax Eclipse Plus C18色谱柱(1.8 μm, 3.0 mm × 150 mm, Agilent), 以0.1%甲酸溶液-乙腈为流动相, 梯度洗脱, 在电喷雾离子化正负离子模式下, 以多反应监测方式(MRM) 检测。53种待测物在各自浓度范围内均成良好线性关系, 相关系数均在0.99以上; 三水平平均加样回收率为70.4%~118.7%, 相对标准偏差(RSD) 为0.69%~12.07%, 检出限为0.1~50 μg·kg-1, 定量限为0.2~100 μg·kg-1。本方法已应用于实际样品的测定。
, correspAuthors=孙健, 胡青, authorNote=null, correspAuthorsNote=
, copyrightStatement=版权所有©《药学学报》编辑部2025, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=1BsAUsCuR9y9O1IzUg0oeQ==, magXml=2JsYXFZulIWifYMXF4Vk8w==, pdfUrl=null, pdf=zTs5bwv0jkWT4sBbfTdwCA==, pdfFileSize=623891, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=glXEVkwqjl3zNb4pyUbY9g==, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=劳柏豪, 孙健, 张静娴, 于泓, 冉莹瑛, 黄帆, 季申, 胡青)}, authors=[Author(id=1194703704122171943, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1194703704201863723, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703704122171943, language=EN, stringName=Bai-hao LAO, firstName=Bai-hao, middleName=null, lastName=LAO, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
1, 2, address=1. School of Pharmacy, Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China
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1, 2, address=1.上海中医药大学中药学院, 上海 201203
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2, *, address=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1194703704520630837, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703704357052976, language=CN, stringName=孙健, firstName=健, middleName=null, lastName=孙, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, *, address=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1194703704050868770, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, xref=null, ext=[AuthorCompanyExt(id=1194703704059257379, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China), AuthorCompanyExt(id=1194703704063451684, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203)])]), Author(id=1194703704608711224, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, orderNo=2, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1194703704700985915, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703704608711224, language=EN, stringName=Jing-xian ZHANG, firstName=Jing-xian, middleName=null, lastName=ZHANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, address=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1194703704755511869, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703704608711224, language=CN, stringName=张静娴, firstName=静娴, middleName=null, lastName=张, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, address=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1194703704050868770, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, xref=null, ext=[AuthorCompanyExt(id=1194703704059257379, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China), AuthorCompanyExt(id=1194703704063451684, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203)])]), Author(id=1194703704826815040, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, orderNo=3, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1194703704927478339, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703704826815040, language=EN, stringName=Hong YU, firstName=Hong, middleName=null, lastName=YU, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, address=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1194703705011364421, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703704826815040, language=CN, stringName=于泓, firstName=泓, middleName=null, lastName=于, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, address=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1194703704050868770, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, xref=null, ext=[AuthorCompanyExt(id=1194703704059257379, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China), AuthorCompanyExt(id=1194703704063451684, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203)])]), Author(id=1194703705070084680, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, orderNo=4, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1194703705153970763, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703705070084680, language=EN, stringName=Ying-ying RAN, firstName=Ying-ying, middleName=null, lastName=RAN, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, address=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1194703705233662541, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703705070084680, language=CN, stringName=冉莹瑛, firstName=莹瑛, middleName=null, lastName=冉, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, address=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1194703704050868770, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, xref=null, ext=[AuthorCompanyExt(id=1194703704059257379, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China), AuthorCompanyExt(id=1194703704063451684, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203)])]), Author(id=1194703705304965711, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, orderNo=5, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=null, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1194703705401434706, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703705304965711, language=EN, stringName=Fan HUANG, firstName=Fan, middleName=null, lastName=HUANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
2, address=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1194703705502098004, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, authorId=1194703705304965711, language=CN, stringName=黄帆, firstName=帆, middleName=null, lastName=黄, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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1, 2, address=1. School of Pharmacy, Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China
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β2-受体激动剂残留高准确度测量方法研究) [D]. Shanghai: Shanghai University of Engineering Science, 2021., articleTitle=null, refAbstract=null), Reference(id=1194703713077011130, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, doi=null, pmid=null, pmcid=null, year=null, volume=null, issue=null, pageStart=null, pageEnd=null, url=null, language=null, rfNumber=[35], rfOrder=34, authorNames=null, journalName=null, refType=null, unstructuredReference=Zhang KM, Liang FY, Deng M, et al. Multi-residue determination of veterinary drugs in porcine muscle by QuEChERS and liquid chromatography-tandem mass spectrometry [J]. Chin J Chromatogr (色谱), 2016, 34: 860-867., articleTitle=null, refAbstract=null)], funds=[Fund(id=1194703709335691914, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, awardId=21DZ2290200, language=CN, fundingSource=上海市科委研发平台专项(21DZ2290200), fundOrder=null, country=null)], companyList=[AuthorCompany(id=1194703703954399774, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, xref=null, ext=[AuthorCompanyExt(id=1194703703962788383, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703703954399774, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1. School of Pharmacy, Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China), AuthorCompanyExt(id=1194703703966982688, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703703954399774, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=1.上海中医药大学中药学院, 上海 201203)]), AuthorCompany(id=1194703704050868770, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, xref=null, ext=[AuthorCompanyExt(id=1194703704059257379, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2. National Medical Products Administration Key Laboratory for Quality Control of Traditional Chinese Medicine, Shanghai Institute for Food and Drug Control, Shanghai 201203, China), AuthorCompanyExt(id=1194703704063451684, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, companyId=1194703704050868770, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=2.上海市食品药品检验研究院, 国家药品监督管理局中药质量控制重点实验室, 上海 201203)])], figs=[ArticleFig(id=1194703708450693751, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=EN, label=null, caption=null, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | CAS number | Chemical formula | Dissolved solvent | Lot. number | Purity | M.W. |
| β-Agonist | | | | | | |
| Clorprenaline | 3811-25-4 | C11H16ClNO | Methanol | S177845 | 0.828 | 213.1 |
| Tulobuterol | 41570-61-0 | C12H18ClNO | Methanol | S139505 | 0.999 | 227.1 |
| Ractopamine | 97825-25-7 | C18H23NO3 | Methanol | S177845 | 0.989 | 301.2 |
| Bambuterol | 81732-65-2 | C18H29N3O5 | Methanol | S177845 | 0.993 | 367.2 |
| Phenylethanolamine A | 1346746-81-3 | C19H24N2O4 | Methanol | S148439 | 0.998 | 344.2 |
| Mabuterol | 56341-08-3 | C13H18ClF3N2O | Methanol | S177845 | 0.999 | 310.1 |
| Salbutamol | 18559-94-9 | C13H21NO3 | Methanol | S177845 | 0.994 | 239.2 |
| Zilpaterol | 117827-79-9 | C14H19N3O2 | Methanol | S177845 | 0.961 | 261.2 |
| Cimaterol | 54239-37-1 | C12H17N3O | Methanol | S172505 | 0.980 | 219.1 |
| Terbutaline | 23031-25-6 | C12H19NO3 | Methanol | S177845 | 0.999 | 225.1 |
| Clenbuterol | 37148-27-9 | C12H18Cl2N2O | Methanol | S177845 | 0.988 | 276.1 |
| Cimbuterol | 54239-39-3 | C13H19N3O | Methanol | S096141 | 0.999 | 233.2 |
| Brombuterol | 41937-02-4 | C12H18Br2N2O | Methanol | S134561 | 0.994 | 364.0 |
| Formoterol | 73573-87-2 | C19H24N2O4 | Methanol | S146953 | 0.999 | 344.2 |
| Amphenicol | | | | | | |
| Chloramphenicol | 56-75-7 | C11H12Cl2N2O5 | Methanol | S145561 | 0.998 | 322.0 |
| Tranquilizer | | | | | | |
| Chlorpromazine | 50-53-3 | C17H19ClN2S | Methanol | S167751 | 0.980 | 318.1 |
| Methaqualone | 72-44-6 | C16H14N2O | Methanol | ALT028069 | 0.999 | 250.1 |
| Xylazine | 7361-61-7 | C12H16N2S | Methanol | S159793 | 0.990 | 220.1 |
| Estazolam | 29975-16-4 | C16H11ClN4 | Methanol | S119943 | 0.999 | 294.1 |
| Midazolam | 59467-70-8 | C18H13ClFN3 | Methanol | S119943 | 0.994 | 325.8 |
| Triazolam | 28911-01-5 | C17H12Cl2N4 | Methanol | S119943 | 0.992 | 342.0 |
| Alprazolam | 28981-97-7 | C17H13ClN4 | Methanol | S119943 | 0.999 | 308.1 |
| Diazepam | 439-14-5 | C16H13ClN2O | Methanol | S119943 | 0.999 | 284.1 |
| Nitrazepam | 146-22-5 | C15H11N3O3 | Methanol | S119943 | 0.999 | 281.1 |
| Oxazepam | 604-75-1 | C15H11ClN2O2 | Methanol | S119943 | 0.996 | 286.1 |
| Clonazepam | 1622-61-3 | C15H10ClN3O3 | Methanol | S119943 | 0.999 | 315.0 |
| Lorazepam | 846-49-1 | C15H10Cl2N2O2 | Methanol | S119943 | 0.999 | 320.0 |
| Phenobarbital | 50-06-6 | C12H12N2O3 | Methanol | S142179 | 0.999 | 232.1 |
| Barbital | 57-44-3 | C8H12N2O3 | Methanol | S142179 | 0.999 | 184.1 |
| Amobarbital | 57-43-2 | C11H18N2O3 | Methanol | S142179 | 0.999 | 226.1 |
| Secobarbital | 76-73-3 | C12H18N2O3 | Methanol | S142179 | 0.999 | 238.1 |
| Fluoroquinolone | | | | | | |
| Norfloxacin | 70458-96-7 | C16H18FN3O3 | Methanol | S117199 | 0.999 | 319.1 |
| Pefloxacin | 70458-92-3 | C17H20FN3O3 | Methanol | S117199 | 0.987 | 333.2 |
| Lomefloxacin | 98079-51-7 | C17H19F2N3O3 | Methanol | S117199 | 0.904 | 351.1 |
| Ofloxacin | 82419-36-1 | C18H20FN3O4 | Methanol | S117199 | 0.995 | 361.1 |
| Nitroimidazole | | | | | | |
| Dimetridazole | 551-92-8 | C5H7N3O2 | Methanol | S169555 | 0.999 | 141.1 |
| Dimetridazole-2-hydroxy | 936-05-0 | C5H7N3O3 | Methanol | S169555 | 0.980 | 157.1 |
| Metronidazole-hydroxy | 4812-40-2 | C6H9N3O4 | Methanol | S169555 | 0.996 | 187.1 |
| Metronidazole | 443-48-1 | C6H9N3O3 | Methanol | S169555 | 0.999 | 171.1 |
| Ronidazole | 7681-76-7 | C6H8N4O4 | Methanol | S169555 | 0.990 | 200.1 |
| Ipronidazole | 14885-29-1 | C7H11N3O2 | Methanol | S094613 | 0.999 | 169.1 |
| Tinidazole | 19387-91-8 | C8H13N3O4S | Methanol | S143801 | 0.999 | 247.1 |
| Quinoxaline | | | | | | |
| 2-Quinoxaline-carboxylic acid (2-QCA) | 879-65-2 | C9H6N2O2 | Methanol | S153963 | 0.950 | 174.0 |
| 3-Methyl-2-quinoxaline-carboxylic acid (MQCA) | 74003-63-7 | C10H8N2O2 | Methanol | S160521 | 0.999 | 188.1 |
| Carbadox | 6804-07-5 | C11H10N4O4 | Methanol/DMSO (3∶1) | S095207 | 0.972 | 262.1 |
| Others | | | | | | |
| Dapsone | 80-08-0 | C12H12N2O2S | Acetonitrile | S125593 | 0.994 | 248.1 |
| Leucomalachite green | 129-73-7 | C23H26N2 | Methanol | S167117 | 0.994 | 330.2 |
| Malachite green | 569-64-2 | C23H25ClN2 | Methanol | S167117 | 0.981 | 364.9 |
| Clonidine | 4205-90-7 | C9H9Cl2N3 | Methanol | S146723 | 0.998 | 229.0 |
| Cyproheptadine | 129-03-3 | C21H21N | Methanol | S149739 | 0.998 | 287.4 |
| Carbofuran | 1563-66-2 | C12H15NO3 | Acetonitrile | 2250832 | 0.999 | 221.1 |
| Chlordimeform | 6164-98-3 | C10H13ClN2 | Methanol | S168431 | 0.989 | 196.1 |
| Fipronil | 120068-37-3 | C12H4Cl2F6N4OS | Acetonitrile | S163547 | 0.995 | 435.9 |
| Internal standard (IS) | | | | | | |
| Cimbuterol-d9 | 1246819-04-4 | C13H10D9N3O | Methanol | G0065083 | 0.977 | 242.2 |
| Zilpaterol-d7 | 1217818-36-4 | C14H12D7N3O2 | Methanol | G0088143 | > 0.98 | 268.2 |
| 2-QCA-d4 | 2244217-89-6 | C9H2D4N2O2 | Methanol | H0095896 | 0.980 | 178.1 |
| Metronidazole-hydroxy-d2 | 2196180-19-3 | C6H7D2N3O4 | Methanol | H3000662 | 0.980 | 189.1 |
| Pefloxacin-d5 | 1228182-51-1 | C17H15D5FN3O3 | Methanol | F0058438 | 0.996 | 338.2 |
| Dapsone-d8 | 557794-38-4 | C12H4D8N2O2S | Methanol | D0054643 | 1.000 | 256.1 |
| Carbofuran-d3 | 1007459-98-4 | C12H12D3NO3 | Methanol | E0066530 | 0.998 | 224.1 |
| Fipronil-13C415N2 | - | C813C4H4Cl2F6N215N2OS | Methanol | A0069672 | 1.000 | 443.1 |
| Leucomalachite green-d6 | 1173021-13-0 | C23H20D6N2 | Acetonitrile | G0093712 | 0.998 | 336.3 |
| Malachite green-d5 | - | C23H20D5ClN2 | Acetonitrile | G0093712 | 0.596 | 369.9 |
), ArticleFig(id=1194703708547162745, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=CN, label=Table 1, caption=
The information of 53 analysts and internal standards
, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | CAS number | Chemical formula | Dissolved solvent | Lot. number | Purity | M.W. |
| β-Agonist | | | | | | |
| Clorprenaline | 3811-25-4 | C11H16ClNO | Methanol | S177845 | 0.828 | 213.1 |
| Tulobuterol | 41570-61-0 | C12H18ClNO | Methanol | S139505 | 0.999 | 227.1 |
| Ractopamine | 97825-25-7 | C18H23NO3 | Methanol | S177845 | 0.989 | 301.2 |
| Bambuterol | 81732-65-2 | C18H29N3O5 | Methanol | S177845 | 0.993 | 367.2 |
| Phenylethanolamine A | 1346746-81-3 | C19H24N2O4 | Methanol | S148439 | 0.998 | 344.2 |
| Mabuterol | 56341-08-3 | C13H18ClF3N2O | Methanol | S177845 | 0.999 | 310.1 |
| Salbutamol | 18559-94-9 | C13H21NO3 | Methanol | S177845 | 0.994 | 239.2 |
| Zilpaterol | 117827-79-9 | C14H19N3O2 | Methanol | S177845 | 0.961 | 261.2 |
| Cimaterol | 54239-37-1 | C12H17N3O | Methanol | S172505 | 0.980 | 219.1 |
| Terbutaline | 23031-25-6 | C12H19NO3 | Methanol | S177845 | 0.999 | 225.1 |
| Clenbuterol | 37148-27-9 | C12H18Cl2N2O | Methanol | S177845 | 0.988 | 276.1 |
| Cimbuterol | 54239-39-3 | C13H19N3O | Methanol | S096141 | 0.999 | 233.2 |
| Brombuterol | 41937-02-4 | C12H18Br2N2O | Methanol | S134561 | 0.994 | 364.0 |
| Formoterol | 73573-87-2 | C19H24N2O4 | Methanol | S146953 | 0.999 | 344.2 |
| Amphenicol | | | | | | |
| Chloramphenicol | 56-75-7 | C11H12Cl2N2O5 | Methanol | S145561 | 0.998 | 322.0 |
| Tranquilizer | | | | | | |
| Chlorpromazine | 50-53-3 | C17H19ClN2S | Methanol | S167751 | 0.980 | 318.1 |
| Methaqualone | 72-44-6 | C16H14N2O | Methanol | ALT028069 | 0.999 | 250.1 |
| Xylazine | 7361-61-7 | C12H16N2S | Methanol | S159793 | 0.990 | 220.1 |
| Estazolam | 29975-16-4 | C16H11ClN4 | Methanol | S119943 | 0.999 | 294.1 |
| Midazolam | 59467-70-8 | C18H13ClFN3 | Methanol | S119943 | 0.994 | 325.8 |
| Triazolam | 28911-01-5 | C17H12Cl2N4 | Methanol | S119943 | 0.992 | 342.0 |
| Alprazolam | 28981-97-7 | C17H13ClN4 | Methanol | S119943 | 0.999 | 308.1 |
| Diazepam | 439-14-5 | C16H13ClN2O | Methanol | S119943 | 0.999 | 284.1 |
| Nitrazepam | 146-22-5 | C15H11N3O3 | Methanol | S119943 | 0.999 | 281.1 |
| Oxazepam | 604-75-1 | C15H11ClN2O2 | Methanol | S119943 | 0.996 | 286.1 |
| Clonazepam | 1622-61-3 | C15H10ClN3O3 | Methanol | S119943 | 0.999 | 315.0 |
| Lorazepam | 846-49-1 | C15H10Cl2N2O2 | Methanol | S119943 | 0.999 | 320.0 |
| Phenobarbital | 50-06-6 | C12H12N2O3 | Methanol | S142179 | 0.999 | 232.1 |
| Barbital | 57-44-3 | C8H12N2O3 | Methanol | S142179 | 0.999 | 184.1 |
| Amobarbital | 57-43-2 | C11H18N2O3 | Methanol | S142179 | 0.999 | 226.1 |
| Secobarbital | 76-73-3 | C12H18N2O3 | Methanol | S142179 | 0.999 | 238.1 |
| Fluoroquinolone | | | | | | |
| Norfloxacin | 70458-96-7 | C16H18FN3O3 | Methanol | S117199 | 0.999 | 319.1 |
| Pefloxacin | 70458-92-3 | C17H20FN3O3 | Methanol | S117199 | 0.987 | 333.2 |
| Lomefloxacin | 98079-51-7 | C17H19F2N3O3 | Methanol | S117199 | 0.904 | 351.1 |
| Ofloxacin | 82419-36-1 | C18H20FN3O4 | Methanol | S117199 | 0.995 | 361.1 |
| Nitroimidazole | | | | | | |
| Dimetridazole | 551-92-8 | C5H7N3O2 | Methanol | S169555 | 0.999 | 141.1 |
| Dimetridazole-2-hydroxy | 936-05-0 | C5H7N3O3 | Methanol | S169555 | 0.980 | 157.1 |
| Metronidazole-hydroxy | 4812-40-2 | C6H9N3O4 | Methanol | S169555 | 0.996 | 187.1 |
| Metronidazole | 443-48-1 | C6H9N3O3 | Methanol | S169555 | 0.999 | 171.1 |
| Ronidazole | 7681-76-7 | C6H8N4O4 | Methanol | S169555 | 0.990 | 200.1 |
| Ipronidazole | 14885-29-1 | C7H11N3O2 | Methanol | S094613 | 0.999 | 169.1 |
| Tinidazole | 19387-91-8 | C8H13N3O4S | Methanol | S143801 | 0.999 | 247.1 |
| Quinoxaline | | | | | | |
| 2-Quinoxaline-carboxylic acid (2-QCA) | 879-65-2 | C9H6N2O2 | Methanol | S153963 | 0.950 | 174.0 |
| 3-Methyl-2-quinoxaline-carboxylic acid (MQCA) | 74003-63-7 | C10H8N2O2 | Methanol | S160521 | 0.999 | 188.1 |
| Carbadox | 6804-07-5 | C11H10N4O4 | Methanol/DMSO (3∶1) | S095207 | 0.972 | 262.1 |
| Others | | | | | | |
| Dapsone | 80-08-0 | C12H12N2O2S | Acetonitrile | S125593 | 0.994 | 248.1 |
| Leucomalachite green | 129-73-7 | C23H26N2 | Methanol | S167117 | 0.994 | 330.2 |
| Malachite green | 569-64-2 | C23H25ClN2 | Methanol | S167117 | 0.981 | 364.9 |
| Clonidine | 4205-90-7 | C9H9Cl2N3 | Methanol | S146723 | 0.998 | 229.0 |
| Cyproheptadine | 129-03-3 | C21H21N | Methanol | S149739 | 0.998 | 287.4 |
| Carbofuran | 1563-66-2 | C12H15NO3 | Acetonitrile | 2250832 | 0.999 | 221.1 |
| Chlordimeform | 6164-98-3 | C10H13ClN2 | Methanol | S168431 | 0.989 | 196.1 |
| Fipronil | 120068-37-3 | C12H4Cl2F6N4OS | Acetonitrile | S163547 | 0.995 | 435.9 |
| Internal standard (IS) | | | | | | |
| Cimbuterol-d9 | 1246819-04-4 | C13H10D9N3O | Methanol | G0065083 | 0.977 | 242.2 |
| Zilpaterol-d7 | 1217818-36-4 | C14H12D7N3O2 | Methanol | G0088143 | > 0.98 | 268.2 |
| 2-QCA-d4 | 2244217-89-6 | C9H2D4N2O2 | Methanol | H0095896 | 0.980 | 178.1 |
| Metronidazole-hydroxy-d2 | 2196180-19-3 | C6H7D2N3O4 | Methanol | H3000662 | 0.980 | 189.1 |
| Pefloxacin-d5 | 1228182-51-1 | C17H15D5FN3O3 | Methanol | F0058438 | 0.996 | 338.2 |
| Dapsone-d8 | 557794-38-4 | C12H4D8N2O2S | Methanol | D0054643 | 1.000 | 256.1 |
| Carbofuran-d3 | 1007459-98-4 | C12H12D3NO3 | Methanol | E0066530 | 0.998 | 224.1 |
| Fipronil-13C415N2 | - | C813C4H4Cl2F6N215N2OS | Methanol | A0069672 | 1.000 | 443.1 |
| Leucomalachite green-d6 | 1173021-13-0 | C23H20D6N2 | Acetonitrile | G0093712 | 0.998 | 336.3 |
| Malachite green-d5 | - | C23H20D5ClN2 | Acetonitrile | G0093712 | 0.596 | 369.9 |
), ArticleFig(id=1194703708618465915, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=EN, label=null, caption=null, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | Precursor ion (m/z) | Product ion (m/z) | Retention time/min | Fragmentor/V | Collision energy/V | Polarity | IS |
| β-Agonist | | | | | | | |
| Clorprenaline | 214.1 | 196.0*/153.9 | 5.97 | 380 | 8/12 | + | |
| Tulobuterol | 228.1 | 154.0*/119.1 | 7.00 | 380 | 12/32 | + | |
| Ractopamine | 302.2 | 284.2*/164.1 | 5.81 | 380 | 8/12 | + | |
| Bambuterol | 368.2 | 72.0*/46.1 | 8.29 | 380 | 57/25 | + | |
| Phenylethanolamine A | 345.2 | 327.2*/150.2 | 11.61 | 380 | 13/21 | + | |
| Mabuterol | 311.0 | 293.0/237.0* | 8.68 | 380 | 9/17 | + | |
| Salbutamol | 240.2 | 166.1/148.1* | 3.64 | 380 | 4/16 | + | Zilpaterol-d7 |
| Zilpaterol | 262.2 | 202.0/185.1* | 3.62 | 380 | 21/25 | + | Zilpaterol-d7 |
| Cimaterol | 220.1 | 202.1*/160.1 | 3.80 | 380 | 4/12 | + | Cimbuterol-d9 |
| Terbutaline | 226.1 | 170.1/152.1* | 3.64 | 380 | 8/12 | + | Cimbuterol-d9 |
| Clenbuterol | 277.1 | 259.1/203.0* | 7.10 | 380 | 4/12 | + | Cimbuterol-d9 |
| Cimbuterol | 234.0 | 160.0*/143.0 | 4.35 | 380 | 13/29 | + | Cimbuterol-d9 |
| Brombuterol | 365.0 | 290.9*/212.0 | 8.09 | 380 | 17/33 | + | Cimbuterol-d9 |
| Formoterol | 345.2 | 149.1*/121.3 | 6.98 | 380 | 21/33 | + | Cimbuterol-d9 |
| Amphenicol | | | | | | | |
| Chloramphenicol | 321.0 | 257.0/152.1* | 9.61 | 380 | 16/14 | - | |
| Tranquilizer | | | | | | | |
| Chlorpromazine | 319.1 | 86.1/58.2* | 13.94 | 380 | 16/44 | + | |
| Methaqualone | 251.1 | 132.1/91.0* | 14.16 | 380 | 37/49 | + | |
| Xylazine | 221.1 | 90.0*/72.0 | 6.94 | 380 | 40/40 | + | |
| Estazolam | 295.1 | 267.0*/192.0 | 13.55 | 380 | 25/23 | + | |
| Midazolam | 326.1 | 291.1*/223.2 | 10.83 | 380 | 29/45 | + | |
| Triazolam | 343.1 | 314.9/308.0* | 14.01 | 380 | 25/28 | + | |
| Alprazolam | 309.1 | 281.3/205.2* | 13.88 | 380 | 29/53 | + | |
| Diazepam | 285.1 | 222.1/193.1* | 15.23 | 380 | 33/37 | + | |
| Nitrazepam | 282.1 | 207.2*/180.2 | 13.58 | 380 | 37/41 | + | |
| Oxazepam | 287.1 | 241.0*/162.9 | 13.51 | 380 | 25/45 | + | |
| Clonazepam | 316.0 | 240.9/213.8* | 13.89 | 380 | 34/38 | + | |
| Lorazepam | 321.0 | 302.9/275.0* | 13.79 | 380 | 21/25 | + | |
| Barbital | 183.2 | 140.1*/84.9 | 5.92 | 380 | 9/9 | - | |
| Secobarbital | 237.2 | 194.2*/84.9 | 13.71 | 380 | 9/9 | - | |
| Phenobarbital | 231.0 | 188.1*/84.9 | 9.51 | 380 | 9/9 | - | |
| Amobarbital | 225.2 | 182.2*/84.9 | 13.02 | 380 | 13/13 | - | |
| Fluoroquinolone | | | | | | | |
| Norfloxacin | 320.1 | 302.1*/231.1 | 5.32 | 380 | 25/40 | + | Pefloxacin-d5 |
| Pefloxacin | 334.2 | 316.3*/290.1 | 5.47 | 380 | 21/28 | + | Pefloxacin-d5 |
| Lomefloxacin | 352.2 | 334.0/265.0* | 5.86 | 380 | 20/25 | + | Pefloxacin-d5 |
| Ofloxacin | 362.2 | 318.2*/261.1 | 5.38 | 380 | 20/40 | + | Pefloxacin-d5 |
| Nitroimidazole | | | | | | | |
| Dimetridazole | 142.1 | 96.1*/81.1 | 5.22 | 380 | 16/28 | + | Metronidazole-hydroxy-d2 |
| Dimetridazole-2-hydroxy | 158.1 | 140.0/55.2* | 4.25 | 380 | 8/20 | + | Metronidazole-hydroxy-d2 |
| Metronidazole-hydroxy | 188.1 | 126.1*/123.1 | 3.76 | 380 | 16/8 | + | Metronidazole-hydroxy-d2 |
| Metronidazole | 172.1 | 128.0*/82.1 | 4.31 | 380 | 12/24 | + | Metronidazole-hydroxy-d2 |
| Ronidazole | 201.1 | 140.1*/55.2 | 4.69 | 380 | 8/25 | + | Metronidazole-hydroxy-d2 |
| Ipronidazole | 170.1 | 124.0*/109.0 | 9.62 | 380 | 16/26 | + | Metronidazole-hydroxy-d2 |
| Tinidazole | 248.1 | 121.0/29.2* | 6.00 | 380 | 17/21 | + | |
| Quinoxaline | | | | | | | |
| 2-QCA | 175.0 | 128.9/102.0* | 5.22 | 380 | 16/40 | + | 2-QCA-d4 |
| MQCA | 189.1 | 145.0*/143.0 | 5.24 | 380 | 12/16 | + | 2-QCA-d4 |
| Carbadox | 263.1 | 231.2*/130.1 | 5.43 | 380 | 13/21 | + | 2-QCA-d4 |
| Others | | | | | | | |
| Dapsone | 249.1 | 156.0/92.0* | 7.76 | 380 | 10/28 | + | Dapsone-d8 |
| Leucomalachite green | 331.2 | 316.2/239.2* | 17.57 | 380 | 20/28 | + | Leucomalachite green-d6 |
| Malachite green | 329.2 | 313.1*/284.1 | 14.66 | 380 | 41/65 | + | Malachite green-d5 |
| Clonidine | 230.0 | 133.1/74.2* | 4.55 | 380 | 53/73 | + | |
| Cyproheptadine | 288.2 | 215.1/96.2* | 13.34 | 380 | 65/25 | + | |
| Carbofuran | 222.1 | 165.1*/123.0 | 13.62 | 380 | 13/25 | + | Carbofuran-d3 |
| Chlordimeform | 197.1 | 125.0/117.1* | 6.55 | 380 | 33/29 | + | |
| Fipronil | 434.9 | 278.0/250.0* | 16.16 | 380 | 37/33 | - | Fipronil-13C415N2 |
| IS | | | | | | | |
| Cimbuterol-d9 | 243.2 | 160.9 | 4.35 | 380 | 17 | + | |
| Zilpaterol-d7 | 269.0 | 202.9 | 3.62 | 380 | 21 | + | |
| 2-QCA-d4 | 179.0 | 132.9 | 5.22 | 380 | 21 | + | |
| Metronidazole-hydroxy-d2 | 190.1 | 127.9 | 3.76 | 380 | 17 | + | |
| Pefloxacin-d5 | 339.2 | 321.1 | 5.47 | 380 | 25 | + | |
| Dapsone-d8 | 257.4 | 159.9 | 7.76 | 380 | 17 | + | |
| Carbofuran-d3 | 225.1 | 164.8 | 13.62 | 380 | 13 | + | |
| Fipronil-13C415N2 | 441.0 | 251.8 | 16.16 | 380 | 29 | - | |
| Leucomalachite green-d6 | 337.3 | 240.1 | 17.57 | 380 | 37 | + | |
| Malachite green-d5 | 334.2 | 318.2 | 14.66 | 380 | 41 | + | |
), ArticleFig(id=1194703708681380477, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=CN, label=Table 2, caption=
Detailed MS/MS parameters of 53 analytes. *Quantitative ion
, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | Precursor ion (m/z) | Product ion (m/z) | Retention time/min | Fragmentor/V | Collision energy/V | Polarity | IS |
| β-Agonist | | | | | | | |
| Clorprenaline | 214.1 | 196.0*/153.9 | 5.97 | 380 | 8/12 | + | |
| Tulobuterol | 228.1 | 154.0*/119.1 | 7.00 | 380 | 12/32 | + | |
| Ractopamine | 302.2 | 284.2*/164.1 | 5.81 | 380 | 8/12 | + | |
| Bambuterol | 368.2 | 72.0*/46.1 | 8.29 | 380 | 57/25 | + | |
| Phenylethanolamine A | 345.2 | 327.2*/150.2 | 11.61 | 380 | 13/21 | + | |
| Mabuterol | 311.0 | 293.0/237.0* | 8.68 | 380 | 9/17 | + | |
| Salbutamol | 240.2 | 166.1/148.1* | 3.64 | 380 | 4/16 | + | Zilpaterol-d7 |
| Zilpaterol | 262.2 | 202.0/185.1* | 3.62 | 380 | 21/25 | + | Zilpaterol-d7 |
| Cimaterol | 220.1 | 202.1*/160.1 | 3.80 | 380 | 4/12 | + | Cimbuterol-d9 |
| Terbutaline | 226.1 | 170.1/152.1* | 3.64 | 380 | 8/12 | + | Cimbuterol-d9 |
| Clenbuterol | 277.1 | 259.1/203.0* | 7.10 | 380 | 4/12 | + | Cimbuterol-d9 |
| Cimbuterol | 234.0 | 160.0*/143.0 | 4.35 | 380 | 13/29 | + | Cimbuterol-d9 |
| Brombuterol | 365.0 | 290.9*/212.0 | 8.09 | 380 | 17/33 | + | Cimbuterol-d9 |
| Formoterol | 345.2 | 149.1*/121.3 | 6.98 | 380 | 21/33 | + | Cimbuterol-d9 |
| Amphenicol | | | | | | | |
| Chloramphenicol | 321.0 | 257.0/152.1* | 9.61 | 380 | 16/14 | - | |
| Tranquilizer | | | | | | | |
| Chlorpromazine | 319.1 | 86.1/58.2* | 13.94 | 380 | 16/44 | + | |
| Methaqualone | 251.1 | 132.1/91.0* | 14.16 | 380 | 37/49 | + | |
| Xylazine | 221.1 | 90.0*/72.0 | 6.94 | 380 | 40/40 | + | |
| Estazolam | 295.1 | 267.0*/192.0 | 13.55 | 380 | 25/23 | + | |
| Midazolam | 326.1 | 291.1*/223.2 | 10.83 | 380 | 29/45 | + | |
| Triazolam | 343.1 | 314.9/308.0* | 14.01 | 380 | 25/28 | + | |
| Alprazolam | 309.1 | 281.3/205.2* | 13.88 | 380 | 29/53 | + | |
| Diazepam | 285.1 | 222.1/193.1* | 15.23 | 380 | 33/37 | + | |
| Nitrazepam | 282.1 | 207.2*/180.2 | 13.58 | 380 | 37/41 | + | |
| Oxazepam | 287.1 | 241.0*/162.9 | 13.51 | 380 | 25/45 | + | |
| Clonazepam | 316.0 | 240.9/213.8* | 13.89 | 380 | 34/38 | + | |
| Lorazepam | 321.0 | 302.9/275.0* | 13.79 | 380 | 21/25 | + | |
| Barbital | 183.2 | 140.1*/84.9 | 5.92 | 380 | 9/9 | - | |
| Secobarbital | 237.2 | 194.2*/84.9 | 13.71 | 380 | 9/9 | - | |
| Phenobarbital | 231.0 | 188.1*/84.9 | 9.51 | 380 | 9/9 | - | |
| Amobarbital | 225.2 | 182.2*/84.9 | 13.02 | 380 | 13/13 | - | |
| Fluoroquinolone | | | | | | | |
| Norfloxacin | 320.1 | 302.1*/231.1 | 5.32 | 380 | 25/40 | + | Pefloxacin-d5 |
| Pefloxacin | 334.2 | 316.3*/290.1 | 5.47 | 380 | 21/28 | + | Pefloxacin-d5 |
| Lomefloxacin | 352.2 | 334.0/265.0* | 5.86 | 380 | 20/25 | + | Pefloxacin-d5 |
| Ofloxacin | 362.2 | 318.2*/261.1 | 5.38 | 380 | 20/40 | + | Pefloxacin-d5 |
| Nitroimidazole | | | | | | | |
| Dimetridazole | 142.1 | 96.1*/81.1 | 5.22 | 380 | 16/28 | + | Metronidazole-hydroxy-d2 |
| Dimetridazole-2-hydroxy | 158.1 | 140.0/55.2* | 4.25 | 380 | 8/20 | + | Metronidazole-hydroxy-d2 |
| Metronidazole-hydroxy | 188.1 | 126.1*/123.1 | 3.76 | 380 | 16/8 | + | Metronidazole-hydroxy-d2 |
| Metronidazole | 172.1 | 128.0*/82.1 | 4.31 | 380 | 12/24 | + | Metronidazole-hydroxy-d2 |
| Ronidazole | 201.1 | 140.1*/55.2 | 4.69 | 380 | 8/25 | + | Metronidazole-hydroxy-d2 |
| Ipronidazole | 170.1 | 124.0*/109.0 | 9.62 | 380 | 16/26 | + | Metronidazole-hydroxy-d2 |
| Tinidazole | 248.1 | 121.0/29.2* | 6.00 | 380 | 17/21 | + | |
| Quinoxaline | | | | | | | |
| 2-QCA | 175.0 | 128.9/102.0* | 5.22 | 380 | 16/40 | + | 2-QCA-d4 |
| MQCA | 189.1 | 145.0*/143.0 | 5.24 | 380 | 12/16 | + | 2-QCA-d4 |
| Carbadox | 263.1 | 231.2*/130.1 | 5.43 | 380 | 13/21 | + | 2-QCA-d4 |
| Others | | | | | | | |
| Dapsone | 249.1 | 156.0/92.0* | 7.76 | 380 | 10/28 | + | Dapsone-d8 |
| Leucomalachite green | 331.2 | 316.2/239.2* | 17.57 | 380 | 20/28 | + | Leucomalachite green-d6 |
| Malachite green | 329.2 | 313.1*/284.1 | 14.66 | 380 | 41/65 | + | Malachite green-d5 |
| Clonidine | 230.0 | 133.1/74.2* | 4.55 | 380 | 53/73 | + | |
| Cyproheptadine | 288.2 | 215.1/96.2* | 13.34 | 380 | 65/25 | + | |
| Carbofuran | 222.1 | 165.1*/123.0 | 13.62 | 380 | 13/25 | + | Carbofuran-d3 |
| Chlordimeform | 197.1 | 125.0/117.1* | 6.55 | 380 | 33/29 | + | |
| Fipronil | 434.9 | 278.0/250.0* | 16.16 | 380 | 37/33 | - | Fipronil-13C415N2 |
| IS | | | | | | | |
| Cimbuterol-d9 | 243.2 | 160.9 | 4.35 | 380 | 17 | + | |
| Zilpaterol-d7 | 269.0 | 202.9 | 3.62 | 380 | 21 | + | |
| 2-QCA-d4 | 179.0 | 132.9 | 5.22 | 380 | 21 | + | |
| Metronidazole-hydroxy-d2 | 190.1 | 127.9 | 3.76 | 380 | 17 | + | |
| Pefloxacin-d5 | 339.2 | 321.1 | 5.47 | 380 | 25 | + | |
| Dapsone-d8 | 257.4 | 159.9 | 7.76 | 380 | 17 | + | |
| Carbofuran-d3 | 225.1 | 164.8 | 13.62 | 380 | 13 | + | |
| Fipronil-13C415N2 | 441.0 | 251.8 | 16.16 | 380 | 29 | - | |
| Leucomalachite green-d6 | 337.3 | 240.1 | 17.57 | 380 | 37 | + | |
| Malachite green-d5 | 334.2 | 318.2 | 14.66 | 380 | 41 | + | |
), ArticleFig(id=1194703708765266559, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=EN, label=null, caption=null, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | LOD/μg·kg-1 | LOQ/μg·kg-1 | Linear equation | Linear range/μg·L-1 | r | ME/% |
| β-Agonist | | | | | | |
| Clorprenaline | 0.1 | 0.2 | y = 5 841 216.26 x + 87 425.55 | 0.1-1 | 0.995 | 95.64 |
| Tulobuterol | 0.1 | 0.2 | y = 6 027 646.87 x + 18 522.54 | 0.1-1 | 1.000 | 86.96 |
| Ractopamine | 0.1 | 0.2 | y = 2 747 991.54 x + 29 099.74 | 0.1-1 | 1.000 | 66.30 |
| Bambuterol | 0.1 | 0.2 | y = 5 194 463.70 x + 44 581.13 | 0.1-1 | 0.998 | 89.90 |
| Phenylethanolamine A | 0.1 | 0.2 | y = 4 057 591.55 x + 99 910.70 | 0.1-1 | 0.998 | 128.25 |
| Mabuterol | 0.1 | 0.2 | y = 5 193 449.89 x + 48 044.08 | 0.1-1 | 0.999 | 69.61 |
| Salbutamol | 0.1 | 0.2 | y = 13.89 x - 0.53 | 0.1-1 | 0.993 | 73.17 |
| Zilpaterol | 0.1 | 0.2 | y = 3.15 x - 0.27 | 0.1-1 | 0.991 | 65.09 |
| Cimaterol | 0.1 | 0.2 | y = 0.41 x - 0.01 | 0.1-1 | 0.995 | 49.36 |
| Terbutaline | 0.1 | 0.2 | y = 1.19 x - 0.01 | 0.1-1 | 0.997 | 55.38 |
| Clenbuterol | 0.1 | 0.2 | y = 0.88 x + 0.02 | 0.1-1 | 0.996 | 78.58 |
| Cimbuterol | 0.1 | 0.2 | y = 1.26 x + 0.09 | 0.1-1 | 0.997 | 73.32 |
| Brombuterol | 0.1 | 0.2 | y = 0.20 x + 0.01 | 0.1-1 | 0.997 | 62.23 |
| Formoterol | 0.1 | 0.2 | y = 1.48 x + 0.02 | 0.1-1 | 0.993 | 101.37 |
| Amphenicol | | | | | | |
| Chloramphenicol | 0.1 | 0.2 | y = 95 516.35 x - 14.83 | 0.1-1 | 0.999 | 69.46 |
| Tranquilizer | | | | | | |
| Chlorpromazine | 0.1 | 0.2 | y = 4 311 198.01 x - 123 375.27 | 0.1-1 | 0.998 | 91.62 |
| Methaqualone | 0.1 | 0.2 | y = 5 181 626.41 x - 67 016.44 | 0.1-1 | 0.998 | 76.57 |
| Xylazine | 0.1 | 0.2 | y = 1 414 153.91 x + 11 363.70 | 0.1-1 | 1.000 | 86.53 |
| Estazolam | 0.1 | 0.2 | y = 1 079 542.68 x + 12 236.56 | 0.1-1 | 0.998 | 116.99 |
| Midazolam | 0.1 | 0.2 | y = 1 694 281.78 x + 2 928.75 | 0.1-1 | 0.998 | 58.64 |
| Triazolam | 0.1 | 0.2 | y = 784 153.47 x - 427.84 | 0.1-1 | 0.999 | 107.84 |
| Alprazolam | 0.1 | 0.2 | y = 722 016.87 x - 7 329.70 | 0.1-1 | 0.999 | 73.13 |
| Diazepam | 0.1 | 0.2 | y = 563 673.41 x - 10 515.61 | 0.1-1 | 0.999 | 81.37 |
| Nitrazepam | 0.1 | 0.2 | y = 75 022.22 x - 1 339.64 | 0.1-1 | 0.997 | 57.22 |
| Oxazepam | 0.1 | 0.2 | y = 374 484.50 x + 7 089.87 | 0.1-1 | 0.999 | 263.27 |
| Clonazepam | 0.1 | 0.2 | y = 51 232.53 x + 520.24 | 0.1-1 | 0.996 | 52.90 |
| Lorazepam | 0.1 | 0.2 | y = 261 090.69 x + 2 415.79 | 0.1-1 | 0.997 | 234.22 |
| Phenobarbital | 50 | 100 | y = 442.00 x + 3 375.35 | 50-500 | 0.998 | 91.27 |
| Barbital | 50 | 100 | y = 349.63 x - 3 857.60 | 50-500 | 0.998 | 63.24 |
| Amobarbital | 50 | 100 | y = 1 200.29 x + 15 337.73 | 50-500 | 0.997 | 85.00 |
| Secobarbital | 50 | 100 | y = 554.73 x - 4 923.25 | 50-500 | 0.998 | 39.30 |
| Fluoroquinolone | | | | | | |
| Norfloxacin | 0.2 | 0.4 | y = 0.37 x - 0.03 | 0.2-2 | 0.993 | 268.90 |
| Pefloxacin | 0.2 | 0.4 | y = 0.47 x + 0.01 | 0.2-2 | 0.999 | 177.75 |
| Lomefloxacin | 0.2 | 0.4 | y = 0.13 x - 0.00 | 0.2-2 | 0.996 | 60.97 |
| Ofloxacin | 0.2 | 0.4 | y = 0.42 x - 0.01 | 0.2-2 | 0.997 | 111.81 |
| Nitroimidazole | | | | | | |
| Dimetridazole | 2 | 4 | y = 0.17 x - 0.04 | 1-10 | 0.999 | 86.52 |
| Dimetridazole-2-hydroxy | 2 | 4 | y = 0.05 x - 0.05 | 1-10 | 0.996 | 36.07 |
| Metronidazole-hydroxy | 2 | 4 | y = 0.09 x + 0.15 | 1-10 | 0.995 | 57.96 |
| Metronidazole | 2 | 4 | y = 0.52 x - 0.08 | 1-10 | 0.996 | 161.30 |
| Ronidazole | 2 | 4 | y = 0.72 x - 0.40 | 1-10 | 0.998 | 142.78 |
| Ipronidazole | 2 | 4 | y = 0.22 x + 0.08 | 1-10 | 0.999 | 78.37 |
| Tinidazole | 2 | 4 | y = 310 695.06 x + 52 015.05 | 1-10 | 1.000 | 91.53 |
| Quinoxaline | | | | | | |
| 2-QCA | 25 | 50 | y = 0.534 x + 0.03 | 25-250 | 0.996 | 112.92 |
| MQCA | 25 | 50 | y = 5.11 x + 0.01 | 25-250 | 0.998 | 120.07 |
| Carbadox | 25 | 50 | y = 35.29 x + 0.40 | 25-250 | 0.999 | 109.83 |
| Others | | | | | | |
| Dapsone | 0.1 | 0.2 | y = 1.46 x - 0.01 | 0.1-1 | 0.997 | 95.36 |
| Leucomalachite green | 0.1 | 0.2 | y = 0.59 x - 0.06 | 0.1-1 | 0.995 | 108.42 |
| Malachite green | 0.1 | 0.2 | y = 1.46 x - 0.18 | 0.1-1 | 0.996 | 60.44 |
| Clonidine | 0.1 | 0.2 | y = 301 538.77 x - 7 590.75 | 0.1-1 | 0.997 | 76.02 |
| Cyproheptadine | 0.1 | 0.2 | y = 2 368 886.83 x - 24 673.13 | 0.1-1 | 0.998 | 78.51 |
| Carbofuran | 0.1 | 0.2 | y = 0.82 x - 0.00 | 0.1-1 | 0.999 | 49.77 |
| Chlordimeform | 0.1 | 0.2 | y = 1 083 880.45 x + 15 761.62 | 0.1-1 | 0.996 | 84.15 |
| Fipronil | 0.1 | 0.2 | y = 0.86 x - 0.03 | 0.1-1 | 1.000 | 122.19 |
), ArticleFig(id=1194703708832375425, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=CN, label=Table 3, caption=
The LODs, LOQs, linear equations, ranges, and MEs for 53 analytes
, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | LOD/μg·kg-1 | LOQ/μg·kg-1 | Linear equation | Linear range/μg·L-1 | r | ME/% |
| β-Agonist | | | | | | |
| Clorprenaline | 0.1 | 0.2 | y = 5 841 216.26 x + 87 425.55 | 0.1-1 | 0.995 | 95.64 |
| Tulobuterol | 0.1 | 0.2 | y = 6 027 646.87 x + 18 522.54 | 0.1-1 | 1.000 | 86.96 |
| Ractopamine | 0.1 | 0.2 | y = 2 747 991.54 x + 29 099.74 | 0.1-1 | 1.000 | 66.30 |
| Bambuterol | 0.1 | 0.2 | y = 5 194 463.70 x + 44 581.13 | 0.1-1 | 0.998 | 89.90 |
| Phenylethanolamine A | 0.1 | 0.2 | y = 4 057 591.55 x + 99 910.70 | 0.1-1 | 0.998 | 128.25 |
| Mabuterol | 0.1 | 0.2 | y = 5 193 449.89 x + 48 044.08 | 0.1-1 | 0.999 | 69.61 |
| Salbutamol | 0.1 | 0.2 | y = 13.89 x - 0.53 | 0.1-1 | 0.993 | 73.17 |
| Zilpaterol | 0.1 | 0.2 | y = 3.15 x - 0.27 | 0.1-1 | 0.991 | 65.09 |
| Cimaterol | 0.1 | 0.2 | y = 0.41 x - 0.01 | 0.1-1 | 0.995 | 49.36 |
| Terbutaline | 0.1 | 0.2 | y = 1.19 x - 0.01 | 0.1-1 | 0.997 | 55.38 |
| Clenbuterol | 0.1 | 0.2 | y = 0.88 x + 0.02 | 0.1-1 | 0.996 | 78.58 |
| Cimbuterol | 0.1 | 0.2 | y = 1.26 x + 0.09 | 0.1-1 | 0.997 | 73.32 |
| Brombuterol | 0.1 | 0.2 | y = 0.20 x + 0.01 | 0.1-1 | 0.997 | 62.23 |
| Formoterol | 0.1 | 0.2 | y = 1.48 x + 0.02 | 0.1-1 | 0.993 | 101.37 |
| Amphenicol | | | | | | |
| Chloramphenicol | 0.1 | 0.2 | y = 95 516.35 x - 14.83 | 0.1-1 | 0.999 | 69.46 |
| Tranquilizer | | | | | | |
| Chlorpromazine | 0.1 | 0.2 | y = 4 311 198.01 x - 123 375.27 | 0.1-1 | 0.998 | 91.62 |
| Methaqualone | 0.1 | 0.2 | y = 5 181 626.41 x - 67 016.44 | 0.1-1 | 0.998 | 76.57 |
| Xylazine | 0.1 | 0.2 | y = 1 414 153.91 x + 11 363.70 | 0.1-1 | 1.000 | 86.53 |
| Estazolam | 0.1 | 0.2 | y = 1 079 542.68 x + 12 236.56 | 0.1-1 | 0.998 | 116.99 |
| Midazolam | 0.1 | 0.2 | y = 1 694 281.78 x + 2 928.75 | 0.1-1 | 0.998 | 58.64 |
| Triazolam | 0.1 | 0.2 | y = 784 153.47 x - 427.84 | 0.1-1 | 0.999 | 107.84 |
| Alprazolam | 0.1 | 0.2 | y = 722 016.87 x - 7 329.70 | 0.1-1 | 0.999 | 73.13 |
| Diazepam | 0.1 | 0.2 | y = 563 673.41 x - 10 515.61 | 0.1-1 | 0.999 | 81.37 |
| Nitrazepam | 0.1 | 0.2 | y = 75 022.22 x - 1 339.64 | 0.1-1 | 0.997 | 57.22 |
| Oxazepam | 0.1 | 0.2 | y = 374 484.50 x + 7 089.87 | 0.1-1 | 0.999 | 263.27 |
| Clonazepam | 0.1 | 0.2 | y = 51 232.53 x + 520.24 | 0.1-1 | 0.996 | 52.90 |
| Lorazepam | 0.1 | 0.2 | y = 261 090.69 x + 2 415.79 | 0.1-1 | 0.997 | 234.22 |
| Phenobarbital | 50 | 100 | y = 442.00 x + 3 375.35 | 50-500 | 0.998 | 91.27 |
| Barbital | 50 | 100 | y = 349.63 x - 3 857.60 | 50-500 | 0.998 | 63.24 |
| Amobarbital | 50 | 100 | y = 1 200.29 x + 15 337.73 | 50-500 | 0.997 | 85.00 |
| Secobarbital | 50 | 100 | y = 554.73 x - 4 923.25 | 50-500 | 0.998 | 39.30 |
| Fluoroquinolone | | | | | | |
| Norfloxacin | 0.2 | 0.4 | y = 0.37 x - 0.03 | 0.2-2 | 0.993 | 268.90 |
| Pefloxacin | 0.2 | 0.4 | y = 0.47 x + 0.01 | 0.2-2 | 0.999 | 177.75 |
| Lomefloxacin | 0.2 | 0.4 | y = 0.13 x - 0.00 | 0.2-2 | 0.996 | 60.97 |
| Ofloxacin | 0.2 | 0.4 | y = 0.42 x - 0.01 | 0.2-2 | 0.997 | 111.81 |
| Nitroimidazole | | | | | | |
| Dimetridazole | 2 | 4 | y = 0.17 x - 0.04 | 1-10 | 0.999 | 86.52 |
| Dimetridazole-2-hydroxy | 2 | 4 | y = 0.05 x - 0.05 | 1-10 | 0.996 | 36.07 |
| Metronidazole-hydroxy | 2 | 4 | y = 0.09 x + 0.15 | 1-10 | 0.995 | 57.96 |
| Metronidazole | 2 | 4 | y = 0.52 x - 0.08 | 1-10 | 0.996 | 161.30 |
| Ronidazole | 2 | 4 | y = 0.72 x - 0.40 | 1-10 | 0.998 | 142.78 |
| Ipronidazole | 2 | 4 | y = 0.22 x + 0.08 | 1-10 | 0.999 | 78.37 |
| Tinidazole | 2 | 4 | y = 310 695.06 x + 52 015.05 | 1-10 | 1.000 | 91.53 |
| Quinoxaline | | | | | | |
| 2-QCA | 25 | 50 | y = 0.534 x + 0.03 | 25-250 | 0.996 | 112.92 |
| MQCA | 25 | 50 | y = 5.11 x + 0.01 | 25-250 | 0.998 | 120.07 |
| Carbadox | 25 | 50 | y = 35.29 x + 0.40 | 25-250 | 0.999 | 109.83 |
| Others | | | | | | |
| Dapsone | 0.1 | 0.2 | y = 1.46 x - 0.01 | 0.1-1 | 0.997 | 95.36 |
| Leucomalachite green | 0.1 | 0.2 | y = 0.59 x - 0.06 | 0.1-1 | 0.995 | 108.42 |
| Malachite green | 0.1 | 0.2 | y = 1.46 x - 0.18 | 0.1-1 | 0.996 | 60.44 |
| Clonidine | 0.1 | 0.2 | y = 301 538.77 x - 7 590.75 | 0.1-1 | 0.997 | 76.02 |
| Cyproheptadine | 0.1 | 0.2 | y = 2 368 886.83 x - 24 673.13 | 0.1-1 | 0.998 | 78.51 |
| Carbofuran | 0.1 | 0.2 | y = 0.82 x - 0.00 | 0.1-1 | 0.999 | 49.77 |
| Chlordimeform | 0.1 | 0.2 | y = 1 083 880.45 x + 15 761.62 | 0.1-1 | 0.996 | 84.15 |
| Fipronil | 0.1 | 0.2 | y = 0.86 x - 0.03 | 0.1-1 | 1.000 | 122.19 |
), ArticleFig(id=1194703708983370372, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=EN, label=null, caption=null, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | 1 LOQ | | 2 LOQ | | 10 LOQ |
| Recovery/% | RSD/% | | Recovery/% | RSD/% | | Recovery/% | RSD/% |
| β-Agonist | | | | | | | | |
| Clorprenaline | 81.65 | 8.99 | 83.27 | 5.52 | 93.53 | 6.40 |
| Tulobuterol | 84.69 | 7.12 | 86.37 | 3.26 | 90.42 | 2.34 |
| Ractopamine | 74.17 | 10.29 | 71.26 | 8.35 | 84.82 | 5.42 |
| Bambuterol | 76.66 | 9.54 | 87.41 | 5.04 | 98.90 | 1.99 |
| Phenylethanolamine A | 70.40 | 6.93 | 72.93 | 5.44 | 92.14 | 4.17 |
| Mabuterol | 77.92 | 6.10 | 87.31 | 2.51 | 92.87 | 2.97 |
| Salbutamol | 101.52 | 9.87 | 93.61 | 9.07 | 94.50 | 8.53 |
| Zilpaterol | 114.34 | 5.21 | 99.62 | 5.73 | 89.48 | 10.47 |
| Cimaterol | 106.96 | 7.20 | 83.02 | 11.04 | 92.25 | 7.08 |
| Terbutaline | 94.65 | 9.77 | 89.19 | 9.41 | 82.22 | 8.99 |
| Clenbuterol | 106.31 | 5.20 | 116.42 | 10.44 | 117.36 | 7.95 |
| Cimbuterol | 79.27 | 10.45 | 86.07 | 9.81 | 118.64 | 7.43 |
| Brombuterol | 102.95 | 9.44 | 113.33 | 11.05 | 117.89 | 1.95 |
| Formoterol | 111.92 | 4.43 | 105.16 | 4.67 | 118.70 | 3.44 |
| Amphenicol | | | | | | |
| Chloramphenicol | 85.65 | 2.32 | 88.29 | 2.71 | 94.70 | 3.43 |
| Tranquilizer | | | | | | |
| Chlorpromazine | 70.92 | 4.22 | 81.41 | 3.42 | 84.73 | 9.71 |
| Methaqualone | 95.55 | 8.78 | 93.92 | 5.17 | 96.72 | 3.60 |
| Xylazine | 76.42 | 5.38 | 88.01 | 3.18 | 97.89 | 3.97 |
| Estazolam | 94.54 | 6.29 | 93.84 | 3.96 | 102.29 | 6.10 |
| Midazolam | 80.00 | 7.39 | 93.12 | 3.64 | 102.31 | 6.14 |
| Triazolam | 92.08 | 7.38 | 107.75 | 2.21 | 116.78 | 4.37 |
| Alprazolam | 110.67 | 8.49 | 116.83 | 2.65 | 118.03 | 4.62 |
| Diazepam | 97.93 | 10.26 | 102.39 | 6.70 | 106.23 | 4.73 |
| Nitrazepam | 74.28 | 7.48 | 81.54 | 8.25 | 86.06 | 4.63 |
| Oxazepam | 78.74 | 8.78 | 82.45 | 8.16 | 93.86 | 4.92 |
| Clonazepam | 86.37 | 6.43 | 81.12 | 10.44 | 95.40 | 8.76 |
| Lorazepam | 80.59 | 8.15 | 81.34 | 7.86 | 91.48 | 3.71 |
| Phenobarbital | 83.52 | 3.85 | 96.46 | 5.93 | 100.19 | 1.45 |
| Barbital | 93.87 | 7.54 | 87.32 | 5.99 | 97.23 | 6.21 |
| Amobarbital | 75.73 | 4.05 | 87.45 | 6.94 | 94.54 | 3.05 |
| Secobarbital | 85.78 | 4.88 | 86.79 | 6.58 | 86.73 | 5.35 |
| Fluoroquinolone | | | | | | |
| Norfloxacin | 100.39 | 5.02 | 89.32 | 1.93 | 84.17 | 4.61 |
| Pefloxacin | 86.99 | 2.91 | 94.55 | 4.22 | 95.97 | 3.97 |
| Lomefloxacin | 109.14 | 4.29 | 104.26 | 2.36 | 104.11 | 3.60 |
| Ofloxacin | 112.11 | 4.70 | 101.32 | 2.14 | 96.25 | 7.12 |
| Nitroimidazole | | | | | | |
| Dimetridazole | 104.62 | 8.29 | 89.95 | 1.55 | 94.29 | 9.77 |
| Dimetridazole-2-hydroxy | 113.47 | 8.58 | 99.60 | 5.50 | 95.19 | 12.07 |
| Metronidazole-hydroxy | 97.53 | 7.23 | 101.34 | 4.77 | 97.18 | 5.16 |
| Metronidazole | 86.93 | 10.67 | 90.35 | 4.39 | 91.06 | 7.65 |
| Ronidazole | 113.83 | 7.29 | 92.73 | 4.15 | 94.21 | 9.84 |
| Ipronidazole | 92.84 | 8.01 | 81.48 | 8.47 | 86.78 | 10.11 |
| Tinidazole | 78.74 | 8.11 | 88.82 | 5.84 | 101.48 | 5.16 |
| Quinoxaline | | | | | | |
| 2-QCA | 84.68 | 10.03 | 100.67 | 8.45 | 98.38 | 1.21 |
| MQCA | 109.14 | 6.24 | 100.36 | 7.68 | 98.07 | 0.69 |
| Carbadox | 104.18 | 9.14 | 101.76 | 6.11 | 99.31 | 6.42 |
| Others | | | | | | |
| Dapsone | 89.94 | 4.16 | 97.97 | 3.55 | 96.88 | 6.76 |
| Leucomalachite green | 105.46 | 10.96 | 80.71 | 8.69 | 94.35 | 3.47 |
| Malachite green | 103.38 | 8.54 | 80.43 | 2.38 | 71.39 | 1.33 |
| Clonidine | 95.29 | 9.74 | 86.11 | 5.31 | 87.89 | 8.25 |
| Cyproheptadine | 74.09 | 3.94 | 71.91 | 6.14 | 83.47 | 2.67 |
| Carbofuran | 88.18 | 4.05 | 93.99 | 5.05 | 98.36 | 2.23 |
| Chlordimeform | 78.45 | 5.35 | 80.89 | 5.82 | 101.92 | 2.03 |
| Fipronil | 96.04 | 4.31 | 90.39 | 4.15 | 91.07 | 6.02 |
), ArticleFig(id=1194703709197279879, tenantId=1146029695717560320, journalId=1189982191388893191, articleId=1193259087325524515, language=CN, label=Table 4, caption=
Recoveries and RSDs for 53 compounds at three spiked levels
, figureFileSmall=null, figureFileBig=null, tableContent=
| Compound | 1 LOQ | | 2 LOQ | | 10 LOQ |
| Recovery/% | RSD/% | | Recovery/% | RSD/% | | Recovery/% | RSD/% |
| β-Agonist | | | | | | | | |
| Clorprenaline | 81.65 | 8.99 | 83.27 | 5.52 | 93.53 | 6.40 |
| Tulobuterol | 84.69 | 7.12 | 86.37 | 3.26 | 90.42 | 2.34 |
| Ractopamine | 74.17 | 10.29 | 71.26 | 8.35 | 84.82 | 5.42 |
| Bambuterol | 76.66 | 9.54 | 87.41 | 5.04 | 98.90 | 1.99 |
| Phenylethanolamine A | 70.40 | 6.93 | 72.93 | 5.44 | 92.14 | 4.17 |
| Mabuterol | 77.92 | 6.10 | 87.31 | 2.51 | 92.87 | 2.97 |
| Salbutamol | 101.52 | 9.87 | 93.61 | 9.07 | 94.50 | 8.53 |
| Zilpaterol | 114.34 | 5.21 | 99.62 | 5.73 | 89.48 | 10.47 |
| Cimaterol | 106.96 | 7.20 | 83.02 | 11.04 | 92.25 | 7.08 |
| Terbutaline | 94.65 | 9.77 | 89.19 | 9.41 | 82.22 | 8.99 |
| Clenbuterol | 106.31 | 5.20 | 116.42 | 10.44 | 117.36 | 7.95 |
| Cimbuterol | 79.27 | 10.45 | 86.07 | 9.81 | 118.64 | 7.43 |
| Brombuterol | 102.95 | 9.44 | 113.33 | 11.05 | 117.89 | 1.95 |
| Formoterol | 111.92 | 4.43 | 105.16 | 4.67 | 118.70 | 3.44 |
| Amphenicol | | | | | | |
| Chloramphenicol | 85.65 | 2.32 | 88.29 | 2.71 | 94.70 | 3.43 |
| Tranquilizer | | | | | | |
| Chlorpromazine | 70.92 | 4.22 | 81.41 | 3.42 | 84.73 | 9.71 |
| Methaqualone | 95.55 | 8.78 | 93.92 | 5.17 | 96.72 | 3.60 |
| Xylazine | 76.42 | 5.38 | 88.01 | 3.18 | 97.89 | 3.97 |
| Estazolam | 94.54 | 6.29 | 93.84 | 3.96 | 102.29 | 6.10 |
| Midazolam | 80.00 | 7.39 | 93.12 | 3.64 | 102.31 | 6.14 |
| Triazolam | 92.08 | 7.38 | 107.75 | 2.21 | 116.78 | 4.37 |
| Alprazolam | 110.67 | 8.49 | 116.83 | 2.65 | 118.03 | 4.62 |
| Diazepam | 97.93 | 10.26 | 102.39 | 6.70 | 106.23 | 4.73 |
| Nitrazepam | 74.28 | 7.48 | 81.54 | 8.25 | 86.06 | 4.63 |
| Oxazepam | 78.74 | 8.78 | 82.45 | 8.16 | 93.86 | 4.92 |
| Clonazepam | 86.37 | 6.43 | 81.12 | 10.44 | 95.40 | 8.76 |
| Lorazepam | 80.59 | 8.15 | 81.34 | 7.86 | 91.48 | 3.71 |
| Phenobarbital | 83.52 | 3.85 | 96.46 | 5.93 | 100.19 | 1.45 |
| Barbital | 93.87 | 7.54 | 87.32 | 5.99 | 97.23 | 6.21 |
| Amobarbital | 75.73 | 4.05 | 87.45 | 6.94 | 94.54 | 3.05 |
| Secobarbital | 85.78 | 4.88 | 86.79 | 6.58 | 86.73 | 5.35 |
| Fluoroquinolone | | | | | | |
| Norfloxacin | 100.39 | 5.02 | 89.32 | 1.93 | 84.17 | 4.61 |
| Pefloxacin | 86.99 | 2.91 | 94.55 | 4.22 | 95.97 | 3.97 |
| Lomefloxacin | 109.14 | 4.29 | 104.26 | 2.36 | 104.11 | 3.60 |
| Ofloxacin | 112.11 | 4.70 | 101.32 | 2.14 | 96.25 | 7.12 |
| Nitroimidazole | | | | | | |
| Dimetridazole | 104.62 | 8.29 | 89.95 | 1.55 | 94.29 | 9.77 |
| Dimetridazole-2-hydroxy | 113.47 | 8.58 | 99.60 | 5.50 | 95.19 | 12.07 |
| Metronidazole-hydroxy | 97.53 | 7.23 | 101.34 | 4.77 | 97.18 | 5.16 |
| Metronidazole | 86.93 | 10.67 | 90.35 | 4.39 | 91.06 | 7.65 |
| Ronidazole | 113.83 | 7.29 | 92.73 | 4.15 | 94.21 | 9.84 |
| Ipronidazole | 92.84 | 8.01 | 81.48 | 8.47 | 86.78 | 10.11 |
| Tinidazole | 78.74 | 8.11 | 88.82 | 5.84 | 101.48 | 5.16 |
| Quinoxaline | | | | | | |
| 2-QCA | 84.68 | 10.03 | 100.67 | 8.45 | 98.38 | 1.21 |
| MQCA | 109.14 | 6.24 | 100.36 | 7.68 | 98.07 | 0.69 |
| Carbadox | 104.18 | 9.14 | 101.76 | 6.11 | 99.31 | 6.42 |
| Others | | | | | | |
| Dapsone | 89.94 | 4.16 | 97.97 | 3.55 | 96.88 | 6.76 |
| Leucomalachite green | 105.46 | 10.96 | 80.71 | 8.69 | 94.35 | 3.47 |
| Malachite green | 103.38 | 8.54 | 80.43 | 2.38 | 71.39 | 1.33 |
| Clonidine | 95.29 | 9.74 | 86.11 | 5.31 | 87.89 | 8.25 |
| Cyproheptadine | 74.09 | 3.94 | 71.91 | 6.14 | 83.47 | 2.67 |
| Carbofuran | 88.18 | 4.05 | 93.99 | 5.05 | 98.36 | 2.23 |
| Chlordimeform | 78.45 | 5.35 | 80.89 | 5.82 | 101.92 | 2.03 |
| Fipronil | 96.04 | 4.31 | 90.39 | 4.15 | 91.07 | 6.02 |
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